Items Standard Result Assay (Ursolic acid) 98%min 98.22% ----------------------------------------------------------------
Cas:312753-06-3
Min.Order:1 Gram
FOB Price: $100.0 / 500.0
Type:Trading Company
inquiryIndacaterol[CAS:312753-06-3] 8-Benzyloxy-5-(2-bromoacetyl)-2-Hydroxyquinoline[CAS:100331-89-3] 5,6-Diethyl-2-Amino Indane[CAS:312753-70-1] 5,6 -Diethyl-2-Amino Indane HCl Salt[CAS:312753-53-0] HANGZHOU THINK CHEMICAL CO., LTD. (TH
Cas:312753-06-3
Min.Order:1 Kilogram
Negotiable
Type:Other
inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:312753-06-3
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiryShanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu
Cas:312753-06-3
Min.Order:1 Kilogram
FOB Price: $1.0
Type:Manufacturers
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
We are leading fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Orga
Cas:312753-06-3
Min.Order:1 Kilogram
FOB Price: $5.0
Type:Lab/Research institutions
inquiryIndacaterol CAS: 312753-06-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediat
Cas:312753-06-3
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:312753-06-3
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
Cas:312753-06-3
Min.Order:1 Kilogram
FOB Price: $9.0 / 99.0
Type:Trading Company
inquiry1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s
Cas:312753-06-3
Min.Order:1 Kilogram
FOB Price: $60.0 / 100.0
Type:Lab/Research institutions
inquiryAppearance:white crystalline powder Storage:Room temperature, tight from air Package:packaged in foil bags or tins Application:312753-06-3 Transportation: By Express,by air, by sea Port:Qingdao,China
Cas:312753-06-3
Min.Order:10 Gram
FOB Price: $1.0 / 10.0
Type:Lab/Research institutions
inquiryOur company provides one-stop services of research - development - production for a variety of special prouducts. Not only do we make effective use of our strong technological strength, but also establish of cooperative relations with several well-
Cas:312753-06-3
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
Cas:312753-06-3
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:312753-06-3
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:312753-06-3
Min.Order:1 Gram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:312753-06-3
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryProduct name: Indacaterol CAS No.:312753-06-3 Molecule Formula:C24H28N2O3 Molecule Weight:392.49 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS SP
Cas:312753-06-3
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiry5-Bromo-8-nitroisoquinoline Cas NO. 63927-23-1 High quality with competitive price Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established
Cas:312753-06-3
Min.Order:1 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:312753-06-3
Min.Order:1 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryGMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:312753-06-3
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:312753-06-3
Min.Order:1 Metric Ton
FOB Price: $1.5
Type:Trading Company
inquiryHigh quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:Active Pharmaceutical I
Superior quality, moderate price & quick delivery. Appearance:white powder Storage:stored in a cool, dry and ventilated place to provent sun and rain Package:25kg/drum, or as per your request. Application:Used for active pharmaceutical ingr
We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
Cas:312753-06-3
Min.Order:1 Metric Ton
FOB Price: $1.0
Type:Trading Company
inquiryhigh purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier
high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
