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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

3-methoxy-4-methylbenzaldehyde

Cas:24973-22-6

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

4-Methyl-m-anisaldehyde (CHO=1)

Cas:24973-22-6

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 6 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

24973-22-6 3-METHOXY-4-METHYLBENZALDEHYDE

Cas:24973-22-6

Min.Order:1 Kilogram

FOB Price: $1000.0

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

3-METHOXY-4-METHYLBENZALDEHYDE CAS:24973-22-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality or

3-METHOXY-4-METHYLBENZALDEHYDE CAS:24973-22-6

Cas:24973-22-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Benzaldehyde,3-methoxy-4-methyl-

Cas:24973-22-6

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Benzaldehyde,3-methoxy-4-methyl-

Cas:24973-22-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Afine Chemicals Limited

Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments

3-Methoxy-4-methylbenzaldehyde

Cas:24973-22-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Benzaldehyde,3-methoxy-4-methyl-

Cas:24973-22-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

3-Methoxy-4-methylbenzaldehyde

Cas:24973-22-6

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

Hebei Mojin Biotechnology Co.,Ltd

1, High quality with competitive price:2, Fast and safe delivery3.Excellent pre-sales and after-sales service4. Well-trained and professional technologist and sales with rich experience in the field for 5-10 yearsAppearance:see detailed specification

Benzaldehyde,3-methoxy-4-methyl-

Cas:24973-22-6

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

3-methoxy-4-methylbenzaldehyde cas no. 24973-22-6 98%

Cas:24973-22-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Dingyan Chem Co., Ltd

R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou

3-Methoxy-4-Methylbenzaldehyde

Cas:24973-22-6

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

3-METHOXY-4-METHYLBENZALDEHYDE

Cas:24973-22-6

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Xian Changyue Biological Technology Co., Ltd.

best seller Application:API

3-METHOXY-4-METHYLBENZALDEHYDE

Cas:24973-22-6

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as

3-Methoxy-4-methylbenzaldehyde

Cas:24973-22-6

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

Benzaldehyde,3-methoxy-4-methyl-

Cas:24973-22-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

DB BIOTECH CO., LTD

best seller Application:API

3-METHOXY-4-METHYLBENZALDEHYDE

Cas:24973-22-6

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hangzhou Fandachem Co.,Ltd

3-methoxy-4-methylbenzaldehydeAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:pharmaceutical intermediate Transportation:by air, by sea, by express

3-methoxy-4-methylbenzaldehyde

Cas:24973-22-6

Min.Order:0

Negotiable

Type:Other

inquiry

Henan Kanbei Chemical Co.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

3-METHOXY-4-METHYLBENZALDEHYDE

Cas:24973-22-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Changzhou Ansciep Chemical Co.,Ltd.

3-Methoxy-4-methylbenzaldehyde

Cas:24973-22-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Chemlyte Solutions

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

3-methoxy-4-methylbenzaldehyde

Cas:24973-22-6

Min.Order:0

Negotiable

Type:Other

inquiry

Shanghai Chinqesen Biotechnology Co., Ltd.

Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen

24973-22-6

Cas:24973-22-6

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hebei Muhuang Technology Co., Ltd

best seller Application:API

3-METHOXY-4-METHYLBENZALDEHYDE

Cas:24973-22-6

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hunan Russell Chemicals Technology Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China

3-Methoxy-4-methylbenzaldehyde 24973-22-6

Cas:24973-22-6

Min.Order:0

Negotiable

Type:Trading Company

inquiry

AstaTech ( Chengdu) BioPharmaceutical Corp.

Quality assurance, stable process and affordable priceAppearance:detailed see specifications Storage:enquiry Package:according to the clients requirement Application:Pharmaceutical intermediates Transportation:Normal Port:chengdu

3-methoxy-4-methylbenzaldehyde

Cas:24973-22-6

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Shanghai Yuanye Bio-Technology Co., Ltd.

