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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

Bicine Manufacturer/High quality/Best price/In stock

Cas:150-25-4

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Hangzhou Dingyan Chem Co., Ltd

Items Standard Result Appearance White crystalline powder Complies Assay 98.0%-101.0%

High purity Various Specifications Bicine CAS:150-25-4

Cas:150-25-4

Min.Order:1 Gram

FOB Price: $100.0 / 500.0

Type:Manufacturers

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality N,N-Dihydroxyethylglycine supplier in China

Cas:150-25-4

Min.Order:0 Metric Ton

Negotiable

Type:Manufacturers

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Wuhan Fortuna Chemical Co.,Ltd

High purity N,N`-Bis(2-Hydroxyethyl)glycine sodium salt CAS 150-25-4 Bicine with attractive price Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical &

High purity N,N`-Bis(2-Hydroxyethyl)glycine sodium salt CAS 150-25-4 Bicine with attractive price

Cas:150-25-4

Min.Order:1 Kilogram

FOB Price: $10.0

Type:Trading Company

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Henan Allgreen Chemical Co.,Ltd

Good price Storage:Sealed, dry, microtherm , avoid light and smell. Package:As per customer's demand Application:Biological buffer Transportation:By Sea or By Air or By Courier Port:Shanghai, Qingdao Port

Bicine 150-25-4

Cas:150-25-4

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply N,N-bis(2-hydroxyethyl)glycine

Cas:150-25-4

Min.Order:1

Negotiable

Type:Other

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Yuan Shi(SuQian)Biotechnology Co.,Ltd

We could give you: 1. Best quality in your requirement 2. Competitive price in China market 3. mature Technical support 4. Professional logistic support 5 . Full experience of large numbers containers loading in Chinese sea p

BICINE

Cas:150-25-4

Min.Order:1 Kilogram

FOB Price: $1.0 / 2000.0

Type:Manufacturers

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

N,N-Bis-(2-hydroxyethyl)-glycine

Cas:150-25-4

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Hubei DiBo chemical co., LTD

Name:Bicine The alias:Bicine CAS NO:150-25-4 Molecular formula:C6H17NO4 Molecular weight:167.2035 Product Quality 12 years of chemical raw materials Mature operation of the industry System stability Data storage Security without vulnera

CAS:150-25-4/Bicine/High purity

Cas:150-25-4

Min.Order:25 Kilogram

FOB Price: $1.0 / 2.0

Type:Other

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Leader Biochemical Group

About Product Details Item Specification Test Results Appearance White crystalline powder Conform

China Largest Manufacturer Supply High Quality N,N-Bis(2-hydroxyethyl)glycine CAS 150-25-4

Cas:150-25-4

Min.Order:1 Kilogram

FOB Price: $1.0 / 5.0

Type:Lab/Research institutions

inquiry

Henan Tianfu Chemical Co., Ltd.

Product Name: Bicine Synonyms: DI(HYDROXYETHYL)GLYCINE;DIETHYLOLGLYCINE;DIETHANOLGLYCINE;[BIS-(2-HYDROXY-ETHYL)-AMINO]-ACETIC ACID;BICINE;BICINE BUFFER;LABOTEST-BB LT00452695;n,n-bis(2-hydroxyethyl)-glycin

Bicine--

Cas:150-25-4

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con

150-25-4 Bicine

Cas:150-25-4

Min.Order:1 Kilogram

FOB Price: $15.0 / 50.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

New production CAS 150-25-4 with best quality

Cas:150-25-4

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W

Bicine CAS150-25-4

Cas:150-25-4

Min.Order:1 Kilogram

FOB Price: $7.0 / 9.0

Type:Trading Company

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Henan Sinotech Import&Export Corporation

Name: Bicine Molecular formula:C6H13NO4 Molecular wt:163.17 CAS No: 150-25-4 Appearance:white crystal powder Storage:Store in cool and dry place, away from sun light. Package:25kg Application:Biological buffer Transportation:By sea or by air Port:Qi

Bicine CAS:150-25-4

Cas:150-25-4

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Glycine,N,N-bis(2-hydroxyethyl)- 150-25-4

Cas:150-25-4

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

Bicine CAS:150-25-4 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates, stero

Bicine CAS:150-25-4

Cas:150-25-4

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Glycine,N,N-bis(2-hydroxyethyl)-

Cas:150-25-4

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Changchun Artel lmport and Export trade company