GMP factory Packing with pallet as buyer's special request Best service after shipment with e-mail Cargos together with container sales seervice available Api, inhibitor, and fine chemicals for more
Cas:312753-06-3
Min.Order:0 Metric Ton
Negotiable
Type:Trading Company
inquiryHigh qualityAppearance:White powder Storage:Room temperature Package:Aluminum bag Application:Used in producing API Transportation:By air Port:Beijing
indacaterol
Conditions | Yield |
---|---|
With lithium hydroxide monohydrate In methanol at 35℃; for 1h; Reagent/catalyst; | 99.84% |
(R)-8-(benzyloxy)-5-[2-[(5,6-diethyl-2,3-dihydro-1H-indole-2-yl)amino]-1-hydroxyethyl]quinolin-2(1H)-one
indacaterol
Conditions | Yield |
---|---|
Stage #1: (R)-8-(benzyloxy)-5-[2-[(5,6-diethyl-2,3-dihydro-1H-indole-2-yl)amino]-1-hydroxyethyl]quinolin-2(1H)-one With 5%-palladium/activated carbon; hydrogen In ethanol at 20℃; for 2h; Stage #2: With 5%-palladium/activated carbon; hydrogen In ethanol at 40℃; under 757.576 Torr; for 4h; | 97% |
With 5%-palladium/activated carbon; hydrogen; acetic acid In methanol at 20℃; | 85% |
With palladium 10% on activated carbon; hydrogen In methanol at 19 - 22℃; for 1h; Inert atmosphere; | 83% |
indacaterol
Conditions | Yield |
---|---|
With 5%-palladium/activated carbon; hydrogen; acetic acid In methanol at 20℃; | 86.2% |
With palladium 10% on activated carbon; hydrogen; acetic acid at 40℃; under 15201 Torr; Pressure; Reagent/catalyst; Temperature; |
indacaterol
Conditions | Yield |
---|---|
With palladium on activated charcoal; hydrogen; acetic acid In methanol at 25 - 30℃; under 2250.23 - 3000.3 Torr; for 4h; | 85.5% |
indacaterol
Conditions | Yield |
---|---|
With 5%-palladium/activated carbon; hydrogen; acetic acid; tetra-n-butylammoniumfluoride trihydrate In methanol at 20℃; | 84.5% |
indacaterol
Conditions | Yield |
---|---|
With 5%-palladium/activated carbon; hydrogen; acetic acid; tetra-n-butylammoniumfluoride trihydrate In methanol at 20℃; | 83.7% |
8-(phenylmethoxy)-5-[(R)-2-(5,6-diethyl-indan-2-ylamino)-1-hydroxy-ethyl]-(1H)-quinolin-2-one tartrate
indacaterol
Conditions | Yield |
---|---|
With 5%-palladium/activated carbon; hydrogen In methanol under 225.023 Torr; Inert atmosphere; | 77% |
With 5%-palladium/activated carbon; hydrogen In methanol under 225.023 Torr; Inert atmosphere; | 77% |
indacaterol
Conditions | Yield |
---|---|
With triethylamine In ethanol; hexane at 25℃; Resolution of racemate; | 49% |
indacaterol
Conditions | Yield |
---|---|
With hydrogen; 5%-palladium/activated carbon In acetic acid for 2 - 8h; | |
With hydrogen; 5%-palladium/activated carbon In acetic acid for 2 - 8h; |
5,6-diethyl-2,3-dihydro-1H-inden-2-amine
indacaterol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: toluene-4-sulfonic acid; -butyl vinyl ether / tetrahydrofuran; toluene / 0.5 h / 20 - 25 °C / Molecular sieve 1.2: 100 °C 2.1: 5%-palladium/activated carbon; hydrogen / methanol / 225.02 Torr / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1.1: tetrahydrofuran / 1 h / 20 °C 1.2: 16 h / 0 - 20 °C 2.1: Chiralcel AS-V / aq. phosphate buffer; acetonitrile / 25 °C / Resolution of racemate 3.1: 5%-palladium/activated carbon; hydrogen / ethanol / 2 h / 20 °C 3.2: 4 h / 40 °C / 757.58 Torr View Scheme | |
Multi-step reaction with 3 steps 1.1: tetrahydrofuran / 1 h / 20 °C 1.2: 16 h / 0 - 20 °C 2.1: 5%-palladium/activated carbon; hydrogen / ethanol / 8 h / 20 - 40 °C / 757.58 Torr 3.1: triethylamine / ethanol; hexane / 25 °C / Resolution of racemate View Scheme | |