Known for its best quality and competitve price, this chemicals we offered is widely appreciated by our customers.Appearance:White powder Storage:keep sealed and keep from direct light Package:According client's requirements Application:pharmaceutica

3-Methoxy-4-Methylbenzaldehyde manufacturer

Cas:24973-22-6

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Shenzhen Foris Technology Co. LTD

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China

3-Methoxy-4-methylbenzaldehyde 24973-22-6

Cas:24973-22-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

3-METHOXY-4-METHYLBENZALDEHYDE

Cas:24973-22-6

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Bide Pharmatech Ltd

Our mission is to provide high-quality and innovative products to our customers. By offering a broad range of products, custom synthesis and personalized services, Bide can help scientists speeding up their research in the chemical and pharmaceutical

3-Methoxy-4-methylbenzaldehyde

Cas:24973-22-6

Min.Order:0

Negotiable

Type:Other

inquiry

Amadis Chemical Co., Ltd.

1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G

3-methoxy-4-methylbenzaldehyde

Cas:24973-22-6

Min.Order:10 Milligram

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

3-methoxy-4-methylbenzyl alcohol
4685-50-1

3-methoxy-4-methylbenzyl alcohol

3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

Conditions
ConditionsYield
With Dess-Martin periodane In dichloromethane at 0℃; for 0.5h;100%
With manganese(IV) oxide In tetrahydrofuran for 2h;95%
With manganese(IV) oxide In dichloromethane for 2h; Heating;90%
3-hydroxy-4-methylbenzaldehyde
57295-30-4

3-hydroxy-4-methylbenzaldehyde

dimethyl sulfate
77-78-1

dimethyl sulfate

3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

Conditions
ConditionsYield
With potassium hydroxide at 45℃;91%
With potassium hydroxide87%
3-hydroxy-4-methylbenzaldehyde
57295-30-4

3-hydroxy-4-methylbenzaldehyde

methyl iodide
74-88-4

methyl iodide

3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

Conditions
ConditionsYield
With potassium carbonate91%
Stage #1: 3-hydroxy-4-methylbenzaldehyde With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 0.5h;
Stage #2: methyl iodide In N,N-dimethyl-formamide at 20℃;
91%
3-methoxy-benzaldehyde
591-31-1

3-methoxy-benzaldehyde

methyl iodide
74-88-4

methyl iodide

3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

Conditions
ConditionsYield
Stage #1: 3-methoxy-benzaldehyde With 1-methyl-piperazine; n-butyllithium In tetrahydrofuran; hexane at -20℃; for 0.5h;
Stage #2: With sec.-butyllithium In tetrahydrofuran; hexane; cyclohexane for 0.166667h;
Stage #3: methyl iodide In tetrahydrofuran; hexane; cyclohexane at -78 - 20℃; Further stages.;
29%
Yield given. Multistep reaction;
Succinimide
123-56-8

Succinimide

(2-Bromo-5-methoxy-4-methyl-phenyl)-methanol
57295-33-7

(2-Bromo-5-methoxy-4-methyl-phenyl)-methanol

A

2-Brom-5-methoxy-4-methylbenzaldehyd
57295-32-6

2-Brom-5-methoxy-4-methylbenzaldehyd

B

3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

C

N-(2-Formyl-4-methoxy-5-methylphenyl)succinimid
90163-04-5

N-(2-Formyl-4-methoxy-5-methylphenyl)succinimid

Conditions
ConditionsYield
With copper(l) iodide; sodium hydride 1) dimethylacetamide, 2.,5-3 h, r.t., 2) 6 h, reflux; Yield given. Multistep reaction. Yields of byproduct given;
With copper(l) iodide; sodium hydride 1) dimethylacetamide, 2.5-3 h, r.t., 2) 6 h, reflux; Yield given. Multistep reaction. Yields of byproduct given;
With copper(l) iodide; sodium hydride 1) dimethylacetamide, 2.5-3 h, r.t., 2) 6 h, reflux; Yield given. Multistep reaction. Yields of byproduct given;
formaldehyd
50-00-0

formaldehyd

ortho-cresidine
16452-01-0

ortho-cresidine

3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

Conditions
ConditionsYield
(i) aq. NH2OH*HCl, NaOAc, (ii) CuSO4, Na2SO3, aq. NaOAc, (iii) /BRN= 742602/, NaNO2, aq. HCl; Multistep reaction;
3-methoxy-p-toluic acid
7151-68-0

