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inquiryIt is a kind of important chemical raw materials with a colorless liquid at room temperature. It has a strong unpleasant ammonia smell under high concentrations of compressed or liquefied, and Soluble in water, methanol, ethanol, acetone, butanone,
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inquiry1,3-Bis(aminomethyl)benzene Basic information Product Name: 1,3-Bis(aminomethyl)benzene Synonyms: LABOTEST-BB LT00053687;1,3-BIS(AMINOMETHYL)BENZENE;1,3-Benzenedimethanamine;ALPHA,ALPHA&
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A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiry1,3-Bis(aminomethyl)benzene CAS 1477-55-0 Description Purity: 99% Min Application: Intermediates Appearance: Powder Package: Bag Delivery: 3-5days Our Advantage & Service 1.Top quality: Using high quality material and establishing
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inquirymoderate price & quick delivery. Appearance:clear slightly yellow liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Mainly used in the m
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiry3-Cyanobenzaldehyde
1,3-di(aminomethyl)benzene
Conditions | Yield |
---|---|
With ammonia; hydrogen In methanol at 100℃; under 37503.8 Torr; for 5h; | 100% |
With ammonia; hydrogen In methanol at 80℃; under 22502.3 Torr; for 5h; | 74% |
Conditions | Yield |
---|---|
With ammonia; hydrogen In methanol at 100℃; under 22502.3 Torr; for 2h; Pressure; Reagent/catalyst; Temperature; | 99% |
With hydrogen; cobalt/diatomaceous earth catalyst "G67", cobalt content=56percent; pretreatment is given in full text In 1,2,4-Trimethylbenzene; ammonia at 100℃; for 50h; Product distribution / selectivity; | 96.2% |
With hydrogen; Ni(NO3)2, Cu(NO3)2, Cr(NO3)3, Na2CO3; calcined at 380 deg C for 18 h; pretreatment is given in full text In 1,2,4-Trimethylbenzene; ammonia at 80℃; for 24h; Product distribution / selectivity; | 95.2% |
Conditions | Yield |
---|---|
With Co-doped zirconium dioxide; ammonia; hydrogen; N-butylamine In methanol at 99.84℃; for 10h; Autoclave; chemoselective reaction; | 97% |
benzene-1,3-dicarbonitrile
A
1,3-di(aminomethyl)benzene
B
3-methyl-benzenemethanamine
Conditions | Yield |
---|---|
With hydrogen; Ni(NO3)2, Cu(NO3)2, Cr(NO3)3, Na2CO3; calcined at 380 deg C for 18 h; pretreatment is given in full text In 1,2,4-Trimethylbenzene; ammonia at 80℃; for 24h; Product distribution / selectivity; | A 96.8% B 0.1% |
With hydrogen; Ni(NO3)2, Cu(NO3)2, Cr(NO3)3, Na2CO3; calcined at 380 deg C for 18 h; activated with H2 In 1,2,4-Trimethylbenzene; ammonia at 80℃; for 24h; Product distribution / selectivity; | A 92.1% B 0.1% |
Conditions | Yield |
---|---|
With ammonia; hydrogen; catalyst A In mata-xylene at 80 - 110℃; Conversion of starting material; | A 93.1% B 5.5% |
benzene-1,3-dicarbonitrile
A
1,3-di(aminomethyl)benzene
B
3-(aminomethyl)benzonitrile
Conditions | Yield |
---|---|
With hydrogen; nickel catalyst "NDHT"; pretreatment is given in full text In methanol; ammonia at 65℃; for 4h; Product distribution / selectivity; | A 92.8% B 0.2% |
With hydrogen; Pd-alumina In ammonia; 1,3,5-trimethyl-benzene at 50℃; under 36753.7 Torr; | A 7.7% B 87.3% |
With hydrogen; nickel catalyst "NDHT" In methanol; ammonia at 65℃; for 4h; Product distribution / selectivity; autoclave; | A 84.8% B 0.2% |
benzene-1,3-dicarbonitrile
3-(aminomethyl)benzonitrile
1,3-di(aminomethyl)benzene