Multi-step reaction with 4 steps 1: sodium cyanoborohydride / ethanol / 4 h / -25 - 80 °C / Inert atmosphere 2: sodium carbonate; potassium iodide / acetonitrile / 24 h / -25 - 80 °C 3: (-)-diisopinocamphenylborane chloride / dichloromethane; tetrahydrofuran / 25 h / 10 - 20 °C 4: hydrogen; acetic acid; palladium 10% on activated carbon / 40 °C / 15201 Torr View Scheme | |
Multi-step reaction with 4 steps 1: butan-1-ol / 3 h / 100 - 110 °C 2: (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran / 0 - 3 °C / Inert atmosphere 3: potassium carbonate / water; methanol / 1 h 4: acetic acid; palladium 10% on activated carbon; hydrogen / methanol / 6 h / 0 - 8 °C / 750.08 - 1500.15 Torr / Inert atmosphere View Scheme |
8-(benzyloxy)-5-[(1R)-2-bromo-1-hydroxyethyl]quinolin-2(1H)-one
indacaterol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: toluene-4-sulfonic acid; -butyl vinyl ether / tetrahydrofuran; toluene / 0.5 h / 20 - 25 °C / Molecular sieve 1.2: 100 °C 2.1: 5%-palladium/activated carbon; hydrogen / methanol / 225.02 Torr / Inert atmosphere View Scheme | |
Multi-step reaction with 4 steps 1.1: 1H-imidazole / chloroform / 10 h / 25 °C / Reflux 2.1: 1-methyl-pyrrolidin-2-one / 12 h / 95 - 100 °C 3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 50 - 55 °C 3.2: 1 h / 25 - 30 °C 4.1: acetic acid; palladium on activated charcoal; hydrogen / methanol / 4 h / 25 - 30 °C / 2250.23 - 3000.3 Torr View Scheme | |
Multi-step reaction with 4 steps 1.1: N-ethyl-N,N-diisopropylamine; sodium iodide / N,N-dimethyl-formamide / 90 °C 2.1: hydrazine hydrate / ethanol / 6 h / Reflux 2.2: 80 °C 3.1: N-ethyl-N,N-diisopropylamine; sodium iodide / N,N-dimethyl-formamide / 20 - 90 °C 4.1: acetic acid; 5%-palladium/activated carbon; hydrogen / methanol View Scheme |
5-(2,2-Dihydroxyacetyl)-8-(benzyloxy)-carbostyril
indacaterol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: tetrahydrofuran / 1 h / 20 °C 1.2: 16 h / 0 - 20 °C 2.1: Chiralcel AS-V / aq. phosphate buffer; acetonitrile / 25 °C / Resolution of racemate 3.1: 5%-palladium/activated carbon; hydrogen / ethanol / 2 h / 20 °C 3.2: 4 h / 40 °C / 757.58 Torr View Scheme | |
Multi-step reaction with 3 steps 1.1: tetrahydrofuran / 1 h / 20 °C 1.2: 16 h / 0 - 20 °C 2.1: 5%-palladium/activated carbon; hydrogen / ethanol / 8 h / 20 - 40 °C / 757.58 Torr 3.1: triethylamine / ethanol; hexane / 25 °C / Resolution of racemate View Scheme |
indacaterol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 5%-palladium/activated carbon; hydrogen / ethanol / 8 h / 20 - 40 °C / 757.58 Torr 2: triethylamine / ethanol; hexane / 25 °C / Resolution of racemate View Scheme |
8-benzyloxy-5-(2-bromoacetyl)-1H-quinolin-2-one
indacaterol
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; dimethylsulfide borane complex / tetrahydrofuran / 0 - 30 °C / Inert atmosphere 1.2: 0 - 30 °C 2.1: 1H-imidazole / chloroform / 10 h / 25 °C / Reflux 3.1: 1-methyl-pyrrolidin-2-one / 12 h / 95 - 100 °C 4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 50 - 55 °C 4.2: 1 h / 25 - 30 °C 5.1: acetic acid; palladium on activated charcoal; hydrogen / methanol / 4 h / 25 - 30 °C / 2250.23 - 3000.3 Torr View Scheme | |
Multi-step reaction with 5 steps 1.1: potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 20 °C 1.2: 1.33 h / 50 °C 2.1: (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; borane N,N-diethylaniline complex / dichloromethane; toluene; tetrahydrofuran / 2 h / -10 °C 3.1: hydrazine hydrate / ethanol / 6 h / Reflux 3.2: 80 °C 4.1: N-ethyl-N,N-diisopropylamine; sodium iodide / N,N-dimethyl-formamide / 20 - 90 °C 5.1: acetic acid; 5%-palladium/activated carbon; hydrogen / methanol View Scheme |
(R)-8-(benzyloxy)-5-(2-bromo-1-((tert-butyldimethylsilyl)oxy)ethyl)quinolin-2(1H)-one