3-methoxy-p-toluic acid

3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

Conditions
ConditionsYield
(i) SOCl2, (ii) Li; Multistep reaction;
Multi-step reaction with 2 steps
1: LiAlH4 / tetrahydrofuran / 20 °C
2: MnO2 / CHCl3 / 3 h / Heating
View Scheme
Multi-step reaction with 3 steps
1: 91 percent / acetic acid / diethyl ether
2: 88 percent / LiAlH4 / diethyl ether / 2.5 h / Heating
3: 90 percent / active MnO2 / CH2Cl2 / 2 h / Heating
View Scheme
3-Methoxybenzaldehyde 2,4-Dimethylpent-3-ylimine

3-Methoxybenzaldehyde 2,4-Dimethylpent-3-ylimine

methyl iodide
74-88-4

methyl iodide

A

3-methoxy-2-methyl-benzaldehyde
56724-03-9

3-methoxy-2-methyl-benzaldehyde

B

3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

Conditions
ConditionsYield
With hydrogenchloride; N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium 1) ether, cyclohexane, -72 deg C, 1 h; 2) ether, cyclohexane, -72 deg C --> rt; 3) THF, reflux, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
3-hydroxy-4-methylbenzoic acid
586-30-1

3-hydroxy-4-methylbenzoic acid

3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: K2CO3 / acetone / 10 h / Heating
2: LiAlH4 / tetrahydrofuran / 20 °C
3: MnO2 / CHCl3 / 3 h / Heating
View Scheme
4-methyl-3-nitrobenzaldehyde
31680-07-6

4-methyl-3-nitrobenzaldehyde

3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

Conditions
ConditionsYield
Multi-step reaction with 2 steps
2: 91 percent / 33 percent KOH / 45 °C
View Scheme
4-methyl-benzaldehyde
104-87-0

4-methyl-benzaldehyde

KOH

KOH

3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 91 percent / KNO3 / H2SO4
3: 91 percent / 33 percent KOH / 45 °C
View Scheme
methyl 4-methyl-3-methoxybenzoate
3556-83-0

methyl 4-methyl-3-methoxybenzoate

3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 88 percent / LiAlH4 / diethyl ether / 2.5 h / Heating
2: 90 percent / active MnO2 / CH2Cl2 / 2 h / Heating
View Scheme
Multi-step reaction with 2 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 25 °C
2: manganese(IV) oxide / tetrahydrofuran / 2 h
View Scheme
Multi-step reaction with 2 steps
1: diisobutylaluminium hydride / tetrahydrofuran / 5.5 h / -78 - 20 °C
2: pyridinium chlorochromate / dichloromethane / 2 h / 0 - 20 °C
View Scheme
Multi-step reaction with 2 steps
1: diisobutylaluminium hydride / tetrahydrofuran / 5 h / -78 - 20 °C
2: pyridinium chlorochromate / dichloromethane / 2 h / 0 - 20 °C
View Scheme
Multi-step reaction with 2 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere
2: manganese(IV) oxide / chloroform / 18 h / 20 °C
View Scheme
2,6-dimethylpyridine
108-48-5