Product Detail Minimum Order Qty. 10 Gram

High-quality products and high-quality prices from factory CAS NO.150-25-4

Cas:150-25-4

Min.Order:10 Gram

Negotiable

Type:Trading Company

inquiry

Hubei Jiutian Bio-medical Technology Co., Ltd

1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie

CAS 150-25-4 Bicine

Cas:150-25-4

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Glycine,N,N-bis(2-hydroxyethyl)-

Cas:150-25-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

N,N-Dihydroxyethylglycine

Cas:150-25-4

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

N,N-Bis(2-Hydroxyethyl)Glycine

Cas:150-25-4

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

Bicine

Cas:150-25-4

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Afine Chemicals Limited

Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments

BICINE

Cas:150-25-4

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Bicine

Cas:150-25-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

Bicine

Cas:150-25-4

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality N,N-Dihydroxyethylglycine

Cas:150-25-4

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

Hangzhou Lingrui Chemical Co.,Ltd.

Bicine 150-25-4Appearance:white powder Storage:Room temperature Package:according to customers' requirements Application:For organic use Transportation:By air(EMS or EUB or FedEx or TNT ect...) or by sea(FOB or CIF or CNF ect...)or according to you

Bicine 150-25-4

Cas:150-25-4

Min.Order:1 Gram

Negotiable

Type:Other

inquiry

SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

Bicine

Cas:150-25-4

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

inquiry

Synthetic route

Glyoxal
131543-46-9

Glyoxal

2,2'-iminobis[ethanol]
111-42-2

2,2'-iminobis[ethanol]

N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

Conditions
ConditionsYield
In ethanol; water at 70℃; for 16h;96%
oxirane
75-21-8

oxirane

GlyOEt*HCl
459-73-4

GlyOEt*HCl

N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

Conditions
ConditionsYield
at 25℃;
at 25℃; im Rohr;
4-(2-hydroxy-ethyl)-morpholin-2-one
5038-12-0

4-(2-hydroxy-ethyl)-morpholin-2-one

N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

Conditions
ConditionsYield
With water at 25℃; Rate constant; at pD 7.0; hydrolysis also in humid air;
With water at 120℃;
With water (heating);
With water
N,N-bis-(2-chloro-ethyl)-glycine
98486-41-0

N,N-bis-(2-chloro-ethyl)-glycine

A

4-(2-chloro-ethyl)-morpholin-2-one
86240-92-8

4-(2-chloro-ethyl)-morpholin-2-one

B

N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

Conditions
ConditionsYield
With sodium hydrogencarbonate; benzene
With sodium hydrogencarbonate
Iodoacetic acid
64-69-7

Iodoacetic acid

2,2'-iminobis[ethanol]
111-42-2

2,2'-iminobis[ethanol]

N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

Conditions
ConditionsYield
With methanol
sodium monochloroacetic acid
3926-62-3

sodium monochloroacetic acid

2,2'-iminobis[ethanol]
111-42-2

2,2'-iminobis[ethanol]

N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

Conditions
ConditionsYield
With water
2,2'-iminobis[ethanol]
111-42-2

2,2'-iminobis[ethanol]

chloroacetic acid
79-11-8

chloroacetic acid

N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

Conditions
ConditionsYield
With ethanol
In ethanol
Nα,Nα-bis(-2-hydroxyethyl)glycine amide

Nα,Nα-bis(-2-hydroxyethyl)glycine amide

A

4-(2-hydroxy-ethyl)-morpholin-2-one
5038-12-0

4-(2-hydroxy-ethyl)-morpholin-2-one

B

N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

Conditions
ConditionsYield
With water at 25℃; Rate constant; Product distribution; Mechanism; pH varied: 4 to 8; hydrolysis of C-terminal amide group of various α-aminoacids having one or two hydroxyethyl groups at N-terminal, via cyclization to a morpholinolactone; reaction monitored by 1H NMR;
4-(2-hydroxy-ethyl)-morpholin-2-one
5038-12-0

4-(2-hydroxy-ethyl)-morpholin-2-one

water
7732-18-5

water

N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

<2-chloroacetoxy-ethyl>-<2-chloro-ethyl>-amine hydrochloride

<2-chloroacetoxy-ethyl>-<2-chloro-ethyl>-amine hydrochloride

N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

Conditions
ConditionsYield
With potassium carbonate
formaldehyd
50-00-0

formaldehyd

potassium cyanide
151-50-8

potassium cyanide

bis-<2-hydroxy-ethyl>-amine hydrochloride

bis-<2-hydroxy-ethyl>-amine hydrochloride

N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

Conditions
ConditionsYield
With water und Hydrolyse des Reaktionsprodukts mit wss.HCl;
bromoacetic acid methyl ester
96-32-2

bromoacetic acid methyl ester

2,2'-iminobis[ethanol]
111-42-2

2,2'-iminobis[ethanol]

