As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for the fine c
Cas:217-59-4
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryTriphenylene Basic information Product Name: Triphenylene Synonyms: BENZO(L)PHENANTHRENE;ISOCHRYSENE;9,10-BENZOPHENANTHRENE;1,2:3,4-DIBENZNAPHTHALENE;TRIPHENYLENE;9
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Product Description Product website: http://www.finerchem.com/pro01en/id/1480.html Product Name Triphenylene CAS No.
Triphenylene Basic information Product Name: Triphenylene Synonyms: BENZO(L)PHENANTHRENE;ISOCHRYSENE;9,10-BENZOPHENANTHRENE;1,2:3,4-DIBENZNAPHTHALENE;TRIPHENYLENE;9
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
Cas:217-59-4
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryCAS 217-59-4 Name Triphenylene Appearance White powder Application Organic Intermediate Appearance: White powder Storage:Store in cool and dry
Cas:217-59-4
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Minimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,MoneyGram Package 10g,20g,50g,100g,500g,1KGS,
Triphenylene CAS: 217-59-4 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
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Cas:217-59-4
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
advantage: 1. The best price, satisfactory quality; 2. customers have the right to choose the delivery of parcels (EMS, DHL, FedEx, UPS); 3. customers have the right to choose from the recent effective packaging methods of their products packaging
Cas:217-59-4
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:217-59-4
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:217-59-4
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inquiryGMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
Triphenylene Basic information Product Name: Triphenylene Synonyms: BENZO(L)PHENANTHRENE;ISOCHRYSENE;9,10-BENZOPHENANTHRENE;1,2:3,4-DIBENZNAPHTHALENE;TRIPHENYLENE;9,10-Benzphenanthrene;benzo(1)phenanthrene;Triphenylene,98% CAS: 217-59-4 MF:
factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:217-59-4
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inquiryHangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
Cas:217-59-4
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:217-59-4
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:217-59-4
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inquiryConditions | Yield |
---|---|
With {Co(II)(DBF2)2(H2O)2} In acetonitrile at 20℃; for 18h; Catalytic behavior; Time; Sealed tube; UV-irradiation; Inert atmosphere; | 100% |
With trifluorormethanesulfonic acid; 5% Pd/Al2O3; oxygen In dichloromethane at 20℃; for 1.4h; | 96% |
With iodine In benzene for 168h; UV-irradiation; | 63.9% |
2-(2-bromophenyl)biphenyl
triphenylene
Conditions | Yield |
---|---|
With bis(benzonitrile)palladium(II) chloride; caesium carbonate; tris<3,5-bis(trifluoromethyl)phenyl>phosphane In toluene at 110℃; for 24h; | 100% |
Conditions | Yield |
---|---|
With aluminum oxide at 250℃; for 0.166667h; Inert atmosphere; | 99.5% |
With dimethyldimesitylsilane In chlorobenzene at 110℃; for 8h; Friedel Crafts reaction; Inert atmosphere; | 97% |
Conditions | Yield |
---|---|
With palladium 10% on activated carbon at 300℃; for 10h; Inert atmosphere; | 99% |
palladium on activated charcoal at 310℃; for 25h; | 82% |
5% Pd(II)/C(eggshell) In Exxsol D110 at 225℃; for 40h; Product distribution / selectivity; Industry scale; | 70% |
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; potassium carbonate; p-benzoquinone In dimethyl sulfoxide at 140℃; for 4h; Schlenk technique; Inert atmosphere; | 99% |
triphenylene
Conditions | Yield |
---|---|