2,6-dimethylpyridine

3-methoxy-4-methylbenzoyl chloride
87808-44-4

3-methoxy-4-methylbenzoyl chloride

3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

Conditions
ConditionsYield
palladium In tetrahydrofuran
malonic acid
141-82-2

malonic acid

3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

3-(3-Methoxy-4-methylphenyl)-2-propenoic acid
132980-20-2

3-(3-Methoxy-4-methylphenyl)-2-propenoic acid

Conditions
ConditionsYield
Stage #1: malonic acid; 3-methoxy-4-methylbenzaldehyde With piperidine; pyridine for 2.5h; Heating / reflux;
Stage #2: With hydrogenchloride In water
100%
In piperidine; pyridine for 2.5h; Heating / reflux;100%
With piperidine; pyridine for 5h; Heating;99.7%
malonic acid
141-82-2

malonic acid

3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

ferulic acid
209287-19-4

ferulic acid

Conditions
ConditionsYield
With piperidine; pyridine for 2.5h; Heating / reflux; Neat (no solvent);100%
With piperidine; pyridine for 2.5h; Heating / reflux;100%
With piperidine; pyridine at 100℃; Condensation;
malonic acid
141-82-2

malonic acid

3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

3-(3-methyl-4-methoxy-phenyl)-acrylic acid

3-(3-methyl-4-methoxy-phenyl)-acrylic acid

Conditions
ConditionsYield
Stage #1: malonic acid; 3-methoxy-4-methylbenzaldehyde With piperidine; pyridine for 11h; Heating / reflux;
Stage #2: With hydrogenchloride In water
100%
3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

aniline
62-53-3

aniline

(E)-3-Methoxy-4-methyl-N-phenylbenzaldimin

(E)-3-Methoxy-4-methyl-N-phenylbenzaldimin

Conditions
ConditionsYield
99%
3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

3-methoxy-4-methylbenzyl alcohol
4685-50-1

3-methoxy-4-methylbenzyl alcohol

Conditions
ConditionsYield
With sodium tetrahydroborate In methanol98.7%
3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

C9H14O3
115928-76-2

C9H14O3

C18H22O4

C18H22O4

Conditions
ConditionsYield
With piperidine; acetic acid In benzene for 2h; Knoevenagel Condensation; Dean-Stark; Reflux;92%
3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

malonic acid dimethyl ester
108-59-8

malonic acid dimethyl ester

Dimethyl 3-Methoxy-4-methylbenzylidenemalonate
130921-06-1

Dimethyl 3-Methoxy-4-methylbenzylidenemalonate

Conditions
ConditionsYield
With piperidine; benzoic acid In benzene Heating;91%
3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

dimedone
126-81-8

dimedone

β-naphthol
135-19-3

β-naphthol

C27H26O3
1427548-18-2

C27H26O3

Conditions
ConditionsYield
With (2,3,4,5,6-pentafluorophenyl)ammonium triflate In toluene at 50℃; for 6h; Green chemistry;90%
6-methoxy-1,3-benzothiazole
2942-13-4

6-methoxy-1,3-benzothiazole

3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

(6-methoxy-1,3-benzothiazol-2-yl)(4-methyl-3-methoxyphenyl)methanol
1361253-14-6

(6-methoxy-1,3-benzothiazol-2-yl)(4-methyl-3-methoxyphenyl)methanol

Conditions
ConditionsYield
Stage #1: 6-methoxy-1,3-benzothiazole With n-butyllithium In tetrahydrofuran; hexane for 1h; Cooling with acetone-dry ice;
Stage #2: 3-methoxy-4-methylbenzaldehyde In tetrahydrofuran; hexane for 2h; Cooling with acetone-dry ice;
89%
3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

1-(4-methoxyphenyl)ethanone
100-06-1

1-(4-methoxyphenyl)ethanone

(E)-3-(3-methoxy-4-methylphenyl)-1-(4-methoxyphenyl)prop-2-en-1-one

(E)-3-(3-methoxy-4-methylphenyl)-1-(4-methoxyphenyl)prop-2-en-1-one

Conditions
ConditionsYield
Stage #1: 1-(4-methoxyphenyl)ethanone With lithium hydroxide monohydrate In ethanol at 20℃; for 0.25h;
Stage #2: 3-methoxy-4-methylbenzaldehyde In ethanol at 20℃; for 24h;
88%
Nitroethane
79-24-3

