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Cas:1476-23-9
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inquiryProduct Name: ALLYL ISOCYANATE CAS: 1476-23-9 MF: C4H5NO MW: 83.09 EINECS: 629-197-7 Mol File: 1476-23-9.mol ALLYL ISOCYANATE Structure ALLYL ISOCYANATE Chemical Properties Boiling point 87-89 °C(lit.) density 0.94 g/m
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Conditions | Yield |
---|---|
With hydrogenchloride; tetrabutylammomium bromide; sodium nitrite In water; toluene at 0℃; for 5.5h; Temperature; | 92% |
methyl allylcarbamate
allylisocyanate
Conditions | Yield |
---|---|
With trichloro(dichloromethyl)silane at 95 - 150℃; for 0.5h; | 81% |
Conditions | Yield |
---|---|
With hydrogenchloride; toluene dann Erhitzen bis auf 220grad oder beim Behandeln mit Chlorwasserstoff bei 130grad; |
allyl-carbamic acid-(2-hydroxy-phenyl ester)
A
benzene-1,2-diol
B
allylisocyanate
Conditions | Yield |
---|---|
at 240 - 270℃; |
allyl-carbamic acid-(2-hydroxy-phenyl ester)
allylisocyanate
Conditions | Yield |
---|---|
at 240 - 270℃; |
Conditions | Yield |
---|---|
Behandlung des entstandenen Allylcarbamidsaeure-chlorids mit Ca(OH)2 oder mit Aethylenoxyd-Derivaten; |
Conditions | Yield |
---|---|
With phosgene; toluene Behandeln des Reaktionsgemisches mit Calciumoxid oder mit Chinolin; |
trimethylsilyl allylcarbamate
allylisocyanate
Conditions | Yield |
---|---|
With tetrachlorosilane | |
Stage #1: trimethylsilyl allylcarbamate With chloro-trimethyl-silane; 1,1,1,3,3,3-hexamethyl-disilazane for 72h; Stage #2: at 200℃; Further stages.; |
O-Allylthiocarbamat
allylisocyanate
Conditions | Yield |
---|---|
With magnesium sulfate; silver(l) oxide In tetrachloromethane |
Conditions | Yield |
---|---|
(i) Et3N, isopropylbenzene, (ii) Cl2CHSiCl3; Multistep reaction; |
Conditions | Yield |
---|---|
With carbon disulfide; sodium hydroxide 1.) 2h, heating, 2.) 35-40 deg C, 30 min; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
With Phenyltrichlorosilane at 150 - 210℃; | A 51 % Chromat. B 43.6 % Chromat. C 5.4 % Chromat. |
Conditions | Yield |
---|---|
With pyrographite In ethyl acetate Condensation; Heating; |
allylisocyanate
Conditions | Yield |
---|---|
With hydrogen sulfide at 20℃; |
Conditions | Yield |
---|---|
With 2-chloropyridine; trifluoromethylsulfonic anhydride In dichloromethane at 20℃; for 1.08333h; |
allylisocyanate
anthranilic acid nitrile
2-(3-allylureido)benzonitrile
Conditions | Yield |
---|---|
for 48h; Ambient temperature; | 100% |
for 48h; Ambient temperature; | 100% |
In dichloromethane for 3h; Ambient temperature; | 88% |
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate In diethyl ether for 3h; Ambient temperature; | 100% |
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate In diethyl ether for 3h; Ambient temperature; | 100% |
N-amino{3,4-difluoro-2-[(2-fluoro-4-iodophenyl)amino]phenyl}carboxamide; 2-(4-iodo-2-fluoro-phenylamino)-3,4-difluoro-benzoic acid hydrazide
allylisocyanate
4'-allyl-1'[3,4-difluoro-2-(2-fluoro-4-iodo-phenylamino)]-semicarbazole
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 2h; | 100% |
Conditions | Yield |
---|---|
100% | |
With pyridine In toluene for 2h; Reflux; |
allylisocyanate
4-chlorobenzoic acid hydrazide
2-[(4-chlorophenyl)carbonyl]-N-(prop-2-en-1-yl)hydrazinecarboxamide
Conditions | Yield |
---|---|
In tetrahydrofuran at 50℃; for 2h; | 100% |
In tetrahydrofuran at 50℃; for 2h; | 100% |
allylisocyanate
5-diazoimidazole-4-carboxamide
3-allyl-8-carbamoyl-[3H]-imidazo[5,1-d]-1,2,3,5-tetrazin-4-one
Conditions | Yield |
---|---|
In dimethyl sulfoxide at 25℃; for 24h; Inert atmosphere; | 100% |
4-ferrocenylbutan-1-ol
allylisocyanate
(4-ferrocenylbutyl)-N-allylcarbamate
Conditions | Yield |
---|---|
In dichloromethane for 2.5h; Inert atmosphere; Reflux; | 99.4% |
N-phenyl-2-[(triphenylphosphoranylidene)amino]benzenesulfonamide