Stage #1: 1-(biphenyl-2-yl)cyclopent-3-ene-1-carbaldehyde With trifluorormethanesulfonic acid In dichloromethane at 0℃; for 3h; Stage #2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone In toluene for 3h; Reflux; | 97% |
[1,1':2',1"-terphenyl]-2-yl trifluoromethanesulfonate
triphenylene
Conditions | Yield |
---|---|
With potassium carbonate; palladium dichloride; tris[tert-butyl]phosphonium tetrafluoroborate; Trimethylacetic acid at 140℃; for 20h; Schlenk technique; Inert atmosphere; | 96% |
2-chloro-1,1':2',1''-terphenyl
triphenylene
Conditions | Yield |
---|---|
With sodium carbonate In water; acetone for 48h; UV-irradiation; Inert atmosphere; Sealed tube; regioselective reaction; | 95% |
Conditions | Yield |
---|---|
With n-butyllithium In hexane at -78 - 25℃; | 93% |
Conditions | Yield |
---|---|
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate In 1,2-dimethoxyethane at 135℃; for 24h; Catalytic behavior; Reagent/catalyst; Schlenk technique; Inert atmosphere; | A 92% B 10% |
Conditions | Yield |
---|---|
Stage #1: 2-bromo-1-chlorobenzene With tert.-butyl lithium; manganese(ll) chloride In tetrahydrofuran; pentane at -78℃; for 0.333333h; Inert atmosphere; Schlenk technique; Stage #2: In tetrahydrofuran; pentane at 25℃; for 1h; Inert atmosphere; Schlenk technique; | 91% |
With n-butyllithium; diethyl ether at -60℃; anschliessendes Erwaermen; |
2-(trimethylsilyl)phenyl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate
triphenylene
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); cesium fluoride In acetonitrile at 55℃; for 16h; Microwave irradiation; | 90% |
A
triphenylene
Conditions | Yield |
---|---|
With C18H19Cl2N2PPd; sodium acetate In N,N-dimethyl-formamide at 160℃; for 0.333333h; Inert atmosphere; Schlenk technique; | A 8% B 90% |
2-(trimethylsilyl)phenyl trifluoromethanesulfonate
triphenylene
Conditions | Yield |
---|---|
With (triphenylphosphine)gold(I) chloride; cesium fluoride In acetonitrile at 60℃; for 6h; Catalytic behavior; Reagent/catalyst; Solvent; Temperature; Inert atmosphere; | 88% |
With sodium amalgam; tetrakis(triphenylphosphine) palladium(0); 18-crown-6 ether; cesium fluoride In tetrahydrofuran at 20℃; for 16h; Catalytic behavior; Inert atmosphere; | 87% |
With C23H20Br2N4O4Pd; cesium fluoride In acetonitrile at 60℃; for 2h; Reagent/catalyst; Temperature; Inert atmosphere; | 85% |
Conditions | Yield |
---|---|
With bis(tri-t-butylphosphine)palladium(0) In tetrahydrofuran at 60℃; for 12h; | 87% |
2-(trimethylsilyl)phenyl trifluoromethanesulfonate
dimethyl acetylenedicarboxylate
A
triphenylene
B
dimethyl 9,10-phenanthrenedicarboxylic acid
C
tetramethyl naphthalene-1,2,3,4-tetracarboxylate
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); cesium fluoride In acetonitrile Ambient temperature; | A 2% B 84% C 7% |
With cesium fluoride; tetrakis(triphenylphosphine) palladium(0) In acetonitrile at 20℃; for 13h; Product distribution; Further Variations:; Catalysts; cocyclization; | A 2% B 84% C 7% |
With cesium fluoride; tetrakis(triphenylphosphine) palladium(0) In acetonitrile at 20℃; for 12h; cocyclization; | A 2% B 84% C 7% |
2-(trimethylsilyl)phenyl trifluoromethanesulfonate
phenylacetylene
triphenylene
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0) In acetonitrile at 20℃; for 12h; Inert atmosphere; | 83% |
2,5-dimethylfuran
1-(tri-n-butylstannyl)-2-fluorobenzene
A
triphenylene
B
1,4-dihydro-1,4-dimethyl-1,4-epoxynaphthalene
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran; hexane at -78 - 25℃; | A 83% B 17% |
With n-butyllithium In hexane at -78 - 25℃; | A 28% B 72% |
Conditions | Yield |
---|---|
With (bis(tricyclohexyl)phosphine)palladium(II) dichloride; P(p-CH3OC6H4)3; caesium carbonate In 1,4-dioxane for 24h; Suzuki-Miyaura Coupling; Inert atmosphere; Reflux; regioselective reaction; | 83% |