Nitroethane

3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

1-(3-methoxy-4-methylphenyl)-2-nitropropene
132980-18-8

1-(3-methoxy-4-methylphenyl)-2-nitropropene

Conditions
ConditionsYield
With ammonium acetate for 2.5h; Heating;83.5%
3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

methyl chloroacetate
96-34-4

methyl chloroacetate

methyl (3-methoxy-4-methylphenyl)glycidate
122333-96-4

methyl (3-methoxy-4-methylphenyl)glycidate

Conditions
ConditionsYield
With sodium methylate In methanol 1) -5 deg C, 2 h, 2) room temperature, 3 h;80%
3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

methyl-triphenylphosphonium iodide
2065-66-9

methyl-triphenylphosphonium iodide

2-methoxy-1-methyl-4-vinylbenzene
501371-37-5

2-methoxy-1-methyl-4-vinylbenzene

Conditions
ConditionsYield
Stage #1: methyl-triphenylphosphonium iodide With sodium hexamethyldisilazane In tetrahydrofuran at 25℃; for 1h; Inert atmosphere;
Stage #2: 3-methoxy-4-methylbenzaldehyde In tetrahydrofuran at 25℃; for 1h; Inert atmosphere;
80%
BARBITURIC ACID
67-52-7

BARBITURIC ACID

3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

malononitrile
109-77-3

malononitrile

C16H14N4O4

C16H14N4O4

Conditions
ConditionsYield
With β‐cyclodextrin In water at 80℃; for 0.633333h;78.5%
3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

cyanomethylene triphenylphosphorane
16640-68-9

cyanomethylene triphenylphosphorane

3-(3-methoxy-4-methylphenyl)acrylonitrile
913073-72-0

3-(3-methoxy-4-methylphenyl)acrylonitrile

Conditions
ConditionsYield
77%
3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

(4-chlorphenyl)magnesium bromide
873-77-8

(4-chlorphenyl)magnesium bromide

(4-chlorophenyl)(3-methoxy-4-methylphenyl)methanone
1096987-59-5

(4-chlorophenyl)(3-methoxy-4-methylphenyl)methanone

Conditions
ConditionsYield
In tetrahydrofuran for 6h; Reflux;77%
nitromethane
75-52-5

nitromethane

3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

3-methoxy-4-methyl-1-[(E)-2′-nitrovinyl]benzene
1391042-74-2

3-methoxy-4-methyl-1-[(E)-2′-nitrovinyl]benzene

Conditions
ConditionsYield
With ammonium acetate In toluene for 18h; Inert atmosphere; Reflux;73%
diethoxyphosphoryl-acetic acid ethyl ester
867-13-0

diethoxyphosphoryl-acetic acid ethyl ester

3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

3-(3-methoxy-4-methylphenyl)-2-propenoic acid ethyl ester
134058-08-5

3-(3-methoxy-4-methylphenyl)-2-propenoic acid ethyl ester

Conditions
ConditionsYield
Stage #1: diethoxyphosphoryl-acetic acid ethyl ester With sodium hydride In tetrahydrofuran Inert atmosphere;
Stage #2: 3-methoxy-4-methylbenzaldehyde In tetrahydrofuran at 20℃; for 20h; Inert atmosphere;
63%
Stage #1: diethoxyphosphoryl-acetic acid ethyl ester With sodium hydride In tetrahydrofuran; hexane for 0.416667h; Inert atmosphere;
Stage #2: 3-methoxy-4-methylbenzaldehyde In tetrahydrofuran; hexane at 20℃; for 20.5h;
63%
With sodium hydride 1.) toluene, 0 deg C, 1 h, 2.) toluene, THF, RT, 20 h; Yield given. Multistep reaction;
N-(5,6-Dihydro-4H-cyclopentathiazol-2-yl)-N'-isopropylidene-hydrazine
21938-30-7

