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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

1-Phenylhexan-3-one

Cas:29898-25-7

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 1-Phenyl-3-Hexanone supplier in China

Cas:29898-25-7

Min.Order:0 Metric Ton

Negotiable

Type:Manufacturers

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

1-Phenyl-3-hexanone

Cas:29898-25-7

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

1-Phenylhexan-3-one

Cas:29898-25-7

Min.Order:1 Kilogram

FOB Price: $9.0 / 99.0

Type:Trading Company

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

1-Phenylhexan-3-one 29898-25-7

Cas:29898-25-7

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

1-Phenylhexan-3-one

Cas:29898-25-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Wuhan Zenuo Biological Medicine Technology Co Ltd

Product Name: 1-Phenylhexan-3-one Synonyms: B-PHENYLETHYL PROPYL KETONE;1-Phenylhexan-3-one;1-PHENYLHEXANE-3-ONE;1P3H;1-PHENYL-3-HEXANONE;1-Phenylhexanone-3;1-phenyl-3-Cyclohexanone CAS: 29898-25-7 MF: C12H16O MW: 176.25 EINECS: 249-937-9

1-Phenylhexan-3-one Supplier best quality

Cas:29898-25-7

Min.Order:100 Gram

Negotiable

Type:Lab/Research institutions

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

1-Phenyl-3-Hexanone

Cas:29898-25-7

Min.Order:0

Negotiable

Type:Manufacturers

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Taizhou Crene Biotechnology co.ltd

Our company provides one-stop services of research - development - production for a variety of special prouducts. Not only do we make effective use of our strong technological strength, but also establish of cooperative relations with several well-

1-Phenylhexan-3-one cas 29898-25-7

Cas:29898-25-7

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Afine Chemicals Limited

Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments

1-PHENYLHEXAN-3-ONE

Cas:29898-25-7

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 1-phenyl-3-hexanone

Cas:29898-25-7

Min.Order:0 Metric Ton

Negotiable

Type:Other

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

1-Phenyl-3-Hexanone

Cas:29898-25-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Siwei Development Group Ltd.

Product name: 1-Phenylhexan-3-One CAS No.:29898-25-7 Molecule Formula:C12H16O Molecule Weight:176.25 Purity: 99% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS

High Quality 1-Phenylhexan-3-One in stock

Cas:29898-25-7

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

1-Phenyl-hexan-3-one 29898-25-7

Cas:29898-25-7

Min.Order:1 Metric Ton

Negotiable

Type:Lab/Research institutions

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Xiamen Jenny Chemical Technology Co., Ltd.

GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,

1-Phenylhexan-3-one

Cas:29898-25-7

Min.Order:1 Milligram

Negotiable

Type:Trading Company

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Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

1-Phenyl-3-hexanone

Cas:29898-25-7

Min.Order:0

Negotiable

Type:Manufacturers

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Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

1-Phenylhexan-3-one Cas no.29898-25-7 98%

Cas:29898-25-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Greenutra Resource Inc

1-Phenyl-3-hexanoneAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air

1-Phenyl-3-hexanone

Cas:29898-25-7

Min.Order:0

Negotiable

Type:Trading Company

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GIHI CHEMICALS CO.,LIMITED

Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

1-Phenyl-3-hexanone

Cas:29898-25-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

1-Phenyl-3-hexanone

Cas:29898-25-7

Min.Order:0

Negotiable

Type:Other

inquiry

Hangzhou Dingyan Chem Co., Ltd

R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates

1-Phenylhexan-3-one

Cas:29898-25-7

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

DB BIOTECH CO., LTD

Q1: Are you a manufacturer Answer: Yes, we are factory founded on 2012.Q2: How to contact with us Click "contact supplier" And then send us message the product you interest in, you will get reply within 12 hours.Q3:Which kind of payment terms do you

1-Phenylhexan-3-one

Cas:29898-25-7

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Aecochem Corp.

Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS

1-Phenyl-3-Hexanone

Cas:29898-25-7

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Chemsigma International Co.,Ltd.

bulk productiongoods in stockswe have the best competitive price in the marketmeantime,we are committed to service to our every customer Chemsigma International Co.,Ltd. is a chemical manufacturer, specialize in custom synthesis and organic chemical

1-Phenylhexan-3-one

Cas:29898-25-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Antimex Chemical Limied

29898-25-7 C12H16O 1-Phenylhexan-3-oneAppearance:white powder Storage:Normal temperature Package:Woven bag Application:Intermediate Transportation:Ocean shipping Express delivery

29898-25-7 C12H16O 1-Phenylhexan-3-one

Cas:29898-25-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Guangdong Juda Chemical Industrial Co.,Limited

Factory supply high purity low priceAppearance:solid or liquid Storage:sealed in cool and dry place Package:As customer's requested Application:Pharma Intermediate Transportation:by courier/air/sea Port:Any port in China

1-Phenylhexan-3-one CAS No.29898-25-7

Cas:29898-25-7

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hangzhou Fandachem Co.,Ltd

1-Phenylhexan-3-one cas 29898-25-7Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

1-Phenylhexan-3-one cas 29898-25-7

Cas:29898-25-7

Min.Order:0

Negotiable

Type:Other

inquiry

Henan Kanbei Chemical Co.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

1-Phenylhexan-3-one

Cas:29898-25-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hunan Russell Chemicals Technology Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China

1-Phenyl-3-hexanone 29898-25-7

Cas:29898-25-7

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Shenzhen Foris Technology Co. LTD

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China

1-Phenyl-3-hexanone 29898-25-7

Cas:29898-25-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Synthetic route

(E)-1-phenylhex-1-en-3-one
82297-62-9

(E)-1-phenylhex-1-en-3-one

1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

Conditions
ConditionsYield
Pd-C In ethyl acetate99.4%
hex-3-yne
928-49-4

hex-3-yne

N-(3-methyl-2-pyridyl)-N-[(E)-3-phenyl-2-propenyl]amine
256379-28-9

N-(3-methyl-2-pyridyl)-N-[(E)-3-phenyl-2-propenyl]amine

1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

Conditions
ConditionsYield
Stage #1: hex-3-yne; N-(3-methyl-2-pyridyl)-N-[(E)-3-phenyl-2-propenyl]amine With Wilkinson's catalyst; cyclohexylamine In toluene at 130℃; for 12h;
Stage #2: With water; hydrogen cation Further stages.;
93%
3-phenyl-propionaldehyde
104-53-0

3-phenyl-propionaldehyde

hex-3-yne
928-49-4

hex-3-yne

1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

Conditions
ConditionsYield
With 3-methylpyridin-2-ylamine; Wilkinson's catalyst; cyclohexylamine; aluminium trichloride In toluene at 130℃; for 12h;91%
1-phenyl-3-hexanol
2180-43-0

1-phenyl-3-hexanol

1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

Conditions
ConditionsYield
With tert.-butylnitrite; 2-azatricyclo[3.3.1.13,7]dec-2-yloxidanyl In acetonitrile at 20℃; for 6h; chemoselective reaction;90%
With dipyridinium dichromate In dichloromethane for 8h;65%
With chromium(VI) oxide; acetic acid
1-hexene-3-ol
4798-44-1

1-hexene-3-ol

sodium benzenesulfonate
873-55-2

sodium benzenesulfonate

1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

Conditions
ConditionsYield
With 4,7-Dimethyl-1,10-phenanthroline; palladium(II) trifluoroacetate; copper (II) trifluoroacetate hydrate In 1,4-dioxane at 100℃; for 20h; Sealed tube; regioselective reaction;80%
iodobenzene
591-50-4

iodobenzene

1-hexene-3-ol
4798-44-1

1-hexene-3-ol

1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

Conditions
ConditionsYield
With potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)); Tedicyp In N,N-dimethyl-formamide at 130℃; for 20h; Heck reaction;78%
3-phenyl-propionaldehyde
104-53-0

