CAS No.1730-04-7,1,8-Diiodonaphthalene Suppliers,MSDS download

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Naphthalene, 1,8-diiodo-

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1,8-Diiodonaphthalene

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Synthetic route

: 518-05-8
Naphthalene-1,8-dicarboxylic acid

: 1730-04-7
1,8-diiodonaphthalene

Conditions

Conditions	Yield
With [bis(acetoxy)iodo]benzene; iodine In tetrachloromethane for 2h; Heating; Irradiation;	80%

: 479-27-6
naphthalene-1,8-diamine

: 1730-04-7
1,8-diiodonaphthalene

Conditions

Conditions	Yield
With sulfuric acid; 7,14-bis(trimethylsilyl)acenaphtho[1,2-k]fluoranthene; sodium nitrite In water at -20 - 80℃; for 0.5h; Inert atmosphere;	70%
Stage #1: naphthalene-1,8-diamine With sulfuric acid; sodium nitrite In water at -20 - -15℃; Stage #2: With potassium iodide In water	63%
Stage #1: naphthalene-1,8-diamine With sulfuric acid; sodium nitrite In water at -20 - -15℃; Stage #2: With potassium iodide In water at -20 - 80℃;	61%

: 86-55-5
1-naphthalenecarboxylic acid

A: 1730-04-7
1,8-diiodonaphthalene

B: 90-14-2
1-Iodonaphthalene

Conditions

Conditions	Yield
With potassium phosphate; iodine In acetonitrile at 140℃; for 16h; Glovebox; Inert atmosphere; chemoselective reaction;	A 7% B 57%

: 8-iodo-[1]naphthylamine; hydrochloride

: 1730-04-7
1,8-diiodonaphthalene

Conditions

Conditions	Yield
(i) NaNO2, aq. HCl, (ii) KI; Multistep reaction;
With hydrogenchloride; potassium iodide; sodium nitrite 1.) H2O, -1 deg C, 2.) H2O, heating, 2 h; Multistep reaction;

diazotized 8-iodo-naphthylamine-(1): diazotized 8-iodo-naphthylamine-(1)

: 1730-04-7
1,8-diiodonaphthalene

Conditions

Conditions	Yield
With hydrogenchloride Behandeln der Diazoniumsalzloesung mit KI;

: 1730-04-7
1,8-diiodonaphthalene

: 115-19-5
2-methyl-but-3-yn-2-ol

: 1,1'-(naphthalene-1,8-diyl)bis(2-methylbut-3-yn-2-ol)

Conditions

Conditions	Yield
With copper(l) iodide; diisopropylamine; tetrakis(triphenylphosphine) palladium(0) at 50℃; for 16h; Sonogashira reaction;	99%
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine at 80℃; for 20h; Sonogashira coupling; Inert atmosphere; Sealed flask;	94%

: 1730-04-7
1,8-diiodonaphthalene

: 118486-94-5
2-(tributylstannyl)furan

: 1248481-21-1
1,8-di(furan-2-yl)naphthalene

Conditions

Conditions	Yield
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); cesium fluoride In N,N-dimethyl-formamide at 45℃; for 14h; Inert atmosphere;	99%

: 1730-04-7
1,8-diiodonaphthalene

: 208399-66-0
4-methoxy-2-methylphenyl boronic acid

: 1,8-bis(2'-methyl-4'-methoxyphenyl)naphthalene

Conditions

Conditions	Yield
With potassium phosphate; tetrakis(triphenylphosphine) palladium(0) In toluene at 100℃; for 18h; Suzuki coupling; Inert atmosphere;	99%
With potassium phosphate; tetrakis(triphenylphosphine) palladium(0) In toluene at 100℃; for 18h; Product distribution / selectivity;	99%

: indium(III) chloride

: 1730-04-7
1,8-diiodonaphthalene

: 81698-99-9
1,3,5-trimethyl 2-(α-furyl)benzene

: 1,8-bis(5-mesitylfuran-2-yl)naphthalene

Conditions

Conditions	Yield
Stage #1: 1,3,5-trimethyl 2-(α-furyl)benzene With n-butyllithium In tetrahydrofuran; hexane at 0℃; for 0.5h; Inert atmosphere; Stage #2: indium(III) chloride In tetrahydrofuran at -78 - 25℃; for 0.5h; Stage #3: 1,8-diiodonaphthalene With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride In tetrahydrofuran; methanol for 18h; Reflux;	99%