1,2-bis(4,4,5,5-tetramethyl-[1,3,2]dioxabororan-2-yl)benzene
2,2'-dibromobiphenyl
triphenylene
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water at 60℃; for 48h; Inert atmosphere; | 82% |
Conditions | Yield |
---|---|
With 2,3-dicyano-5,6-dichloro-p-benzoquinone In toluene at 110℃; for 4h; Inert atmosphere; | 81% |
With 2,3-dicyano-5,6-dichloro-p-benzoquinone Inert atmosphere; | 8% |
With selenium at 320℃; |
Conditions | Yield |
---|---|
With bis(benzonitrile)palladium(II) dichloride; caesium carbonate; tris<3,5-bis(trifluoromethyl)phenyl>phosphane In toluene at 110℃; for 24h; Reagent/catalyst; Inert atmosphere; Schlenk technique; | 81% |
With bis(benzonitrile)palladium(II) chloride; caesium carbonate; tris<3,5-bis(trifluoromethyl)phenyl>phosphane In toluene at 110℃; for 24h; Catalytic behavior; Mechanism; Time; Reagent/catalyst; Solvent; Temperature; Inert atmosphere; Schlenk technique; | 81% |
[1,1'-biphenyl]-2,2'-iodonium trifluoromethanesulfonate
benzoic acid
triphenylene
Conditions | Yield |
---|---|
With potassium phosphate; palladium diacetate In N,N-dimethyl-formamide at 145℃; for 16h; Catalytic behavior; Reagent/catalyst; Solvent; Temperature; Concentration; | 81% |
With palladium diacetate; potassium carbonate In N,N-dimethyl-formamide at 145℃; for 15h; | 30% |
With palladium diacetate; potassium carbonate In 1-methyl-pyrrolidin-2-one at 110℃; for 17h; | 15% |
With silver hexafluoroantimonate; palladium(II) trifluoroacetate; trifluoroacetic acid at 130℃; for 24h; Molecular sieve; Sealed tube; | 6% |
[1,1'-biphenyl]-2,2'-iodonium trifluoromethanesulfonate
ortho-chlorobenzoic acid
triphenylene
Conditions | Yield |
---|---|
With palladium diacetate; potassium carbonate In 1-methyl-pyrrolidin-2-one at 110℃; for 17h; Catalytic behavior; Reagent/catalyst; Solvent; Temperature; | 81% |
With palladium diacetate; potassium carbonate In 1-methyl-pyrrolidin-2-one at 110℃; for 17h; | 80% |
2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl trifluoromethanesulfonate
triphenylene
Conditions | Yield |
---|---|
With potassium tert-butylate; bis[2-(diphenylphosphino)phenyl] ether; bis(dibenzylideneacetone)-palladium(0) In toluene at 100℃; Schlenk technique; Inert atmosphere; | 80% |
2-(trimethylsilyl)phenyl trifluoromethanesulfonate
triphenylene
Conditions | Yield |
---|---|
With sodium amalgam; tetrakis(triphenylphosphine) palladium(0); 18-crown-6 ether; cesium fluoride In tetrahydrofuran at 20℃; for 16h; Catalytic behavior; Inert atmosphere; | 80% |
naphthalen-1-yl-2-iodobenzoate
A
triphenylene
B
6H-benzo[d]naphtho[1,2-b]pyran-6-one
Conditions | Yield |
---|---|
With C18H19Cl2N2PPd; sodium acetate In N,N-dimethyl-formamide at 160℃; for 0.333333h; Inert atmosphere; Schlenk technique; | A 7% B 79% |
2-(trimethylsilyl)phenyl trifluoromethanesulfonate
A
triphenylene
Conditions | Yield |
---|---|
With sodium amalgam; tetrakis(triphenylphosphine) palladium(0); 18-crown-6 ether; cesium fluoride In tetrahydrofuran at 20℃; for 16h; Catalytic behavior; Reagent/catalyst; Schlenk technique; Inert atmosphere; | A 67% B 79% |
Conditions | Yield |
---|---|
With hydrazine hydrate; palladium on activated charcoal In ethanol for 0.5h; Heating; | A 4% B 78% |
2-(2-bromophenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane
triphenylene
Conditions | Yield |
---|---|
With potassium tert-butylate; bis[2-(diphenylphosphino)phenyl] ether; bis(dibenzylideneacetone)-palladium(0) In toluene at 100℃; for 16h; Catalytic behavior; Reagent/catalyst; Solvent; Temperature; Time; Schlenk technique; Inert atmosphere; Sealed tube; | 78% |
Conditions | Yield |
---|---|
With aluminum (III) chloride In dichloromethane at 0 - 20℃; Friedel-Crafts Acylation; Inert atmosphere; | 100% |