3-phenyl-propionaldehyde

2-bromoprop-1-ene
557-93-7

2-bromoprop-1-ene

1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

Conditions
ConditionsYield
With acetylacetonatodicarbonylrhodium(l); potassium formate; potassium carbonate; triphenylphosphine In 1,2-dimethoxyethane at 130℃; for 16h; Inert atmosphere; Sealed tube;78%
bromobenzene
108-86-1

bromobenzene

methyl 3-hydroxy-2-methylenehexanoate
18020-64-9

methyl 3-hydroxy-2-methylenehexanoate

1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

Conditions
ConditionsYield
With tetrabutylammomium bromide; sodium formate; sodium hydrogencarbonate; Pd-benzothiazole carbene at 130℃; for 20h;77%
3-phenyl-propionaldehyde
104-53-0

3-phenyl-propionaldehyde

tert-butylethylene
558-37-2

tert-butylethylene

hex-3-yne
928-49-4

hex-3-yne

A

1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

B

6,6-dimethylheptan-3-one
5054-71-7

6,6-dimethylheptan-3-one

C

6,6-dimethyl-1-phenyl-3-heptanone

6,6-dimethyl-1-phenyl-3-heptanone

Conditions
ConditionsYield
With 3-methylpyridin-2-ylamine; Wilkinson's catalyst; hexan-1-amine; 4-trifluoromethylbenzoic acid; water In toluene at 150℃; for 24h;A 75%
B 39%
C 6%
2-Pentanone
107-87-9

2-Pentanone

benzyl alcohol
100-51-6

benzyl alcohol

1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

Conditions
ConditionsYield
With trifuran-2-yl-phosphane; C48H34F6N4O4Pd2; lithium hydroxide In neat (no solvent) at 80 - 100℃; for 24h; Inert atmosphere; Schlenk technique; Sealed tube;72%
nickel In tetrahydrofuran at 76℃; for 8h;36%
With nickel(0) nanoparticles In tetrahydrofuran at 76℃; for 8h; Inert atmosphere;36%
styrene
292638-84-7

styrene

butyraldehyde
123-72-8

butyraldehyde

1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

Conditions
ConditionsYield
With tetrakis(tetrabutylammonium)decatungstate(VI); 4,4'-dimethoxyphenyl disulfide In acetonitrile at 20℃; for 18h; Sealed tube; Inert atmosphere; Irradiation;62%
1-iodo-propane
107-08-4

1-iodo-propane

dihydrocinnamonitrile
645-59-0

dihydrocinnamonitrile

1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

Conditions
ConditionsYield
With nickel(II) iodide; samarium diiodide In tetrahydrofuran at 0℃; for 0.5h; Barbier reaction;60%
[3-cyclopropyl-3-(3-iodoallyloxy)-propyl]-benzene
944449-56-3

[3-cyclopropyl-3-(3-iodoallyloxy)-propyl]-benzene

1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

Conditions
ConditionsYield
Stage #1: [3-cyclopropyl-3-(3-iodoallyloxy)-propyl]-benzene With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride In benzene for 36h; Heating;
Stage #2: With potassium fluoride In benzene for 24h; Further stages.;
33%
2-methyl-1-phenethylcyclopropan-1-ol

2-methyl-1-phenethylcyclopropan-1-ol

1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

Conditions
ConditionsYield
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; 10-phenyl-9-(2,4,6-trimethylphenyl)acridinium tetrafluoroborate; diphenyldisulfane In 1,2-dichloro-ethane for 12h; Inert atmosphere; Irradiation;20%
1-phenylhex-1-en-3-one
82297-62-9, 90729-78-5, 4646-80-4

1-phenylhex-1-en-3-one

1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

Conditions
ConditionsYield
With cyclohexene; monoaluminum phosphate; silica gel; palladium at 100℃; for 3h;19.6%
With ethanol; nickel Hydrogenation;
With hydrogen Product distribution / selectivity;
dipropylcadmium
5905-48-6

dipropylcadmium

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

Conditions
ConditionsYield
With benzene
butyric acid
107-92-6

butyric acid

3-Phenylpropionic acid
501-52-0

3-Phenylpropionic acid

1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

Conditions
ConditionsYield
With thorium dioxide
With thorium dioxide at 460℃;
phenyl-1 hexanol-2
60012-62-6

phenyl-1 hexanol-2

1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

Conditions
ConditionsYield
With chromic acid
(Z)-1-phenyl-3-(trimethylsiloxy)-3-hexene
72551-30-5