N-(5,6-Dihydro-4H-cyclopentathiazol-2-yl)-N'-isopropylidene-hydrazine

3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

N-(5,6-Dihydro-4H-cyclopentathiazol-2-yl)-N'-[1-(3-methoxy-4-methyl-phenyl)-meth-(E)-ylidene]-hydrazine
82814-17-3

N-(5,6-Dihydro-4H-cyclopentathiazol-2-yl)-N'-[1-(3-methoxy-4-methyl-phenyl)-meth-(E)-ylidene]-hydrazine

Conditions
ConditionsYield
In acetic acid for 0.5h; Heating;61%
3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

1,4-diacetyl-3-(2,4,5-trimethoxy-3-methylphenylmethyl)-2,5-piperazinedione
113296-73-4

1,4-diacetyl-3-(2,4,5-trimethoxy-3-methylphenylmethyl)-2,5-piperazinedione

(Z)-1-acetyl-3-(3-methoxy-4-methylphenylmethylene)-6-(2,4,5-trimethoxy-3-methylphenylmethyl)-2,5-piperazinedione
113321-18-9

(Z)-1-acetyl-3-(3-methoxy-4-methylphenylmethylene)-6-(2,4,5-trimethoxy-3-methylphenylmethyl)-2,5-piperazinedione

Conditions
ConditionsYield
With potassium tert-butylate In N,N-dimethyl-formamide; tert-butyl alcohol for 24h; Ambient temperature;58%
3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

sophoridine
6882-68-4

sophoridine

14-(3-methoxy-4-methylphenylmethylene)sophoridine

14-(3-methoxy-4-methylphenylmethylene)sophoridine

Conditions
ConditionsYield
With sodium hydride In tetrahydrofuran; mineral oil at 37℃; for 13h; Reflux;49%
3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

3-hydroxy-4-methylbenzaldehyde
57295-30-4

3-hydroxy-4-methylbenzaldehyde

Conditions
ConditionsYield
With boron tribromide In dichloromethane at -10 - 20℃; for 6h;41.4%
With boron tribromide In dichloromethane at 20℃; for 5h; Cooling with ice;41.4%
3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

malononitrile
109-77-3

malononitrile

2-(3-methoxy-4-methylbenzylidene)malononitrile

2-(3-methoxy-4-methylbenzylidene)malononitrile

Conditions
ConditionsYield
With L-proline In ethanol at 20℃; for 3h; Knoevenagel Condensation; Inert atmosphere;32%
N-cyclopropylguanidine hydrochloride

N-cyclopropylguanidine hydrochloride

3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

ethyl 2-cyanoacetate
105-56-6

ethyl 2-cyanoacetate

C16H16N4O2
945001-76-3

C16H16N4O2

Conditions
ConditionsYield
With potassium carbonate In ethanol at 75℃; for 18h;29%
3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

2-hydroxy-4-methyl-5-methoxybenzaldehyde
74516-54-4

2-hydroxy-4-methyl-5-methoxybenzaldehyde

Conditions
ConditionsYield
With palladium diacetate; toluene-4-sulfonic acid; 1-fluoro-2,4,6-trimethylpyridinium trifluoromethanesulfonate; acetic acid; 2-Amino-4-chlorobenzoic acid at 90℃; for 24h; Sealed tube;28%
2-thioxo-4-thiazolidinone
141-84-4

2-thioxo-4-thiazolidinone

3-methoxy-4-methylbenzaldehyde
24973-22-6

3-methoxy-4-methylbenzaldehyde

5-(3-methoxy-4-methyl-benzylidene)-2-thioxo-thiazolidin-4-one
58264-65-6

5-(3-methoxy-4-methyl-benzylidene)-2-thioxo-thiazolidin-4-one

Conditions
ConditionsYield
With sodium acetate In acetic acid Heating;

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