With aluminium trichloride In nitrobenzene for 12h; Ambient temperature; | 92% |
With aluminium trichloride In nitrobenzene at 0 - 22℃; for 20h; | 81% |
triphenylene
triphenylene-d12
Conditions | Yield |
---|---|
With [mesitylenium]B(C6F5)4; benzene-d6 at 20℃; for 24h; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
With zirconium(IV) chloride In dichloromethane at 20℃; for 64h; Friedel-Crafts Acylation; regioselective reaction; | 97% |
triphenylene
2,3,6,7,10,11-hexabromo-triphenylene
Conditions | Yield |
---|---|
With bromine; iron In nitrobenzene at 20 - 205℃; for 18.25h; | 95% |
With bromine; iron In nitrobenzene at 20 - 205℃; for 18.25h; | 95% |
With bromine; iron In nitrobenzene at 20 - 210℃; for 3.33h; Inert atmosphere; | 94.8% |
2,4,6-tri(4-pyridyl)-1,3,5-triazine
triphenylene
silver trifluoromethanesulfonate
Conditions | Yield |
---|---|
Stage #1: [Cp*2Rh2(2,2'-bisbenzimidazole)Cl2]; silver trifluoromethanesulfonate at 20℃; for 12h; Darkness; Inert atmosphere; Schlenk technique; Stage #2: 2,4,6-tri(4-pyridyl)-1,3,5-triazine for 4h; Inert atmosphere; Schlenk technique; Stage #3: triphenylene | 92.5% |
2,4,6-tri(4-pyridyl)-1,3,5-triazine
triphenylene
(ethylenediamine)palladium(II) dinitrate
water
Conditions | Yield |
---|---|
In water-d2 at 40℃; for 2h; | 92% |
triphenylene
B
2,3,6,7,10,11-hexabromo-triphenylene
Conditions | Yield |
---|---|
With bromine; iron In nitrobenzene at 205℃; for 12h; | A n/a B 92% |
2,4,6-tri(4-pyridyl)-1,3,5-triazine
triphenylene
(ethylenediamine)palladium(II) dinitrate
water
Conditions | Yield |
---|---|
In water-d2 at 40℃; for 23h; | 91% |
triphenylene
(η6-1,3,5-cyclooctatriene)(η4-1,5-cyclooctadiene)ruthenium(0)
[Ru(η6-triphenylene)(1-5-η5-cyclooctadienyl)]PF6
Conditions | Yield |
---|---|
In diethyl ether under N2 atm. to soln. Ru complex and triphenylene in Et2O HPF6 was added; ppt. was recrystd. from CH2Cl2-Et2O at -30°C; elem. anal.; | 90% |
2,4,6-tris(pyridin-3-yl)-1,3,5-triazine
triphenylene
silver trifluoromethanesulfonate
Conditions | Yield |
---|---|
In methanol byproducts: AgCl; stirred at reflux for 24 h; filtered, solvent-removed, dissolved in CH2Cl2, pptd. (Et2O), filtered, dried (vac.); elem. anal.; | 89% |
Conditions | Yield |
---|---|
In methanol at 20℃; for 8h; In air; | 88% |
In methanol react. tetrol and 1,4-benzenedi(boronic acid), triphenylene in MeOH at room temp. for 6 h; | 86% |
triphenylene
3,6‐di‐tert‐butyl‐1,8‐diethynylcarbazole
Conditions | Yield |
---|---|
Stage #1: 3,6‐di‐tert‐butyl‐1,8‐diethynylcarbazole With sodium hydroxide In methanol at 80℃; for 1h; Stage #2: triphenylene; C42H58Au2I2N4 In methanol at 80℃; for 4h; | 88% |
2,4,6-tri(4-pyridyl)-1,3,5-triazine
triphenylene
silver trifluoromethanesulfonate
Conditions | Yield |
---|---|
In methanol to mixt. of Ru complex and Ag triflate in MeOH added triazine deriv. andtriphenylene; mixt. stirred at reflux for 24 h; filtered, solvent removed, residue dissolved in CH2Cl2, Et2O added for pptn.. solid filtered, dried under vac.; elem. anal.; | 87% |
triphenylene
2-bromobenzo[9,10]phenanthrene
Conditions | Yield |
---|---|
With bromine In dichloromethane at 20℃; for 12h; Inert atmosphere; | 86.3% |
With N-Bromosuccinimide; iron(III) chloride hexahydrate In tetrachloromethane for 7h; Reflux; Heating; | 54% |
With carbon disulfide; bromine; iron |
2,4,6-tri(4-pyridyl)-1,3,5-triazine
triphenylene
silver trifluoromethanesulfonate
Conditions | Yield |
---|---|
In dichloromethane Ru compd. (0.14 mmol) and AgOTf (0.28 mmol) stirred at room temp. for 3 h, filtered, tpt (0.09 mmol) and triphenylene (0.04 mmol) added, mixt. refluxed for 15 h; evapd., dissolved (CH2Cl2), pptd. (Et2O), filtered off, dried (vac.), elem. anal.; | 86% |
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