N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

Conditions
ConditionsYield
With sodium hydroxide; triethylamine In propan-1-ol; ethanol
N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

copper hydroxide
20427-59-2

copper hydroxide

copper(II) bis(N,N-bis(2-hydroxyethyl)glycinate)
77180-36-0, 921625-45-8, 13978-30-8

copper(II) bis(N,N-bis(2-hydroxyethyl)glycinate)

Conditions
ConditionsYield
In neat (no solvent, solid phase) grinding at room temp. in air for 30 min; crystn. from EtOH:H2O (1:1) for 2 d at room temp., elem. anal.;99%
N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

octadecyldimethyl[3-(trimethoxysilyl)propyl]ammonium chloride
27668-52-6

octadecyldimethyl[3-(trimethoxysilyl)propyl]ammonium chloride

disodium 7-(2-((carboxymethyl)(2-hydroxyethyl)amino)ethoxy)-7-(3-(heptadecyldimethylammonio)propyl)-3,11-bis(2-hydroxyethyl)-6,8-dioxa-3,11-diaza-7-silatridecanedioate chloride

disodium 7-(2-((carboxymethyl)(2-hydroxyethyl)amino)ethoxy)-7-(3-(heptadecyldimethylammonio)propyl)-3,11-bis(2-hydroxyethyl)-6,8-dioxa-3,11-diaza-7-silatridecanedioate chloride

Conditions
ConditionsYield
Stage #1: N,N-bis-(2-hydroxyethyl)glycine; octadecyldimethyl[3-(trimethoxysilyl)propyl]ammonium chloride In N,N-dimethyl-formamide at 145℃;
Stage #2: With sodium methylate In N,N-dimethyl-formamide
95%
N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

1,2-diamino-benzene
95-54-5

1,2-diamino-benzene

N-(benzimidazol-2-ylmethyl)iminodiethanol
91646-60-5

N-(benzimidazol-2-ylmethyl)iminodiethanol

Conditions
ConditionsYield
With hydrogenchloride for 48h; Heating;93%
With hydrogenchloride; water
N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

1,1,1,3,3,3-hexamethyl-disilazane
999-97-3

1,1,1,3,3,3-hexamethyl-disilazane

Conditions
ConditionsYield
85%
N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

acetic anhydride
108-24-7

acetic anhydride

4-(2-acetoxy-ethyl)-morpholin-2-one
86351-49-7

4-(2-acetoxy-ethyl)-morpholin-2-one

Conditions
ConditionsYield
With triethylamine for 1h; Heating;83%
With pyridine Erwaermen des Reaktionsprodukts in Methanol oder in H2O;
N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

Phenyl-triethoxygerman
42428-34-2

Phenyl-triethoxygerman

1-phenyl-2,8,9-trioxa-5-aza-1-germatricyclo[3.3.3.0(1,5)]undecane-3-one
75713-38-1

1-phenyl-2,8,9-trioxa-5-aza-1-germatricyclo[3.3.3.0(1,5)]undecane-3-one

Conditions
ConditionsYield
In N,N-dimethyl-formamide; benzene byproducts: CH3CH2OH; boiled for 2 h with distillation; cooled; filtered off; washed (benzene and ether); dried (vac.); IR; elem.anal.;72%
N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

Methyl-triaethoxy-germanium
5865-91-8

Methyl-triaethoxy-germanium

1-methyl-2,8,9-trioxa-5-aza-1-germatricyclo[3.3.3.0(1,5)]undecane-3-one
75713-37-0

1-methyl-2,8,9-trioxa-5-aza-1-germatricyclo[3.3.3.0(1,5)]undecane-3-one

Conditions
ConditionsYield
In N,N-dimethyl-formamide; benzene byproducts: CH3CH2OH; boiled for 2 h with distillation; cooled; filtered off; washed (benzene and ether); dried (vac.); IR; elem.anal.;69%
N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