(Z)-1-phenyl-3-(trimethylsiloxy)-3-hexene

1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

Conditions
ConditionsYield
With hydrogenchloride In methanol Yield given;
benzyl bromide
100-39-0

benzyl bromide

2-Pentanone
107-87-9

2-Pentanone

A

1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

B

3-benzyl-2-pentanone
61780-85-6

3-benzyl-2-pentanone

Conditions
ConditionsYield
With lithium chloride; manganese(ll) chloride; lithium diisopropyl amide 1.) 0 deg C, 1 h; 2.) THF, rt, 1 h then -78 deg C, 1 h; 3.) THF/NMP, -78 deg C, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
1-phenyl-2-(phenylsulfonyl)-hex-1-en-3-one
113549-28-3

1-phenyl-2-(phenylsulfonyl)-hex-1-en-3-one

1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

Conditions
ConditionsYield
With aluminum amalgam
n-propyl-styryl ketone

n-propyl-styryl ketone

1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

Conditions
ConditionsYield
With sodium amalgam; ethanol; acetic acid
propyllithium
2417-93-8

propyllithium

hydrocinnamic acid chloride
645-45-4

hydrocinnamic acid chloride

1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

Conditions
ConditionsYield
Stage #1: propyllithium With copper(l) iodide In diethyl ether at -40℃;
Stage #2: hydrocinnamic acid chloride In diethyl ether at -78℃;
(3-cyclopropyl-3-prop-2-ynyloxypropyl)-benzene
944449-49-4

(3-cyclopropyl-3-prop-2-ynyloxypropyl)-benzene

1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: tributyltin hydride; AINB / benzene / 4 h / Heating
1.2: 0.24 g / I2 / CH2Cl2 / 12 h / 20 °C
2.1: AIBN; tributyltin hydride / benzene / 36 h / Heating
2.2: 33 percent / aq. KF / benzene / 24 h
View Scheme
1-cyclopropyl-3-phenyl-1-propanol
52121-67-2

1-cyclopropyl-3-phenyl-1-propanol

1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: cetyltrimethylammonium bromide; aq. NaOH / CH2Cl2 / 1.5 h / 20 °C
1.2: 23 percent / toluene; CH2Cl2 / 60 h / 20 °C
2.1: tributyltin hydride; AINB / benzene / 4 h / Heating
2.2: 0.24 g / I2 / CH2Cl2 / 12 h / 20 °C
3.1: AIBN; tributyltin hydride / benzene / 36 h / Heating
3.2: 33 percent / aq. KF / benzene / 24 h
View Scheme
3-Phenylpropionic acid
501-52-0

3-Phenylpropionic acid

1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: SOCl2; DMF / ethyl acetate
2.1: CuI / diethyl ether / -40 °C
2.2: diethyl ether / -78 °C
View Scheme
1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

1-phenyl-3-hexanol
2180-43-0

1-phenyl-3-hexanol

Conditions
ConditionsYield
With dicarbonyl-(2,4-bis(trimethylsilyl)bicyclo[3.3.0]nona-1,4-dien-3-one)[acetonitrile]iron; isopropyl alcohol at 80℃; for 18h; Inert atmosphere;98%
With diethyl ether; sodium inactive propyl-β-phenethyl-carbinol;
chloro-trimethyl-silane
75-77-4

