Hebei yanxi chemical co. LTD. After many years of efforts, we have established stable and friendly business relations with dozens of European and American pharmaceutical companies, multinational chemical companies and importers.At home and many
Cas:24964-64-5
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inquiry3-cyanobenzaldehyde Cas No.:24964-64-5 Molecular Formula:C8H5NO Boiling point : 209-210℃ Melting point: 79-81 ℃ Assay: 99%min ISO9001 Appearance:white crystal Storage:Store in dry and cool place with good seal Package: 25kg/drum, or as
Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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Established in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
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inquiry3-Cyanobenzaldehyde Basic information Product Name: 3-Cyanobenzaldehyde Synonyms: 3-ForMylbenzonitrile, 97+%;24964-64-5;3-Formylbenzonitrile 98%;3-methanoylbenzonitrile;3-Cyanobenzaldyhyde / benzonitrile, 3-formyl-;M-CYANOBENZALDEHYDE;3-CYANOB
Cas:24964-64-5
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiry3-(hydroxymethyl)benzonitrile
3-Cyanobenzaldehyde
Conditions | Yield |
---|---|
With N-hydroxyphthalimide; oxygen; 3-chlorobenzoate; cobalt(II) acetate In acetonitrile at 20℃; for 2h; | 98% |
With fluorosulfonyl fluoride; potassium carbonate; dimethyl sulfoxide at 20℃; for 12h; chemoselective reaction; | 92% |
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen; rac-Ala-OH; iron(II) bromide In 1,4-dioxane for 12h; Reflux; Green chemistry; | 89% |
ethyl 3-cyanobenzoate
3-Cyanobenzaldehyde
Conditions | Yield |
---|---|
With n-butyllithium; diisobutylaluminium hydride; tert-butyl alcohol In tetrahydrofuran; hexane at 0℃; | 97% |
3-(1,3-dioxolan-2-yl)-benzonitrile
3-Cyanobenzaldehyde
Conditions | Yield |
---|---|
In(OSO2CF3)3 In acetone at 100℃; for 0.0833333h; microwave irradiation; | 94% |
With Ti(4+)-exchanged montmorillonite In water; acetone at 60℃; for 6h; | 95 % Chromat. |
3-cyano-N,N-diethylbenzamide
3-Cyanobenzaldehyde
Conditions | Yield |
---|---|
With zirconocene dichloride; lithium tri-t-butoxyaluminum hydride In tetrahydrofuran at 20℃; for 0.166667h; Inert atmosphere; | 94% |
Conditions | Yield |
---|---|
With dichloro[bis{1-(dicyclohexylphosphanyl)piperidine}]palladium; sodium carbonate In 1-methyl-pyrrolidin-2-one at 140℃; for 6h; Inert atmosphere; | 93% |
With hydrogen tetrachloropalladate; sodium phosphate In N,N-dimethyl-formamide at 120℃; for 8h; Inert atmosphere; | 65 %Spectr. |
With tri-tert-butyl phosphine; potassium carbonate In N,N-dimethyl-formamide at 120℃; for 15h; Inert atmosphere; | 92 %Chromat. |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 120℃; for 9h; Inert atmosphere; | 92% |
With potassium carbonate In N,N-dimethyl-formamide at 120℃; for 9h; Inert atmosphere; | 92 %Chromat. |
4-(methylamino)phenyl thiocyanate
3-Formylphenylboronic acid
3-Cyanobenzaldehyde
Conditions | Yield |
---|---|
With N,N,N-trimethyl-2-(sulfooxy)ethanaminium palladium(II) chloride; sodium carbonate In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; water for 2h; | 91% |
3-(hydroxyimino)methylbenzonitrile
3-Cyanobenzaldehyde
Conditions | Yield |
---|---|
With zinc(II) nitrate; silica gel for 0.0666667h; deoxymation; Irradiation; | 90% |