Mn(H2O)6(2+)*2Br(1-)=MnBr2*6H2O

Mn(H2O)6(2+)*2Br(1-)=MnBr2*6H2O

Mn2(OC(O)CH2N(CH2CH2OH)2)2(H2O)2(2+)*2Br(1-)*2H2O=[Mn2(OC(O)CH2N(CH2CH2OH)2)2(H2O)2]Br2*2H2O

Mn2(OC(O)CH2N(CH2CH2OH)2)2(H2O)2(2+)*2Br(1-)*2H2O=[Mn2(OC(O)CH2N(CH2CH2OH)2)2(H2O)2]Br2*2H2O

Conditions
ConditionsYield
With [(CH3)4N]OH In methanol; water boiling (pH .apprx. 8, 10 min); elem. anal.;68.8%
manganese(II) chloride hexahydrate

manganese(II) chloride hexahydrate

N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

([Mn(N,N-bis(2-hydroxyethyl)glycinate)Cl]2*2(H2O))n
194363-15-0

([Mn(N,N-bis(2-hydroxyethyl)glycinate)Cl]2*2(H2O))n

Conditions
ConditionsYield
With Me4NOH In methanol dropwise addn. of Me4NOH to mixt. of Mn-salt and ligand; crystn. on slow evapn. (few d); elem. anal.;68%
N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

Ethyl-triethoxygermanium
5865-92-9

Ethyl-triethoxygermanium

1-ethyl-2,8,9-trioxa-5-aza-1-germatricyclo[3.3.3.0(1,5)]undecane-3-one
87511-09-9

1-ethyl-2,8,9-trioxa-5-aza-1-germatricyclo[3.3.3.0(1,5)]undecane-3-one

Conditions
ConditionsYield
In N,N-dimethyl-formamide; benzene byproducts: CH3CH2OH; boiled for 2 h with distillation; cooled; filtered off; washed (benzene and ether); dried (vac.); IR; elem.anal.;60%
vanadyl(IV) sulphate pentahydrate

vanadyl(IV) sulphate pentahydrate

diethyl ether
60-29-7

diethyl ether

N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

VO(2+)*HOCH2CH2(OCH2CH2)N(CH2COO)(2-)*0.5(CH3CH2)2O=[VO((HOCH2CH2(OCH2CH2)N(CH2COO)))*0.5(CH3CH2)2O]

VO(2+)*HOCH2CH2(OCH2CH2)N(CH2COO)(2-)*0.5(CH3CH2)2O=[VO((HOCH2CH2(OCH2CH2)N(CH2COO)))*0.5(CH3CH2)2O]

Conditions
ConditionsYield
With barium dihydroxide In water byproducts: BaSO4; org. compd. and Ba compd. dissolved in deionised water under N2 then heated and stirred for 30 min, VO compd. added and react. mixt. stirred for30 min; BaSO4 filtered off, filtrate concd. in vac. to oily residue, washed withEt2O, solid filtered, washed with Et2O and dried in vac.; elem. anal.;58%
cadmium(II) chloride dihydrate

cadmium(II) chloride dihydrate

N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

[CdCl(N,N-bis(2-hydroxyethyl)glycine(-1H))]*H2O
60245-55-8, 1269638-47-2

[CdCl(N,N-bis(2-hydroxyethyl)glycine(-1H))]*H2O

Conditions
ConditionsYield
With LiOH*H2O In methanol; water byproducts: LiCl, H2O; soln. of Cd salt in H2O added to stirred soln. of ligand and LiOH*H2O inMeOH; layered with acetone; crystd. for 5 d; filtered; crystals washed with cold MeOH and acetone; dried in air; elem. anal.;55%
methanol
67-56-1

methanol

cadmium(II) chloride dihydrate

cadmium(II) chloride dihydrate

N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

sodium hydroxide
1310-73-2

sodium hydroxide

[CdNaCl2(N,N-bis(2-hydroxyethyl)glycine(-1H))(methanol)]*0.5(methanol)

[CdNaCl2(N,N-bis(2-hydroxyethyl)glycine(-1H))(methanol)]*0.5(methanol)

Conditions
ConditionsYield
In methanol byproducts: H2O; soln. of Cd salt in MeOH added to stirred soln. of ligand and NaOH in MeOH; refluxed for 25 min; concd. slowly by evapn. over 4 d; filtered; crystals washed with cold MeOH and Et2O; dried in air; elem. anal.;53%
[dichlorobis(triphenylphosphane)(η2-N-benzoylhydrazido(3-)-N',O)rhenium(V)]
83149-20-6

[dichlorobis(triphenylphosphane)(η2-N-benzoylhydrazido(3-)-N',O)rhenium(V)]

