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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

6-Oxoheptanoic acid

Cas:3128-07-2

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 5-Acetylvaleric Acid supplier in China

Cas:3128-07-2

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 5-Acetylvaleric Acid

Cas:3128-07-2

Min.Order:1

Negotiable

Type:Other

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

5-Acetylvaleric acid

Cas:3128-07-2

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

LIDE PHARMACEUTICALS LIMITED

LIDE PHARMACEUTICALS LIMITED is a professional chemicals and APIs leading manufacturer in China. Our core business line covers APIs, Intermediates, Herb extract, etc.

5-ACETYLVALERIC ACID

Cas:3128-07-2

Min.Order:1 Kilogram

FOB Price: $0.9 / 1.0

Type:Lab/Research institutions

inquiry

Henan Tianfu Chemical Co., Ltd.

Product Name: 5-ACETYLVALERIC ACID Synonyms: 6-oxoheptanoate;6-Oxoheptanoic acid 98%;5-Acetylvaleric acid, 97%, 97%;5-Acetylpentanoic acid, 6-Oxoenanthic acid;5-Acetylvaleric acid, 90+%, technical;5-Acetylpentanoic acid;6-Ketoenanthic acid;5-Acety

5-ACETYLVALERIC ACID 3128-07-2

Cas:3128-07-2

Min.Order:1 Kilogram

FOB Price: $500.0

Type:Lab/Research institutions

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

5-ACETYLVALERIC ACID

Cas:3128-07-2

Min.Order:1 Kilogram

FOB Price: $1.0 / 10.0

Type:Trading Company

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Top Purity CAS 3128-07-2 with fast shipping

Cas:3128-07-2

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

inquiry

Shanghai Upbio Tech Co.,Ltd

1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ

Heptanoic acid, 6-oxo-

Cas:3128-07-2

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:3128-07-2

Cas:3128-07-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Fandachem Co.,Ltd

Hangzhou Fanda Chemical Co.,Ltd (FandaChem) , a China-based chemical company, specialize in exporting 5-Acetylvaleric acid CAS:3128-07-2, Please contact us by email freely. We are leading exporter in China. If you really need this car

5-Acetylvaleric acid CAS:3128-07-2 from fandachem

Cas:3128-07-2

Min.Order:0 Metric Ton

Negotiable

Type:Other

inquiry

Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

5-Acetylvaleric Acid

Cas:3128-07-2

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Heptanoic acid, 6-oxo-

Cas:3128-07-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

5-ACETYLVALERIC ACID

Cas:3128-07-2

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

Heptanoic acid, 6-oxo-

Cas:3128-07-2

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

GIHI CHEMICALS CO.,LIMITED

Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

5-Acetylvaleric acid

Cas:3128-07-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

5-Acetylvaleric acid

Cas:3128-07-2

Min.Order:0

Negotiable

Type:Other

inquiry

Lonwin Chemical Group Limited

Shanghai Lonwin Chemical company is a subsidiary of Lonwin Industry Group Limited, was established in 2011 and is headquartered in Shanghai, adjacent to China National Convention and Exhibition Center and Hongqiao transportation hub.Lonwinchem is

Best price 5-Acetylvaleric Acid 3128-07-2

Cas:3128-07-2

Min.Order:100 Kilogram

FOB Price: $100.0 / 150.0

Type:Other

inquiry

JINHUA HUAYI CHEMICAL CO., LTD.

Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands

5-Acetylvaleric Acid

Cas:3128-07-2

Min.Order:100 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Aecochem Corp.

Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS

5-Acetylvaleric Acid

Cas:3128-07-2

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hubei Taiho Chemical Co.,LTD

TAIHO Unique Advantages:1.We're factory2.Free samples available3.Commodity inspection can be done4.ISO9001,Kosher certifications5.10 years experiences Storage:Store in cool &dry place Package:aluminium foil bag/fiber can/plastic drum Application:comp

5-Acetylvaleric acid

Cas:3128-07-2

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Xiamen AmoyChem Co.,Ltd

Amoychem is committed to providing the top-quality chemical products and services Internationally. We offer our customers with friendly, professional service and reliable, high performance products that have been manufactured according to the accredi