2-methyl-3-thiocyanato-1H-indole
3-Formylphenylboronic acid
3-Cyanobenzaldehyde
Conditions | Yield |
---|---|
With N,N,N-trimethyl-2-(sulfooxy)ethanaminium palladium(II) chloride; sodium carbonate In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; water for 2h; | 90% |
3-(bromomethyl)benzonitrile
3-Cyanobenzaldehyde
Conditions | Yield |
---|---|
With pyridine N-oxide; silver(l) oxide In acetonitrile at 50℃; | 84% |
With chloroform; hexamethylenetetramine Erhitzen des Reaktionsprodukts mit wss. Essigsaeure; | |
With potassium carbonate; dimethyl sulfoxide at 90℃; Kornblum Aldehyd Synthesis; |
3-Cyanobenzoic acid
3-Cyanobenzaldehyde
Conditions | Yield |
---|---|
With thexylchloroborane-Me2SO4 In dichloromethane for 24h; Ambient temperature; | 83% |
With palladium(II) acetylacetonate; hydrogen; 2,2-dimethylpropanoic anhydride; dicyclohexylphenylphosphine In tetrahydrofuran at 80℃; under 3750.38 Torr; for 20h; Inert atmosphere; | 78% |
With P(p-CH3OC6H4)3; methylphenylsilane; 2,2-dimethylpropanoic anhydride; bis(dibenzylideneacetone)-palladium(0) In toluene at 80℃; for 20h; Schlenk technique; Inert atmosphere; | 63% |
3-cyanostyrene
3-Cyanobenzaldehyde
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; water at 90℃; for 12h; | 81% |
3-Chlorobenzaldehyde
3-Cyanobenzaldehyde
Conditions | Yield |
---|---|
With 2-[2-(dicyclohexylphosphino)-phenyl]-1-methyl-1H-indole; palladium diacetate; sodium carbonate; triethylamine In water; acetonitrile at 70℃; for 18h; | 71% |
Conditions | Yield |
---|---|
With sodium carbonate; palladium diacetate at 120℃; for 16h; | 66% |
Conditions | Yield |
---|---|
With water; tri tert-butylphosphoniumtetrafluoroborate; zinc; tris(dibenzylideneacetone)dipalladium(0) chloroform complex In 1-methyl-pyrrolidin-2-one at 20℃; for 24h; | 65% |
With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; 1,2-Ph2-3,4-bis(2,4,6-(t-Bu)3-phenylphophinidene)cyclobutene; zinc In various solvent(s) at 100℃; for 16h; | 61% |
Conditions | Yield |
---|---|
With nickel(II) chloride hexahydrate; (4s,6s)-2,4,5,6-tetra(9H-carbazol-9-yl)isophthalonitrile; caesium carbonate; 4,4'-di-tert-butyl-2,2'-bipyridine In N,N-dimethyl-formamide at 20℃; for 24h; Schlenk technique; Inert atmosphere; Irradiation; | 60% |
3-Methylbenzonitrile
3-Cyanobenzaldehyde
Conditions | Yield |
---|---|
With oxygen In water at 150℃; under 30002.4 Torr; for 2h; | 55% |
With bromine at 150℃; Irradiation.UV-Licht; Erwaermen des Reaktionsprodukts mit Calciumcarbonat und Wasser; | |
Multi-step reaction with 2 steps 1: chromium trioxide, acetic acid 2: water View Scheme | |
Multi-step reaction with 2 steps 1: chlorine / 150 °C 2: silver nitrate View Scheme |
3-Cyanobenzaldehyde
Conditions | Yield |
---|---|
With methanesulfonic acid In [D3]acetonitrile at 20℃; for 24h; Molecular sieve; | 31% |
2-acetonyl-5,5-dimethyl-2-oxo-1,3,2-dioxaphosphorinane
4-cyano-1-(dimorpholinomethyl)benzene
A
3-Cyanobenzaldehyde
Conditions | Yield |
---|---|
With chloroacetic acid In toluene for 3h; Ambient temperature; Yield given. Title compound not separated from byproducts; | A 6% B n/a C n/a |
3-(dichloromethyl)benzonitrile
3-Cyanobenzaldehyde
Conditions | Yield |
---|---|
With silver nitrate |
3-(chloromethyl)benzonitrile