...Expand

: 1730-04-7
1,8-diiodonaphthalene

: 116487-12-8
(4-Ethynyl-furan-3-yl)-trimethyl-silane

: 216309-10-3
1,8-bis-[(4-trimethylsilyl)-3-furanylethynyl]naphthalene

Conditions

Conditions	Yield
With triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide at 25℃; for 48h;	97%

: 14275-42-4
di-n-butylchlorogermane

: 1730-04-7
1,8-diiodonaphthalene

: 1578224-45-9
1,8-bis(di-n-butylgermyl)naphthalene

Conditions

Conditions	Yield
With n-butyllithium In diethyl ether; hexane at -60℃; for 1.5h; Inert atmosphere;	96%

: 1730-04-7
1,8-diiodonaphthalene

: 1066-54-2
trimethylsilylacetylene

: 27503-44-2
1,8-bis(2-trimethylsilylethynyl)naphthalene

Conditions

Conditions	Yield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine at 20℃; for 12h; Sonogashira Cross-Coupling; Inert atmosphere;	95%
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine at 100℃; for 1h; Substitution; Sonogashira coupling;	91%
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine at 110℃; for 1h; Schlenk technique; Inert atmosphere;	80%
Stage #1: trimethylsilylacetylene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h; Stage #2: With zinc(II) chloride In tetrahydrofuran; hexane at 20℃; for 1h; Stage #3: 1,8-diiodonaphthalene With tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran; hexane at 20 - 50℃; Negishi coupling; Inert atmosphere;	63%
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diethylamine	30%

: 1730-04-7
1,8-diiodonaphthalene

: 17356-19-3
1-ethynylcyclopentanol

: 1321605-56-4
1,1'-(naphthalene-1,8-diylbis(ethyne-2,1-diyl))dicyclopentanol

Conditions

Conditions	Yield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine at 80℃; for 20h; Sonogashira coupling; Inert atmosphere; Sealed flask;	95%

: 5419-55-6
Triisopropyl borate

: 1730-04-7
1,8-diiodonaphthalene

: 1400770-57-1
diisopropyl 8-iodonaphthalen-1-ylboronate

Conditions

Conditions	Yield
Stage #1: 1,8-diiodonaphthalene With isopropylmagnesium chloride In tetrahydrofuran; diethyl ether at -78℃; for 2h; Inert atmosphere; Stage #2: Triisopropyl borate In tetrahydrofuran; diethyl ether at -78 - 25℃; Inert atmosphere; regioselective reaction;	95%

: 110-00-9
furan

: indium(III) chloride

: 1730-04-7
1,8-diiodonaphthalene

: 1248481-21-1
1,8-di(furan-2-yl)naphthalene

Conditions

Conditions	Yield
Stage #1: furan With n-butyllithium In tetrahydrofuran; hexane at 0℃; for 0.5h; Inert atmosphere; Stage #2: indium(III) chloride In tetrahydrofuran at -78 - 25℃; for 0.5h; Stage #3: 1,8-diiodonaphthalene With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride In tetrahydrofuran; methanol for 18h; Reagent/catalyst; Concentration; Negishi Coupling; Reflux;	95%

...Expand

: 498-66-8
norborn-2-ene

: 1730-04-7
1,8-diiodonaphthalene

: 57704-85-5, 75196-53-1, 119945-30-1
(6bα,7β,10β,10aα)-6b,7,8,9,10,10a-hexahydro-7,10-methanofluoranthene

Conditions

Conditions	Yield
With tetrabutylammomium bromide; potassium carbonate; palladium diacetate In N,N-dimethyl-formamide at 100℃; for 72h;	94%

: 1730-04-7
1,8-diiodonaphthalene

: 108-98-5
thiophenol

: 1,8-bis-(phenylsulfanyl)naphthalene

Conditions

Conditions	Yield
With 2,4,6-trimethyl-pyridine; copper(II) oxide for 10h; Reflux; Inert atmosphere;	94%
With copper(I) oxide In pyridine for 2h; Heating;	55%