allylisocyanate
2-phenyl-N-(prop-2-enyl)-2H-1,2,4-benzothiadiazin-3-amine 1,1-dioxide
Conditions | Yield |
---|---|
In toluene at 110℃; for 3h; | 99% |
3-cyclopentyl-2-(3,4-dichlorophenyl)propionamide
allylisocyanate
1-allyl-3-[3-cyclopentyl-2-(3,4-dichlorophenyl)propionyl]urea
Conditions | Yield |
---|---|
In toluene for 24h; Reflux; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With water; triethylamine In 1,4-dioxane at 20℃; for 0.05h; | 98.5% |
Stage #1: allylisocyanate With [nido-6-Mn(CO)3B9H13][NMe4] In dichloromethane for 0.166667h; Inert atmosphere; Sonication; Stage #2: In dichloromethane for 0.166667h; Irradiation; Inert atmosphere; | 92% |
With [Pr(SPh)3(THF)3] In tetrahydrofuran at 60℃; for 12h; Inert atmosphere; | 85% |
Conditions | Yield |
---|---|
In toluene for 18h; Heating; | 98% |
Conditions | Yield |
---|---|
In tetrachloromethane | 98% |
Conditions | Yield |
---|---|
With 1,3-bis(2,6-diisopropylphenyl)dihydroimidazol-2-ylidene at 20℃; for 1h; | 98% |
With tetraethylammonium 2-(carbamoyl)benzoate at 50℃; for 6h; Neat (no solvent); | 95% |
With 1,3-dimethyl-4,5-diphenyl-2-(propan-2-ylidene)-2,3-dihydro-1H-imidazole; 1,8-diazabicyclo[5.4.0]undec-7-ene In toluene at 20℃; for 48h; Inert atmosphere; Glovebox; | 89% |
3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-D-glucopyranose
allylisocyanate
3,4,6-tri-O-acetyl-1-O-(N-allyl)carbamoyl-2-deoxy-2-phthalimido-β-D-glucopyranose
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane for 12h; Ambient temperature; | 98% |
((2S,3R)-3-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)oxiran-2-yl)methanol
allylisocyanate
Allyl-carbamic acid (2S,3R)-3-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-oxiranylmethyl ester
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In benzene at 60℃; | 98% |
(6-methoxyquinolin-4-yl)methanol
allylisocyanate
(6-methoxyquinolin-4-yl)methyl allylcarbamate
Conditions | Yield |
---|---|
With dibutyltin dilaurate In dichloromethane for 6h; Inert atmosphere; Reflux; | 98% |
Conditions | Yield |
---|---|
In dichloromethane at 20℃; | 98% |
3-amino-12-N-methylcytisine
allylisocyanate
N-(12-methylcytisin-3-yl)-N-allylurea
Conditions | Yield |
---|---|
In benzene at 20℃; | 98% |
Conditions | Yield |
---|---|
In benzene at 20℃; | 98% |
Conditions | Yield |
---|---|
With methyllithium lithium bromide In diethyl ether at -78℃; | 98% |
With methyllithium; lithium bromide In diethyl ether at -78℃; for 1h; chemoselective reaction; | 98% |
Conditions | Yield |
---|---|
With chloro(1,5-cyclooctadiene)rhodium(I) dimer; triphenyl-arsane In 1,4-dioxane at 160℃; chemoselective reaction; | 98% |
allylisocyanate
2-(3-amino-4-hydroxyphenyl)-7-methyl-5,6,7,8-tetrahydroimidazo<1,2-a>pyridine
1-Allyl-3-[2-hydroxy-5-(7-methyl-5,6,7,8-tetrahydro-imidazo[1,2-a]pyridin-2-yl)-phenyl]-urea
Conditions | Yield |
---|---|
In tetrahydrofuran; methanol for 2h; Ambient temperature; | 97% |
Conditions | Yield |
---|---|
at 50 - 60℃; for 3.5h; | 96% |
4-((6,7-dimethoxyquinolin-4-yl)oxy)aniline
allylisocyanate
Conditions | Yield |
---|---|
In water; N,N-dimethyl-formamide | 96% |
allylisocyanate
6-methylisocytosine
1-(3-(6-methyl-4-oxo-1,4-dihydropyrimidin-2-yl)ureido)prop-2-ene
Conditions | Yield |
---|---|
In dimethyl sulfoxide at 170℃; | 96% |
diphenylmethylpiperazine
allylisocyanate
N-allyl-4-(diphenylmethyl)piperazine-1-carboxamide
Conditions | Yield |
---|---|
Stage #1: diphenylmethylpiperazine With triethylamine In dichloromethane for 0.166667h; Cooling with ice; Stage #2: allylisocyanate In dichloromethane at 20℃; | 96% |
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 20℃; for 7h; | 96% |
Conditions | Yield |
---|---|
With platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex at 40 - 85℃; for 4.5h; | 95.7% |
Conditions | Yield |
---|---|
In tetrachloromethane | 95% |
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