3-Cyanobenzaldehyde
Conditions | Yield |
---|---|
With cuprous nitrate |
Conditions | Yield |
---|---|
With water; copper(II) sulfate |
(3-Cyan-benzyl)-phenyl-sulfid
A
diphenyl sulfide
B
1,2-bis(3-cyanophenyl)ethane
C
3-Cyanobenzaldehyde
D
3-Methylbenzonitrile
E
diphenyldisulfane
Conditions | Yield |
---|---|
In tert-butyl alcohol Mechanism; Irradiation; |
3-[(dimethylamino)methyl]benzonitrile
A
3-Cyanobenzaldehyde
B
3-((methylamino)methyl)benzonitrile
Conditions | Yield |
---|---|
With iodosylbenzene; meso-tetraphenylporphyrin iron(III) chloride In benzene | |
With iodosylbenzene; meso-tetraphenylporphyrin iron(III) chloride In benzene relative rate of oxidation; other catalyst; |
ethanedinitrile
benzaldehyde
A
3-Cyanobenzaldehyde
B
o-formylbenzonitrile
C
benzonitrile
D
4-cyanobenzaldehyde
Conditions | Yield |
---|---|
gaseous plasma of glow discharge; Yield given. Further byproducts given. Yields of byproduct given; |
carbon monoxide
benzonitrile
A
3-Cyanobenzaldehyde
B
4-Cyanobenzyl alcohol
C
o-formylbenzonitrile
D
3-(hydroxymethyl)benzonitrile
Conditions | Yield |
---|---|
RhCl(CO)(PMe3)2 under 760 Torr; for 16.5h; Ambient temperature; Irradiation; Yield given. Further byproducts given. Yields of byproduct given; |
carbon monoxide
benzonitrile
A
3-Cyanobenzaldehyde
B
o-formylbenzonitrile
C
3-(hydroxymethyl)benzonitrile
D
4-cyanobenzaldehyde
Conditions | Yield |
---|---|
RhCl(CO)(PMe3)2 under 760 Torr; for 16.5h; Ambient temperature; Irradiation; Yield given. Further byproducts given. Yields of byproduct given; |
3-((Z)-2-Cyano-3-oxo-3-phenyl-propenyl)-benzonitrile
A
3-Cyanobenzaldehyde
B
Benzoylacetonitrile
Conditions | Yield |
---|---|
With hydrogenchloride; water In ethanol; water at 25℃; Rate constant; Thermodynamic data; ΔH(excit.), ΔS(excit), pH dependence of the rate of hydrolysis; |
m-cyanobenzaldiacetate
3-Cyanobenzaldehyde
Conditions | Yield |
---|---|
With water |
3-Cyanobenzaldehyde
3-(hydroxyimino)methylbenzonitrile
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride; sodium hydroxide In ethanol; water at 25℃; for 1h; Cooling with ice; | 100% |
With sodium hydroxide; hydroxylamine hydrochloride In ethanol; water at 25 - 30℃; for 1h; | 94% |
With hydroxylamine In pyridine; ethanol | 90% |
3-Cyanobenzaldehyde
tert‐butyl 3‐aminopiperidine‐1‐carboxylate
trifluoroacetic acid
Conditions | Yield |
---|---|
Multistep reaction; | 100% |
3-Cyanobenzaldehyde
debenzyldonepezil
Conditions | Yield |
---|---|
Stage #1: 3-Cyanobenzaldehyde; debenzyldonepezil In 1,2-dichloro-ethane Stage #2: With sodium tris(acetoxy)borohydride; acetic acid In 1,2-dichloro-ethane at 20℃; for 3h; | 100% |
With sodium tris(acetoxy)borohydride; acetic acid In ethyl acetate; 1,2-dichloro-ethane |
3-Cyanobenzaldehyde
3-(1,3-dioxolan-2-yl)-benzonitrile
Conditions | Yield |
---|---|
With p-toluenesulfonic acid monohydrate In ethylene glycol; toluene | 100% |
tryptamine
3-Cyanobenzaldehyde
3-(2,3,4,9-tetrahydro-1H-pyrido[3,4-b] indol-1-yl)benzonitrile
Conditions | Yield |
---|---|
With trifluoroacetic acid In 1,1-dichloroethane Reflux; | 100% |
With trifluoroacetic acid In dichloromethane at 20℃; for 24h; Pictet-Spengler Synthesis; | 18% |
3-Cyanobenzaldehyde
N-(3-cyano-benzylidene)-N'-(7-morpholin-4-yl-2-phenyl-pyrazolo[1,5-a]pyrimidin-5-yl)-hydrazine