chloro-trimethyl-silane

1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

bromoacetic acid methyl ester
96-32-2

bromoacetic acid methyl ester

3-trimethylsilyloxy-3-(2'-phenylethyl)caproic acid methyl ester
672284-81-0

3-trimethylsilyloxy-3-(2'-phenylethyl)caproic acid methyl ester

Conditions
ConditionsYield
Stage #1: chloro-trimethyl-silane With zinc In ethyl acetate at 20 - 50℃; for 0.25h;
Stage #2: 1-phenylhexan-3-one; bromoacetic acid methyl ester In ethyl acetate at 55 - 60℃; for 0.25h; Reformatsky Reaction;
Stage #3: chloro-trimethyl-silane With piperazine Product distribution / selectivity; more than 3 stages;
95%
Stage #1: chloro-trimethyl-silane With zinc In tetrahydrofuran at 20 - 50℃; for 0.25h;
Stage #2: 1-phenylhexan-3-one; bromoacetic acid methyl ester In tetrahydrofuran at 50℃; for 0.25h; Reformatsky Reaction;
Stage #3: chloro-trimethyl-silane With N,N,N,N,-tetramethylethylenediamine Product distribution / selectivity; more than 3 stages;
92%
Stage #1: chloro-trimethyl-silane With zinc In tetrahydrofuran at 20 - 50℃; for 0.25h;
Stage #2: 1-phenylhexan-3-one; bromoacetic acid methyl ester In tetrahydrofuran at 50℃; for 0.25h; Reformatsky Reaction;
Stage #3: chloro-trimethyl-silane With piperazine Product distribution / selectivity; more than 3 stages;
91%
1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

acetylenemagnesium bromide
4301-14-8

acetylenemagnesium bromide

3-phenethylhex-1-yn-3-ol

3-phenethylhex-1-yn-3-ol

Conditions
ConditionsYield
In tetrahydrofuran at 0℃; for 2h; Inert atmosphere;91%
1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

methanesulfonyl chloride
124-63-0

methanesulfonyl chloride

1-phenylhexan-3-yl methanesulfonate

1-phenylhexan-3-yl methanesulfonate

Conditions
ConditionsYield
Stage #1: 1-phenylhexan-3-one With sodium tetrahydroborate; ethanol at 20℃; for 3h; Inert atmosphere;
Stage #2: methanesulfonyl chloride With triethylamine In dichloromethane at 20℃; for 15h; Inert atmosphere;
77%
1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

diazomethyl-trimethyl-silane
18107-18-1

diazomethyl-trimethyl-silane

C17H26Si
1266614-65-6

C17H26Si

Conditions
ConditionsYield
Stage #1: diazomethyl-trimethyl-silane With n-butyllithium In tetrahydrofuran; diethyl ether; hexane at -78℃; for 0.5h; Inert atmosphere;
Stage #2: 1-phenylhexan-3-one In tetrahydrofuran; diethyl ether; hexane at -78 - 20℃; for 4h; Inert atmosphere; regioselective reaction;
76%
1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

acetone
67-64-1

acetone

C15H22O2
1189366-32-2

C15H22O2

Conditions
ConditionsYield
With lithium diisopropyl amide at -78℃; for 5h;70%
1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

ethyl acetoacetate
141-97-9

ethyl acetoacetate

5,6-dihydro-4-hydroxy-6-phenethyl-6-propyl-2H-pyran-2-one
162174-87-0

5,6-dihydro-4-hydroxy-6-phenethyl-6-propyl-2H-pyran-2-one

Conditions
ConditionsYield
Multistep reaction;48%
malonic acid
141-82-2

malonic acid

1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

2-phenethyl-2-propyl-[1,3]dioxane-4,6-dione
328237-98-5

2-phenethyl-2-propyl-[1,3]dioxane-4,6-dione

Conditions
ConditionsYield
With sulfuric acid; acetic anhydride32%
1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

hexylbenzene
1077-16-3

hexylbenzene

Conditions
ConditionsYield
With hydrogenchloride; amalgamated zinc
1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

1-phenyl-hexan-3-one semicarbazone
16769-44-1

1-phenyl-hexan-3-one semicarbazone

1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

1-phenyl-hexan-3-one oxime

1-phenyl-hexan-3-one oxime

1-phenylhexan-3-one
29898-25-7

1-phenylhexan-3-one

ethyl 2-cyanoacetate
105-56-6

ethyl 2-cyanoacetate

2-cyano-3-phenethyl-hex-2-enoic acid ethyl ester
101582-27-8

2-cyano-3-phenethyl-hex-2-enoic acid ethyl ester

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