Conditions | Yield |
---|---|
With hydrogen; catalyst A In ammonia; 1,3,5-trimethyl-benzene at 50℃; under 36753.7 Torr; | 91.1% |
With hydrogen; Ni-diatomaceous earth In ammonia; 1,3,5-trimethyl-benzene at 50℃; under 36753.7 Torr; | 89.4% |
benzene-1,3-dicarbonitrile
ammonia
m-xylene
A
1,3-di(aminomethyl)benzene
B
3-(aminomethyl)benzonitrile
Conditions | Yield |
---|---|
With hydrogen; Ni-3266E manufactured by Harshaw Co., Ltd.; nickel content: about 50percent at 55℃; under 112511 Torr; Product distribution / selectivity; tube reactor; feed rate = 1.5 t/h; supplying hydrogen rate = 100 Nm3/h; | A 91% B 0.1% |
With hydrogen; catalyst A at 55℃; under 52505.3 Torr; Product distribution / selectivity; tube reactor; feed rate = 32 g/h; supplying hydrogen rate = 20 NL/h; | A 90.9% B 0.1% |
Conditions | Yield |
---|---|
Stage #1: 3-(chloromethyl)benzyl chloride With ammonia In methanol at 50℃; for 6h; Stage #2: With sodium hydroxide In water pH=13; Solvent; | 89% |
Conditions | Yield |
---|---|
81.7% | |
79.5% |
Conditions | Yield |
---|---|
With (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); ammonia; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In tert-Amyl alcohol at 150℃; for 20h; Inert atmosphere; Cooling; | 70% |
With (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); ammonia; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In tert-Amyl alcohol at 150℃; under 12001.2 Torr; for 20h; Inert atmosphere; Autoclave; chemoselective reaction; | 70 %Chromat. |
benzene-1,3-dicarbonitrile
methylamine
A
1,3-di(aminomethyl)benzene
B
N,N'-(1,3-phenylenedimethylidyne)bis(methanamine)
Conditions | Yield |
---|---|
With hydrogen; Raney Nickel In tetrahydrofuran at 125℃; under 19393.6 Torr; for 16.6667h; | A 7% B 45.3% C 14.3% |
Conditions | Yield |
---|---|
With hydrogen In tetrahydrofuran at 125℃; under 19393.6 Torr; for 16.6667h; | 44.9% |
With hydrogen; Rh/Al2O3 In tetrahydrofuran at 125℃; under 19393.6 Torr; for 16.6667h; | |
With hydrogen; palladium 10% on activated carbon In tetrahydrofuran at 125℃; under 19393.6 Torr; for 16.6667h; |
benzene-1,3-dicarbonitrile
methylamine
A
1,3-di(aminomethyl)benzene
B
3-(methylaminomethyl)benzylamine
C
N,N′-dimethyl-m-xylylenediamine
D
N,N'-(1,3-phenylenedimethylidyne)bis(methanamine)
Conditions | Yield |
---|---|
With hydrogen; Raney Nickel In tetrahydrofuran at 125℃; under 19393.6 Torr; for 19.6667h; | A 9.5% B 41.3% C 14.5% D 9.4% |
With hydrogen; Raney nickel In tetrahydrofuran at 125℃; under 19393.6 Torr; for 19.6667h; |
1,3-di(aminomethyl)benzene
Conditions | Yield |
---|---|
With ammonia; hydrogen; catalyst A In m-xylene at 100 - 120℃; under 90009 Torr; Conversion of starting material; | 10.8% |
N,N'-(1,3-phenylenebismethylene)bisphthalimide
1,3-di(aminomethyl)benzene
Conditions | Yield |
---|---|
With potassium hydroxide Erhitzen des Reaktionsprodukts mit wss.Salzsaeure; | |
With hydrazine hydrate In ethanol for 4h; Reflux; | |
With sodium hydroxide at 80 - 120℃; under 760.051 Torr; for 2h; Dean-Stark; | 51.5 g |
Conditions | Yield |
---|---|
anschliessendes Erwaermen mit wss.NaOH; |
hydrogenchloride
N,N'-(1,3-phenylenebismethylene)bisphthalimide
A
1,3-di(aminomethyl)benzene
B
benzene-1,2-dicarboxylic acid
Conditions | Yield |
---|---|
at 200 - 220℃; |
1,3-di(aminomethyl)benzene
Conditions | Yield |
---|---|
With hydrogenchloride at 200 - 220℃; |
3-(aminomethyl)benzonitrile
1,3-di(aminomethyl)benzene
Conditions | Yield |
---|---|