Conditions | Yield |
---|---|
Stage #1: 3-Cyanobenzaldehyde; (7-morpholin-4-yl-2-phenyl-pyrazolo[1,5-a]pyrimidin-5-yl)hydrazine trifluoroacetate In ethanol at 1 - 30℃; for 1h; Stage #2: With NH-silica gel In methanol; dichloromethane | 100% |
3-Cyanobenzaldehyde
1,3-diaminoguanidine hydrochloride
Conditions | Yield |
---|---|
In ethanol for 16h; Reflux; | 100% |
In ethanol for 16h; Reflux; |
3-Cyanobenzaldehyde
1,3-di(aminomethyl)benzene
Conditions | Yield |
---|---|
With ammonia; hydrogen In methanol at 100℃; under 37503.8 Torr; for 5h; | 100% |
With ammonia; hydrogen In methanol at 80℃; under 22502.3 Torr; for 5h; | 74% |
Conditions | Yield |
---|---|
In ethanol at 20℃; | 100% |
diethyl (N-methoxy-N-methylcarbamoylmethyl)phosphonate
3-Cyanobenzaldehyde
Conditions | Yield |
---|---|
Stage #1: diethyl (N-methoxy-N-methylcarbamoylmethyl)phosphonate With sodium hydride In tetrahydrofuran at 20℃; Horner-Wadsworth-Emmons Olefination; Stage #2: 3-Cyanobenzaldehyde In tetrahydrofuran at -78 - 20℃; Horner-Wadsworth-Emmons Olefination; | 100% |
3-Cyanobenzaldehyde
3-(hydroxymethyl)benzonitrile
Conditions | Yield |
---|---|
With [Ir(2,2':6',2'’-terpyridine)(1,10-phenanthroline)Cl](PF6)2; sodium formate In ethanol; water at 100℃; for 0.333333h; Microwave irradiation; chemoselective reaction; | 99% |
With sodium tetrahydroborate In ethanol for 0.666667h; | 98% |
With sodium tetrahydroborate In tetrahydrofuran; methanol | 98% |
3-Cyanobenzaldehyde
Conditions | Yield |
---|---|
With hydrazine hydrate In methanol at 20℃; for 1h; | 99% |
With hydrazine hydrate In ethanol for 3h; Condensation; Heating; | 77% |
With hydrazine hydrate In ethanol at 20℃; for 3h; | 77% |
With hydrazine hydrate In ethanol at 20℃; for 3h; Inert atmosphere; | 77% |
With hydrazine hydrate In ethanol at 20℃; for 3h; Inert atmosphere; |
3-Cyanobenzaldehyde
3-cyanobenzaldehyde oxime
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride; sodium acetate In ethanol at 20℃; for 3h; | 99% |
With hydroxylamine hydrochloride | |
With hydroxylamine hydrochloride In pyridine; ethanol; water | 19.2 g (69%) |
With hydroxylamine hydrochloride In pyridine; ethanol; water | 19.2 g (69%) |
3-Cyanobenzaldehyde
allyl-trimethyl-silane
3-[1-[(trimethylsilyl)oxy]-3-buten-1-yl]benzonitrile
Conditions | Yield |
---|---|
With Montmorillonite K10 clay In dichloromethane at 0 - 20℃; for 1.08333h; Hosomi-Sakurai reaction; | 99% |
Conditions | Yield |
---|---|
With barium hydroxide octahydrate In tetrahydrofuran at 20℃; for 0.25h; Pudovik Reaction; | 99% |
3-Cyanobenzaldehyde
C18H13F6N3O2
3-((4’-oxo-3’-(4-(trifluoromethoxy)phenyl)-7’-(trifluoromethyl)-3’,4’-dihydro-1‘H-spiro[azetidine-3,2’-quinazolin]-1-yl)methyl)benzonitrile
Conditions | Yield |
---|---|
With caesium carbonate In acetonitrile at 50℃; for 2h; | 99% |
3-Cyanobenzaldehyde
4-amino-1-phenylpiperazine
Conditions | Yield |
---|---|
In toluene at 100℃; for 6h; | 99% |
3-Cyanobenzaldehyde
2-amino-1-benzylamine
Conditions | Yield |
---|---|
In methanol at 20℃; Pictet-Spengler Synthesis; Sealed tube; | 99% |
Conditions | Yield |
---|---|
In methanol at 20℃; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With copper(II) bis(trifluoromethanesulfonate) In dichloromethane at 20℃; for 16h; Oleksyszyn Synthesis; | 99% |