: 1730-04-7
1,8-diiodonaphthalene

: 115-19-5
2-methyl-but-3-yn-2-ol

A: 205124-36-3
4-(8-iodonaphthalene-1-yl)-2-methylbut-3-yn-2-ol

B: 1,1'-(naphthalene-1,8-diyl)bis(2-methylbut-3-yn-2-ol)

Conditions

Conditions	Yield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine at 20 - 80℃; Sonogashira coupling reaction; Inert atmosphere; Sealed flask;	A 5% B 94%

...Expand

: 1730-04-7
1,8-diiodonaphthalene

: 768-60-5
4-methoxyphenylacetylen

: 1,8-bis<<(p-hydroxymethyl)phenyl>ethynyl>naphthalene

Conditions

Conditions	Yield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine at 80℃; for 20h; Sonogashira coupling; Inert atmosphere; Sealed flask;	93%
With copper(l) iodide; bis(triphenylphosphine)palladium(II)-chloride; triethylamine; triphenylphosphine at 20 - 50℃; for 10h; Sonogashira coupling; Inert atmosphere;	93%
Stage #1: 1,8-diiodonaphthalene With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine; triphenylphosphine at 20℃; for 0.166667h; Sealed tube; Stage #2: 4-methoxyphenylacetylen at 20℃; for 16h; Sealed tube;	42%

: 1730-04-7
1,8-diiodonaphthalene

: 77-75-8
meparfynol

: 1321605-58-6
1,1'-(naphthalene-1,8-diyl)bis(3-methylpent-1-yn-3-ol)

Conditions

Conditions	Yield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine at 80℃; for 20h; Sonogashira coupling; Inert atmosphere; Sealed flask;	93%

: 1730-04-7
1,8-diiodonaphthalene

: 5720-06-9
2-Methoxyphenylboronic acid

: 1257841-02-3
1,8-bis(2-methoxyphenyl)naphthalene

Conditions

Conditions	Yield
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate In water; N,N-dimethyl-formamide at 125℃; for 2h; Suzuki-Miyaura Coupling; Inert atmosphere;	93%

: 1730-04-7
1,8-diiodonaphthalene

: 115-19-5
2-methyl-but-3-yn-2-ol

: 205124-36-3
4-(8-iodonaphthalene-1-yl)-2-methylbut-3-yn-2-ol

Conditions

Conditions	Yield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine Sonogashira coupling reaction;	92%
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine at 80℃; for 20h; Sonogashira coupling; Inert atmosphere; Sealed flask;	92%
With triethylamine; copper(l) iodide; Pd2(dba)4; triphenylphosphine In toluene at 23℃; for 12h; Sonogashira reaction;	83%

: 13331-23-2
fur-2-ylboronic acid

: 1730-04-7
1,8-diiodonaphthalene

: 1248481-21-1
1,8-di(furan-2-yl)naphthalene

Conditions

Conditions	Yield
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); cesium fluoride Inert atmosphere;	92%

: 6285-06-9
3-ethyl-1-pentyn-3-ol

: 1730-04-7
1,8-diiodonaphthalene

: 1321605-57-5
1,1'-(naphthalene-1,8-diyl)bis(3-ethylpent-1-yn-3-ol)

Conditions

Conditions	Yield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine at 80℃; for 20h; Sonogashira coupling; Inert atmosphere; Sealed flask;	92%

: 1730-04-7
1,8-diiodonaphthalene

: 766-97-2
4-n-methylphenylacetylene

: 17873-54-0
1,8-bis((p-tolyl)ethynyl)naphthalene

Conditions

Conditions	Yield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine at 80℃; for 20h; Sonogashira coupling; Inert atmosphere; Sealed flask;	92%
With copper(l) iodide; bis(triphenylphosphine)palladium(II)-chloride; triethylamine; triphenylphosphine at 20 - 50℃; for 10h; Sonogashira coupling; Inert atmosphere;	92%

: 1730-04-7
1,8-diiodonaphthalene

: 766-46-1
2-bromo-1-ethynylbenzene

: 867194-03-4
1,8-bis[(2-bromophenyl)ethynyl]naphthalene

Conditions

Conditions	Yield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triphenylphosphine In triethylamine at 50℃; for 12h; Sonogashira coupling;	91%
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine at 40 - 50℃; Inert atmosphere; Schlenk technique; Glovebox;