indacaterol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: 1-methyl-pyrrolidin-2-one / 12 h / 95 - 100 °C 2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 50 - 55 °C 2.2: 1 h / 25 - 30 °C 3.1: acetic acid; palladium on activated charcoal; hydrogen / methanol / 4 h / 25 - 30 °C / 2250.23 - 3000.3 Torr View Scheme |
indacaterol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 50 - 55 °C 1.2: 1 h / 25 - 30 °C 2.1: acetic acid; palladium on activated charcoal; hydrogen / methanol / 4 h / 25 - 30 °C / 2250.23 - 3000.3 Torr View Scheme |
N-benzyl-5,6-diethyl-2,3-dihydro-1H-inden-2-amine
indacaterol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: sodium carbonate; potassium iodide / acetonitrile / 24 h / -25 - 80 °C 2: (-)-diisopinocamphenylborane chloride / dichloromethane; tetrahydrofuran / 25 h / 10 - 20 °C 3: hydrogen; acetic acid; palladium 10% on activated carbon / 40 °C / 15201 Torr View Scheme | |
Multi-step reaction with 2 steps 1: triethylamine; sodium iodide / N,N-dimethyl-formamide / 3 h / 20 °C 2: acetic acid; 5%-palladium/activated carbon; hydrogen; tetra-n-butylammoniumfluoride trihydrate / methanol / 20 °C View Scheme |
indacaterol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: (-)-diisopinocamphenylborane chloride / dichloromethane; tetrahydrofuran / 25 h / 10 - 20 °C 2: hydrogen; acetic acid; palladium 10% on activated carbon / 40 °C / 15201 Torr View Scheme |
8-(benzyloxy)-5-[(1R)-2-bromo-1-hydroxyethyl]quinolin-2(1H)-one
5,6-diethyl-2,3-dihydro-1H-inden-2-amine
indacaterol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: triethylamine; sodium iodide / N,N-dimethyl-formamide / 3 h / 20 °C 2: acetic acid; 5%-palladium/activated carbon; hydrogen / methanol / 20 °C View Scheme |
8-(benzyloxy)-5-[(1R)-2-bromo-1-hydroxyethyl]quinolin-2(1H)-one
N-benzyl-5,6-diethyl-2,3-dihydro-1H-inden-2-amine
indacaterol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: triethylamine; sodium iodide / N,N-dimethyl-formamide / 3 h / 20 °C 2: acetic acid; 5%-palladium/activated carbon; hydrogen / methanol / 20 °C View Scheme |
indacaterol
indacaterol
indacaterol
indacaterol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: N-ethyl-N,N-diisopropylamine; sodium iodide / N,N-dimethyl-formamide / 20 - 90 °C 2: acetic acid; 5%-palladium/activated carbon; hydrogen / methanol View Scheme |
indacaterol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; borane N,N-diethylaniline complex / dichloromethane; toluene; tetrahydrofuran / 2 h / -10 °C 2.1: hydrazine hydrate / ethanol / 6 h / Reflux 2.2: 80 °C 3.1: N-ethyl-N,N-diisopropylamine; sodium iodide / N,N-dimethyl-formamide / 20 - 90 °C 4.1: acetic acid; 5%-palladium/activated carbon; hydrogen / methanol View Scheme |
5-(R)-(2-amino-1-hydroxy-ethyl)-8-phenylmethoxy-(1H)-quinolin-2-one
indacaterol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: N-ethyl-N,N-diisopropylamine; sodium iodide / N,N-dimethyl-formamide / 20 - 90 °C 2: acetic acid; 5%-palladium/activated carbon; hydrogen / methanol View Scheme |
indacaterol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: hydrazine hydrate / ethanol / 6 h / Reflux 1.2: 80 °C 2.1: N-ethyl-N,N-diisopropylamine; sodium iodide / N,N-dimethyl-formamide / 20 - 90 °C 3.1: acetic acid; 5%-palladium/activated carbon; hydrogen / methanol View Scheme |
5-acetyl-8-hydroxy-2(1H)-quinolinone
indacaterol
Conditions | Yield |
---|---|
Multi-step reaction with 7 steps 1.1: potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 20 °C 1.2: 2.5 h / 20 °C 2.1: boron trifluoride diethyl etherate / dichloromethane / 0.17 h / 0 °C 2.2: 2.75 h / Reflux 3.1: potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 20 °C 3.2: 1.33 h / 50 °C 4.1: (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; borane N,N-diethylaniline complex / dichloromethane; toluene; tetrahydrofuran / 2 h / -10 °C 5.1: hydrazine hydrate / ethanol / 6 h / Reflux 5.2: 80 °C 6.1: N-ethyl-N,N-diisopropylamine; sodium iodide / N,N-dimethyl-formamide / 20 - 90 °C 7.1: acetic acid; 5%-palladium/activated carbon; hydrogen / methanol View Scheme |