Conditions | Yield |
---|---|
With hydrogenchloride In water at 20 - 45℃; for 3.08333h; | 98.9% |
3-Cyanobenzaldehyde
malononitrile
2-(3-cyanobenzylidene)malononitrile
Conditions | Yield |
---|---|
In neat (no solvent) at 60℃; for 4h; | 98% |
With dimethyl 3-methyl-9-oxo-7-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-2,4-di(pyridin-2-yl)-3,7-diazabicyclo-[3.3.1]nonane-1,5-dicarboxylate In water at 40℃; for 2h; Knoevenagel Condensation; | 91% |
In water at 100℃; for 0.05h; Microwave irradiation; | 82% |
3-Cyanobenzaldehyde
ethyl bromoacetate
ethyl (E)-3-(3-cyanophenyl)-2-propenoate
Conditions | Yield |
---|---|
With triphenylphosphine; nanocrystalline aerogel prepared MgO In N,N-dimethyl-formamide at 20℃; for 4h; Wittig reaction; | 98% |
3-Cyanobenzaldehyde
benzene-1,3-dicarbonitrile
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride; 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; triethylamine In ethyl acetate; N,N-dimethyl-formamide at 100℃; | 98% |
With hydroxylamine hydrochloride; zinc(II) oxide for 0.0166667h; Microwave irradiation; neat (no solvent); | 91% |
Multi-step reaction with 2 steps 1: hydroxylamine hydrochloride 2: 19 percent Chromat. / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / acetonitrile / 0.5 h / Photolysis View Scheme |
3-Cyanobenzaldehyde
ethyl 2-cyanoacetate
2-cyano-3-(3-cyanophenyl)propionic acid ethyl ester
Conditions | Yield |
---|---|
With diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate; L-proline In ethanol at 25℃; cascade Knoevenagel olefination/hydrogenation reaction; Combinatorial reaction / High throughput screening (HTS); stereospecific reaction; | 98% |
3-Cyanobenzaldehyde
cyclohexanone
(2S,1'R)-2-[1'-hydroxy-1'-(3-cyanophenyl)methyl]cyclohexanone
Conditions | Yield |
---|---|
With (S)-N-{(R)-1-[3-(3,5-bis(trifluoromethyl)phenyl)ureido]-2-phenylethyl}pyrrolidine-2-carboxamide; 4-nitro-benzoic acid In toluene at -20℃; for 72h; Aldol Addition; enantioselective reaction; | 98% |
Stage #1: 3-Cyanobenzaldehyde With (S)-N-(2-(adamantane-1-carboxamidophenyl))prolinamide; sodium chloride at 0℃; for 0.25h; Aldol Addition; Stage #2: cyclohexanone for 48h; Aldol Addition; stereoselective reaction; | 90% |
With (2S)-N-[(2S,3S,4R,5S)-2-(tert-butyldiphenylsilyloxy)-4,5-dihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-3-yl]pyrrolidin-2-carboxamide In sodium chloride at 4℃; for 48h; Aldol condensation; optical yield given as %ee; enantioselective reaction; | 86% |
Conditions | Yield |
---|---|
With 3-(7,7-dimethyl-2-oxobicyclo[2.2.1]hept-1-yl)methyl-1-(2,4,6-trimethylphenyl)-1H-imidazol-3-ium iodine salt; caesium carbonate In toluene at 60℃; for 3h; | 98% |
With C22H29N2O(1+)*I(1-); caesium carbonate In toluene at 60℃; for 3h; | 95% |
With potassium carbonate In water at 20℃; for 5h; | 65% |
With potassium cyanide; potassium iodide at 75 - 80℃; for 24h; |
3-Cyanobenzaldehyde
Conditions | Yield |
---|---|
With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane at 20℃; Suzuki Coupling; | 98% |
3-Cyanobenzaldehyde
tert-butyldimethylsilyl cyanide
Conditions | Yield |
---|---|
With cesium fluoride In acetonitrile at 25℃; for 12h; Inert atmosphere; | 98% |
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