N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

[chloro(N,N-bis(2-hydroxyethyl)glycinate)(triphenylphosphane)(η1-N-benzoyldiazenido(2-)-N')rhenium(III)]

[chloro(N,N-bis(2-hydroxyethyl)glycinate)(triphenylphosphane)(η1-N-benzoyldiazenido(2-)-N')rhenium(III)]

Conditions
ConditionsYield
In methanol N2, an excess of amine, refluxed for 8 h; concd. (vac.), diethyl ether added, left for 2 d at room temp., crysts. washed (methanol), dried (vac.); elem. anal.;48%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

praseodymium(III) acetate tetrahydrate

praseodymium(III) acetate tetrahydrate

N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

water
7732-18-5

water

1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

[Pr(O2CCH3)(bicine)(1,10-phenanthroline)(H2O)](ClO4)*1,10-phenanthroline*3H2O

[Pr(O2CCH3)(bicine)(1,10-phenanthroline)(H2O)](ClO4)*1,10-phenanthroline*3H2O

Conditions
ConditionsYield
In ethanol; water byproducts: CH3COOH, CH3COONa; a soln. of bicine in water was added to a soln. of Pr-compound in H2O, stirred, an ethanolic soln. of NaClO4 and phenanthroline were added, allowed to stand for 20 days at room temp.; filtered, washed with cold ethanol and dried in air; elem. anal.;45%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

water
7732-18-5

water

erbium(III) acetate tetrahydrate
15280-57-6

erbium(III) acetate tetrahydrate

1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

[Er(O2CCH3)(bicine)(1,10-phenanthroline)(H2O)](ClO4)*1,10-phenanthroline*3H2O

[Er(O2CCH3)(bicine)(1,10-phenanthroline)(H2O)](ClO4)*1,10-phenanthroline*3H2O

Conditions
ConditionsYield
In ethanol; water byproducts: CH3COOH, CH3COONa; a soln. of bicine in water was added to a soln. of Er-compound in H2O, stirred, an ethanolic soln. of NaClO4 and phenanthroline were added, allowed to stand for 20 days at 5°C; crystals were washed with cold ethanol, diethyl ether and dried in air; elem. anal.;40%
methanol
67-56-1

methanol

[Fe(III)3(μ3-O)(O2CC6H5)6(H2O)3](O2CC6H5)

[Fe(III)3(μ3-O)(O2CC6H5)6(H2O)3](O2CC6H5)

N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

[Fe6(bicine-3H)6]*4H2O*4MeOH

[Fe6(bicine-3H)6]*4H2O*4MeOH

Conditions
ConditionsYield
In acetonitrile byproducts: PhCO2H, H2O; to a soln. of Fe3-contg. compd. (0.25 mmol) in MeCN was added with stirring a soln. of a ligand (0.50 mmol) in MeCN; the soln. was stirred overnight at ambient temp.; the ppt. was collected by filtration, washed with MeCN and dissolved in MeOH-CH2Cl2 (1:1); the soln. was layered with Et2O and left at ambient temp.; after 1 wk the crystals were collected by filtration, washed with CH2Cl2 and dried in vac.; elem. anal.;38%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

water
7732-18-5

water

1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

[Nd(O2CCH3)(bicine)(1,10-phenanthroline)(H2O)](ClO4)*1,10-phenanthroline*3H2O

[Nd(O2CCH3)(bicine)(1,10-phenanthroline)(H2O)](ClO4)*1,10-phenanthroline*3H2O

Conditions
ConditionsYield
In ethanol; water byproducts: CH3COOH, CH3COONa; a soln. of bicine in water was added to a soln. of Nd-compound in H2O, stirred, an ethanolic soln. of NaClO4 and phenanthroline were added, allowed to stand for 20 days at room temp.; filtered, washed with cold ethanol and dried in air; elem. anal.;30%
sodium perchlorate monohydrate
7791-07-3

sodium perchlorate monohydrate

N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

water
7732-18-5

water

1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

[Gd(O2CCH3)(bicine)(1,10-phenanthroline)(H2O)](ClO4)*1,10-phenanthroline*3H2O

[Gd(O2CCH3)(bicine)(1,10-phenanthroline)(H2O)](ClO4)*1,10-phenanthroline*3H2O

Conditions
ConditionsYield
In ethanol; water byproducts: CH3COOH, CH3COONa; a soln. of bicine in water was added to a soln. of Gd-compound in H2O, stirred, an ethanolic soln. of NaClO4 and phenanthroline were added, allowed to stand for 20 days at room temp.; filtered, washed with cold ethanol and dried in air; elem. anal.;25%
cobalt(II) chloride hexahydrate

cobalt(II) chloride hexahydrate

N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

[CoII(N,N-bis(2-hydroxyethyl)glycinato)Cl]