5-acetyl-8-benzyloxy-1H-quinolin-2-one
indacaterol
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1.1: boron trifluoride diethyl etherate / dichloromethane / 0.17 h / 0 °C 1.2: 2.75 h / Reflux 2.1: potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 20 °C 2.2: 1.33 h / 50 °C 3.1: (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; borane N,N-diethylaniline complex / dichloromethane; toluene; tetrahydrofuran / 2 h / -10 °C 4.1: hydrazine hydrate / ethanol / 6 h / Reflux 4.2: 80 °C 5.1: N-ethyl-N,N-diisopropylamine; sodium iodide / N,N-dimethyl-formamide / 20 - 90 °C 6.1: acetic acid; 5%-palladium/activated carbon; hydrogen / methanol View Scheme |
indacaterol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: potassium carbonate / water; methanol / 1 h 2: acetic acid; palladium 10% on activated carbon; hydrogen / methanol / 6 h / 0 - 8 °C / 750.08 - 1500.15 Torr / Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
In isopropyl alcohol at 20 - 80℃; for 18.0833h; | 96.3% |
Conditions | Yield |
---|---|
In butan-1-ol at 20 - 80℃; for 18.25h; | 95.28% |
Conditions | Yield |
---|---|
In ethyl acetate at 20 - 60℃; | 94.8% |
Conditions | Yield |
---|---|
In dichloromethane; ethyl acetate; isopropyl alcohol at 5 - 35℃; for 11h; Temperature; Solvent; | 93.73% |
In isopropyl alcohol at 20 - 80℃; for 17h; | 84.9% |
Conditions | Yield |
---|---|
In isopropyl alcohol for 1h; Reflux; | 92.5% |
In ethanol at 60℃; for 0.166667h; | 83% |
In ethanol at 50 - 60℃; |
Conditions | Yield |
---|---|
In water at 20 - 70℃; for 20.2h; | 86.9% |
indacaterol
Conditions | Yield |
---|---|
With sulfuric acid; acetic acid at 20 - 50℃; for 18.0833h; | 86.9% |
indacaterol
(2E)-but-2-enedioic acid
Conditions | Yield |
---|---|
In methanol at 20 - 50℃; for 3.33333h; | 86.4% |
indacaterol
L-Tartaric acid
Conditions | Yield |
---|---|
In isopropyl alcohol at 50℃; for 15h; | 84.27% |
indacaterol
Conditions | Yield |
---|---|
With hydrogenchloride In methanol at 20 - 50℃; for 17h; | 84.27% |
indacaterol
Conditions | Yield |
---|---|
With hydrogen bromide In methanol at 20 - 50℃; for 3.25h; | 84.27% |
Conditions | Yield |
---|---|
In methanol at 25 - 50℃; for 15h; | 79.37% |
indacaterol
1-hydroxy-2-naphthoic acid
Conditions | Yield |
---|---|
In butan-1-ol at 20 - 100℃; for 17h; | 76% |
indacaterol
Hippuric Acid
Conditions | Yield |
---|---|
In methanol at 20 - 50℃; for 4.16667h; | 75.7% |
indacaterol
glycolic Acid
Conditions | Yield |
---|---|
In methanol at 20 - 50℃; | 71.37% |
indacaterol
ethanesulfonic acid
Conditions | Yield |
---|---|
In water; dimethyl sulfoxide at 20 - 50℃; |
indacaterol
Conditions | Yield |
---|---|
With bromine In acetic acid at 20℃; for 1h; |
indacaterol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: bromine / acetic acid / 1 h / 20 °C 2: palladium 10% on activated carbon; tritium; triethylamine / 5 h / 20 °C View Scheme |
indacaterol
C24H30N2O3
Conditions | Yield |
---|---|
With 10% Pd/C; hydrogen at 25℃; under 760.051 Torr; for 360h; |
indacaterol
Conditions | Yield |
---|---|
With thionyl chloride In acetonitrile for 0.0833333h; Reflux; |
indacaterol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: thionyl chloride / acetonitrile / 0.08 h / Reflux 2.1: sodium tetrahydroborate / ethanol / 18 h / 25 °C 2.2: 2 h / Reflux View Scheme |
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