With hydrogen; nickel/diatomaceous earth catalyst (nickel 50wtpercent) reduced with hydrogen at 200C at 100℃; under 30003 Torr; Product distribution / selectivity; |
1,3-di(aminomethyl)benzene
Conditions | Yield |
---|---|
With hydrogen; catalyst A In ammonia; xylene at 75℃; under 112511 Torr; Conversion of starting material; The continuous flow reaction .The concentration of benzamide compound-0.011%, benzoic acid compound-0.001%; | 90.9 %Chromat. |
With hydrogen; catalyst A In ammonia; xylene at 90℃; under 112511 Torr; for 504h; Conversion of starting material; The continuous flow reaction .The concentration of bezamide compound-0.011%, benzoic acid compound-0.001%; | 90.9 %Chromat. |
A
1,3-di(aminomethyl)benzene
B
3-(aminomethyl)benzonitrile
Conditions | Yield |
---|---|
With hydrogen; catalyst A In methanol; ammonia at 80℃; under 150015 Torr; Conversion of starting material; batch-wise method ; concentration benzamide-0.043w.%, benzoic acid-0.004w.%; | A 75.7 %Chromat. B 0.3 %Chromat. |
1,3-di(aminomethyl)benzene
Conditions | Yield |
---|---|
With hydrogen; catalyst A In ammonia; xylene at 75℃; under 112511 Torr; Conversion of starting material; The continuous flow reaction . The concentration of benzamide compound-0.063%, benzoic acid compound-0.001%; | 89.4 %Chromat. |
With hydrogen; catalyst A In ammonia; xylene at 90℃; under 112511 Torr; for 432h; Conversion of starting material; The continuous flow reaction .The concentration of benzamide compound-0.063%, benzoic acid compound-0.001%; | 89.4 %Chromat. |
A
1,3-di(aminomethyl)benzene
B
3-(aminomethyl)benzonitrile
Conditions | Yield |
---|---|
With hydrogen; catalyst A In methanol; ammonia at 80℃; under 150015 Torr; Conversion of starting material; The butch-wize method.The concentration of bezamide-0.30%, benoic acid-0.004%; | A 74.8 %Chromat. B 0.3 %Chromat. |
A
1,3-di(aminomethyl)benzene
B
3-(aminomethyl)benzonitrile
Conditions | Yield |
---|---|
With hydrogen; catalyst A In methanol; ammonia at 80℃; under 150015 Torr; Conversion of starting material; The batch-wize method; | A 70.2 %Chromat. B 0.5 %Chromat. |
A
1,3-di(aminomethyl)benzene
B
3-(aminomethyl)benzonitrile
Conditions | Yield |
---|---|
With hydrogen; catalyst A In methanol; ammonia at 80℃; under 150015 Torr; Conversion of starting material; The batch-wise method; | A 69.9 %Chromat. B 0.9 %Chromat. |
1,3-di(aminomethyl)benzene
Conditions | Yield |
---|---|
With hydrogen; catalyst A In ammonia; xylene at 75℃; under 112511 Torr; Conversion of starting material; The continuous flow reaction .The concentration of benzamide compound-0.114%, benzoic acid compound-0.002%; | 87.8 %Chromat. |
With hydrogen; catalyst A In ammonia; xylene at 90℃; under 112511 Torr; for 288h; Conversion of starting material; The continuous flow reaction .The concentration of benzamide compound-0.114%, benzoic acid compound-0.002%; | 87.8 %Chromat. |
1,3-di(aminomethyl)benzene
Conditions | Yield |
---|---|
With hydrogen; catalyst A In ammonia; xylene at 75℃; under 112511 Torr; Conversion of starting material; The continuous flow reaction .The concentration of benzamide compound-0.012%, bezoic acid compound-0.012%; | 88.8 %Chromat. |
With hydrogen; catalyst A In ammonia; xylene at 90℃; under 112511 Torr; for 408h; Conversion of starting material; The continuous flow reaction .The concentration of benzamide compound-0.012%, benzoic acid compound-0.012%; | 88.8 %Chromat. |
A
1,3-di(aminomethyl)benzene
B
3-(aminomethyl)benzonitrile