[CoII(N,N-bis(2-hydroxyethyl)glycinato)Cl]

Conditions
ConditionsYield
With triethylamine In ethanol at 140℃; under 15514.9 Torr; for 0.25h; Sealed tube; Microwave irradiation;18%
cobalt(II) chloride hexahydrate

cobalt(II) chloride hexahydrate

N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

[CoII9(N,N-bis(2-hydroxoethyl)glycinato)4(N,N-bis(2-hydroxoethyl)glycinato)2Cl4]

[CoII9(N,N-bis(2-hydroxoethyl)glycinato)4(N,N-bis(2-hydroxoethyl)glycinato)2Cl4]

Conditions
ConditionsYield
With triethylamine In ethanol at 140℃; under 15514.9 Torr; for 0.25h; Sealed tube; Microwave irradiation;17%
cobalt(II) chloride hexahydrate

cobalt(II) chloride hexahydrate

N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

water
7732-18-5

water

[CoII9(N,N-bis(2-hydroxyethyl)glycinato)4(N,N-bis(2-hydroxyethyl)glycinato)2Cl4]*12H2O

[CoII9(N,N-bis(2-hydroxyethyl)glycinato)4(N,N-bis(2-hydroxyethyl)glycinato)2Cl4]*12H2O

Conditions
ConditionsYield
With triethylamine In ethanol at 140℃; under 15514.9 Torr; for 0.25h; Sealed tube; Microwave irradiation;17%
[Fe3O(pivalate)6(H2O)3](pivalate)*2Me3CCO2H

[Fe3O(pivalate)6(H2O)3](pivalate)*2Me3CCO2H

N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

diethylamine
109-89-7

diethylamine

acetonitrile
75-05-8

acetonitrile

[Et2NH2]2[Fe6O2(OH)2(N,N-bis(2hydroxyethyl)glycine(3-))2(pivalate)8]*1.5MeCN*4H2O

[Et2NH2]2[Fe6O2(OH)2(N,N-bis(2hydroxyethyl)glycine(3-))2(pivalate)8]*1.5MeCN*4H2O

Conditions
ConditionsYield
In acetonitrile N,N-bis(2-hydroxyethyl)glycine added to MeCN soln. of Fe pivalate deriv.followed by Et2NH (1:1:1); stirred at ambient temp. for 24 h; filtered; cryst. in a sealed vial after 2 wks; elem. anal.;16%
[Fe3O(pivalate)6(H2O)3](pivalate)*2Me3CCO2H

[Fe3O(pivalate)6(H2O)3](pivalate)*2Me3CCO2H

N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

acetonitrile
75-05-8

acetonitrile

[Fe12O4(N,N-bis(2hydroxyethyl)glycine(3-))4(N,N-bis(2hydroxyethyl)glycine(2-))4(pivalate)8]*2MeCN*4H2O

[Fe12O4(N,N-bis(2hydroxyethyl)glycine(3-))4(N,N-bis(2hydroxyethyl)glycine(2-))4(pivalate)8]*2MeCN*4H2O

Conditions
ConditionsYield
With NaOMe In acetonitrile N,N-bis(2-hydroxyethyl)glycine added to MeCN soln. of Fe pivalate deriv.followed by NaOMe (1:1:1); stirred at ambient temp. for 24 h; filtered; cryst. in a sealed vial after 2 wks; elem. anal.;12%
4,5-Dichloro-1,2-phenylenediamine
5348-42-5

4,5-Dichloro-1,2-phenylenediamine

N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

2,2'-(5,6-dichloro-1H-benzoimidazol-2-ylmethylazanediyl)-bis-ethanol
6478-89-3

2,2'-(5,6-dichloro-1H-benzoimidazol-2-ylmethylazanediyl)-bis-ethanol

Conditions
ConditionsYield
With hydrogenchloride; water
N,N-bis-(2-hydroxyethyl)glycine
150-25-4

N,N-bis-(2-hydroxyethyl)glycine

4-(2-hydroxy-ethyl)-morpholin-2-one
5038-12-0

4-(2-hydroxy-ethyl)-morpholin-2-one

Conditions
ConditionsYield
durch trockne Destillation;
With hydrogenchloride
With hydrogenchloride
In solid at 195℃; for 0.166667h;
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