: 1730-04-7
1,8-diiodonaphthalene

: 536-74-3
phenylacetylene

: 17694-87-0
1,8-bis-(phenylethynyl)naphthalene

Conditions

Conditions	Yield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine at 80℃; for 20h; Sonogashira coupling; Inert atmosphere; Sealed flask;	90%
With copper(l) iodide; bis(triphenylphosphine)palladium(II)-chloride; triethylamine; triphenylphosphine at 20 - 50℃; for 10h; Sonogashira coupling; Inert atmosphere;	90%
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triphenylphosphine In triethylamine at 40℃; for 11h; Sonogashira coupling;	89%
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine In tetrahydrofuran at 20℃; for 12h; Sonogashira coupling; Inert atmosphere;	86%
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine at 20℃; Sonogashira Cross-Coupling;	86%

: 1730-04-7
1,8-diiodonaphthalene

: 101251-09-6
(4-acetylaminophenyl)boronic acid

: 1246218-84-7
1,8-bis(4'-acetamidophenyl)naphthalene

Conditions

Conditions	Yield
With potassium phosphate; tetrakis(triphenylphosphine) palladium(0) In ethanol; water; toluene at 95℃; for 20h; Suzuki coupling; Inert atmosphere;	90%

: 4339-05-3
3-methylhex-1-yn-3-ol

: 1730-04-7
1,8-diiodonaphthalene

: 1321605-59-7
1,1'-(naphthalene-1,8-diyl)bis(3-methylhex-1-yn-3-ol)

Conditions

Conditions	Yield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine at 80℃; for 20h; Sonogashira coupling; Inert atmosphere; Sealed flask;	90%

: 1730-04-7
1,8-diiodonaphthalene

: 78-27-3
1-Ethynyl-1-cyclohexanol

: 1321605-55-3
1,1'-(naphthalene-1,8-diylbis(ethyne-2,1-diyl))dicyclohexanol

Conditions

Conditions	Yield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine at 80℃; for 20h; Sonogashira coupling; Inert atmosphere; Sealed flask;	90%

: 1730-04-7
1,8-diiodonaphthalene

: 4044-58-0
1-bromo-8-iodo-naphthalene

Conditions

Conditions	Yield
Stage #1: 1,8-diiodonaphthalene With n-butyllithium In diethyl ether; hexane at -40℃; for 1h; Inert atmosphere; Stage #2: With 1,2-dibromo-1,1,2,2-tetrachloroethane In diethyl ether at -40 - 20℃; Inert atmosphere;	90%

: 1730-04-7
1,8-diiodonaphthalene

: 34837-55-3
Phenylselenyl bromide

: 1111098-36-2
1,8-bis(phenylselanyl)naphthalene

Conditions

Conditions	Yield
Stage #1: 1,8-diiodonaphthalene With n-butyllithium In tetrahydrofuran at -78℃; for 0.333333h; Inert atmosphere; Stage #2: Phenylselenyl bromide In tetrahydrofuran at -78 - 20℃;	89%

: 1730-04-7
1,8-diiodonaphthalene

1,3-dichloro-2-ethynyl-benzene: 1,3-dichloro-2-ethynyl-benzene

: 1255533-04-0
1-(2,6-dichlorophenylethynyl)-8-iodonaphthalene

Conditions

Conditions	Yield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine at 20 - 50℃; Sonogashira coupling; Inert atmosphere;	88%

: 110-91-8
morpholine

: 1730-04-7
1,8-diiodonaphthalene

: 201230-82-2
carbon monoxide

: 1006863-06-4
1,8-bis[N,N-(3'-oxapenta-1',5'-diyl)carboxamido]-naphthalene

Conditions

Conditions	Yield
With triethylamine; triphenylphosphine; palladium diacetate In N,N-dimethyl-formamide at 50℃; under 750.075 Torr; for 66h;	87%

...Expand

: 1730-04-7
1,8-diiodonaphthalene

: C10H13BrSe

: 1111098-40-8
1,8-bis[(p-tert-butylphenyl)selanyl]naphthalene

Conditions

Conditions	Yield
Stage #1: 1,8-diiodonaphthalene With n-butyllithium In tetrahydrofuran at -78℃; for 0.333333h; Inert atmosphere; Stage #2: C10H13BrSe In tetrahydrofuran at -78 - 20℃;	87%

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