Conditions | Yield |
---|---|
With hydrogen; catalyst A In methanol; ammonia at 80℃; under 150015 Torr; Conversion of starting material; The batch-wise method .The concentration of benzamide0.043%, benzoic acid-0.043%; | A 74.1 %Chromat. B 0.2 %Chromat. |
With hydrogen; sodium hydroxide; PDC-3000 In ammonia at 50℃; under 150015 Torr; for 0.5h; Product distribution / selectivity; The batch-wise method . The concentration of benzamide compound-0.043%, benzoic acid compound-0.043%; | A 8.4 %Chromat. B 76 %Chromat. |
1,3-di(aminomethyl)benzene
(2S,3S,11S,12S)-1,4,7,10,13,16-Hexaoxa-cyclooctadecane-2,3,11,12-tetracarbonyl tetrachloride
C32H40N4O10
Conditions | Yield |
---|---|
In toluene | 100% |
1,3-di(aminomethyl)benzene
7,11,15,28-tetrakis(bromomethyl)-1,21,23,25-tetramethyl-2,20:3,19-dimetheno-1H,21H,23H,25H-bis<1,3>dioxocino<5,4-i:5',4'-i'>benzo<1,2-d:5,4-d'>bis<1,3>benzodioxocin
Conditions | Yield |
---|---|
at 100℃; | 100% |
1,3-di(aminomethyl)benzene
Diethyl vinylphosphonate
1,3-bis{(N,N-bis[(diethoxyphosphoryl)ethyl])aminomethyl}benzene
Conditions | Yield |
---|---|
In water at 20℃; Michael condensation; | 100% |
In water at 20℃; for 120h; Aza-Michael reaction; | 83% |
1,3-di(aminomethyl)benzene
4-[(trimethylsilyl)ethynyl]bezaldehyde
C32H36N2Si2
Conditions | Yield |
---|---|
With magnesium sulfate In diethyl ether at 20℃; for 3h; | 100% |
(2S,3S,4R,5S)-1-benzyloxycarbonyl-2-carboxy-5-methylpyrrolidine-3,4-diol
1,3-di(aminomethyl)benzene
Conditions | Yield |
---|---|
With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; | 100% |
Conditions | Yield |
---|---|
In water | 100% |
1,3-di(aminomethyl)benzene
tetrahydrofuran-2,3,4,5-tetracarboxylic acid
Conditions | Yield |
---|---|
In water | 100% |
1,3-di(aminomethyl)benzene
dianhydride of benzophenone-3,4,3',4'-tetracarboxy acid
Conditions | Yield |
---|---|
In water for 0.5h; | 100% |
1,3-di(aminomethyl)benzene
Conditions | Yield |
---|---|
With hydrogenchloride In 1,4-dioxane; methanol for 0.166667h; | 100% |
Conditions | Yield |
---|---|
Stage #1: 1,3-di(aminomethyl)benzene With hydrogenchloride In water; 1,2-dichloro-benzene at 20℃; Autoclave; Large scale; Stage #2: phosgene In water; 1,2-dichloro-benzene at 145℃; for 2h; Autoclave; Large scale; | 99.9% |
With picoline In dichloromethane at -5 - 140℃; for 4h; Reagent/catalyst; Temperature; | 98.3% |
Stage #1: 1,3-di(aminomethyl)benzene With hydrogenchloride In chlorobenzene at 10℃; under 750.075 Torr; for 1.5h; Flow reactor; Large scale; Stage #2: phosgene In chlorobenzene at 131℃; under 750.075 Torr; for 3h; Temperature; Pressure; Solvent; Flow reactor; Large scale; | 98.5% |
1,3-di(aminomethyl)benzene
di-o-tolyl carbonate
1,3-bis-[(methoxycarbonylamino)-methyl]-benzene
Conditions | Yield |
---|---|
With hydrogenchloride In methanol | 99.7% |
1,3-di(aminomethyl)benzene
bis(2,2,3,3-tetrafluoropropyl) carbonate
m-xylylene bis(2,2,3,3-tetrafluoropropylcarbamate)
Conditions | Yield |
---|---|
at 50℃; for 1h; | 99.4% |
1,3-di(aminomethyl)benzene
4-(4'-tert-butyloxycarbonylphenylethynyl)benzoic acid
Conditions | Yield |
---|---|
Stage #1: 4-(4'-tert-butyloxycarbonylphenylethynyl)benzoic acid With oxalyl dichloride In dichloromethane; N,N-dimethyl-formamide Stage #2: 1,3-di(aminomethyl)benzene With triethylamine In dichloromethane Stage #3: With trifluoroacetic acid In dichloromethane | 99% |
1,3-di(aminomethyl)benzene
epichlorohydrin
N,N,N',N'-tetraglycidyl-m-xylylenediamine
Conditions | Yield |
---|---|
With N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide In water; toluene at 90℃; for 1h; Product distribution / selectivity; Inert atmosphere; | 98.4% |
1,3-di(aminomethyl)benzene
Methyl formate
carbonic acid dimethyl ester
1,3-bis-[(methoxycarbonylamino)-methyl]-benzene
Conditions | Yield |
---|---|
With sodium methylate In methanol at 70℃; for 3h; | 98.4% |
1,3-di(aminomethyl)benzene
carbonic acid dimethyl ester
1,3-bis-[(methoxycarbonylamino)-methyl]-benzene
Conditions | Yield |
---|---|
lipase from Candida antarctica In toluene at 70℃; for 60h; Product distribution / selectivity; | 98% |
With lead(II) acetate trihydrate; zinc(II) acetate dihydrate In water at 180℃; under 2250.23 Torr; for 6h; Reagent/catalyst; Inert atmosphere; | 98.2% |
With water; sodium methylate In methanol at 50℃; for 3.5h; | 97% |
79.3% |
Conditions | Yield |
---|---|
With trifluoroacetic acid In chloroform at 20℃; for 24h; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
Stage #1: 1,3-di(aminomethyl)benzene; 4-(trifluoromethoxy)-2-formylphenylboronic acid In toluene at 50℃; for 12h; Stage #2: With sodium tetrahydroborate In toluene at 25℃; for 4h; Cooling with ice; | 98% |
1,3-di(aminomethyl)benzene
citraconic acid anhydride
1,3-bis(citraconimidomethyl)benzol
Conditions | Yield |
---|---|
With acetic acid In toluene at 110℃; for 5h; Temperature; Reagent/catalyst; Solvent; | 97.5% |
With acetic acid at 110℃; for 4h; Temperature; Time; | 92% |
1,3-di(aminomethyl)benzene
benzoyl chloride
N,N'-(1,3-phenylenebis(methylene))dibenzamide
Conditions | Yield |
---|---|
With sodium hydroxide at 0℃; for 3h; | 97% |
With (+/-)-propylene oxide In tetrahydrofuran at 20℃; | 67% |
With pyridine |
1,3-di(aminomethyl)benzene
4-oxo-2-(N-phenyl)amino-4H-chromene-3-carbaldehyde
Conditions | Yield |
---|---|
In acetonitrile | 97% |
1,3-di(aminomethyl)benzene
3-benzoylquinoxalin-2(1H)-one
Conditions | Yield |
---|---|
In dimethyl sulfoxide at 150℃; for 72h; | 97% |
1,3-di(aminomethyl)benzene
phthalic anhydride
N,N'-(1,3-phenylenebismethylene)bisphthalimide
Conditions | Yield |
---|---|
In 1-methyl-pyrrolidin-2-one; xylene at 120℃; Product distribution / selectivity; | 97% |
With acetic acid Heating; | 91% |
1,3-di(aminomethyl)benzene
2,3-dimethoxybenzoic acid
N,N'-[1,3-phenylenebis(methylene)]bis-(2,3-dimethoxybenzamide)
Conditions | Yield |
---|---|
Stage #1: 2,3-dimethoxybenzoic acid With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane Stage #2: 1,3-di(aminomethyl)benzene With triethylamine In dichloromethane for 18h; Further stages.; | 97% |
1,3-di(aminomethyl)benzene
3-((trimethylsilyl)ethynyl)benzaldehyde
C32H36N2Si2
Conditions | Yield |
---|---|
With magnesium sulfate In diethyl ether at 20℃; for 3h; | 97% |
1,3-di(aminomethyl)benzene
N-(6-(bromomethyl)-2-pyridyl)pivalamide
C52H68N10O4
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile Reflux; | 97% |
1,3-di(aminomethyl)benzene
salicylaldehyde
2,2'-(1,3-phenylenebis(methylene))bis(azan-1-yl-1-ylidene)bis(methan-1-yl-1-ylidene)diphenol
Conditions | Yield |
---|---|
In ethanol at 20℃; for 0.166667h; Temperature; Microwave irradiation; Green chemistry; | 97% |
In methanol for 3h; Schiff reaction; Heating; | 90% |
With formic acid In ethanol for 10h; Reflux; | 75.2% |
In methanol for 4h; Reflux; | 74% |
In methanol for 2h; Reflux; |
Conditions | Yield |
---|---|
In dichloromethane Inert atmosphere; Reflux; | 97% |
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