5-Acetylvaleric acid

Cas:3128-07-2

Min.Order:0

Negotiable

Type:Other

inquiry

Antimex Chemical Limied

factory?direct?sale Application:Fine chemical intermediates, used as the main raw material for the synthesis of various pesticides, medicines, surfactants, polymer monomers, and antifungal agents

Heptanoic acid, 6-oxo-

Cas:3128-07-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

SAGECHEM LIMITED

3128-07-2 Application:intermediate

6-oxo-heptanoic acid

Cas:3128-07-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hunan Russell Chemicals Technology Co.,Ltd

low price and high purityAppearance:solid or liquid Storage:in sealed air resistant place Package:As customer require Application:Pharma;Industry;Agricultural Transportation:by sea or by airplane Port:any port in China

5-Acetylvaleric acid, 96% 3128-07-2

Cas:3128-07-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Shanghai Yuanye Bio-Technology Co., Ltd.

good quality, competitive price, thoughtful after sale serviceAppearance:white powder Storage:Keep it in dry,shady and cool place Package:1g Application:Pharma;Industry;Agricultural;chemical reaserch Transportation:by express or by sea Port:Any port

5-Acetylvaleric Acid

Cas:3128-07-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

5-ACETYLVALERIC ACID

Cas:3128-07-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

LEAP CHEM Co., Ltd.

Best Seller, High Quality, Competitive Price, Fast Delivery, Quick ResponseAppearance:powder, or liquid Storage:Stored in room temperature, ventilated place Package:Bottle, barrel, cargo, container, etc. Application:Pharmaceuticals, intermediates, AP

5-ACETYLVALERIC ACID

Cas:3128-07-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Bide Pharmatech Ltd

Our mission is to provide high-quality and innovative products to our customers. By offering a broad range of products, custom synthesis and personalized services, Bide can help scientists speeding up their research in the chemical and pharmaceutical

5-Acetylvaleric acid

Cas:3128-07-2

Min.Order:0

Negotiable

Type:Other

inquiry

Amadis Chemical Co., Ltd.

1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G

6-oxoheptanoate

Cas:3128-07-2

Min.Order:10 Milligram

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

2-acetylcyclopentanaone
1670-46-8

2-acetylcyclopentanaone

6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

Conditions
ConditionsYield
With tropylium tetrafluoroborate; water In neat (no solvent) at 100℃; for 16h; Solvent; Temperature; Reagent/catalyst; Claisen Condensation; Inert atmosphere;99%
With iron(III) chloride; water at 80℃; for 16h; Neat (no solvent);95%
With indium(III) triflate; 2,6-di-tert-butyl-pyridine; water at 80℃; for 24h; Neat (no solvent); Inert atmosphere;94%
2-Methylcyclohexanone
583-60-8

2-Methylcyclohexanone

6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

Conditions
ConditionsYield
With oxygen; acetic acid In water at 60℃; under 750.075 Torr; for 8h;98%
With oxygen; H7*10H2O In water at 60℃; under 750.06 Torr; for 8h;97%
With oxygen; H6[PMo9V3O40]*11H2O In methanol at 60℃; under 750.06 Torr; for 24h; Product distribution; Kinetics; Further Variations:; Catalysts; Reagents; Solvents; Temperatures; reaction times;97%
1-methylcyclohex-1-ene
591-49-1

1-methylcyclohex-1-ene

6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

Conditions
ConditionsYield
With dihydrogen peroxide; 12-tungstophosphoric acid/Al/C In tert-butyl alcohol at 60℃; for 24h;96%
With tris(cetylpyridinium) 12-tungstophosphate; dihydrogen peroxide In tert-butyl alcohol for 24h; Heating;90%
With tert.-butylhydroperoxide; indium(III) chloride In water at 90℃; for 8.2h;84%
1-methyl-1,2-cyclohexanediol
6296-84-0

1-methyl-1,2-cyclohexanediol

6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

Conditions
ConditionsYield
With tris(cetylpyridinium) 12-tungstophosphate; dihydrogen peroxide In tert-butyl alcohol for 24h; Heating;95%
With potassium permanganate; acetone at 0℃;
With dihydrogen peroxide In water; tert-butyl alcohol at 80℃; for 24h;91 %Chromat.
Conditions
ConditionsYield
With hydrogenchloride; sodium tungstate; phosphoric acid; dihydrogen peroxide at 90℃; for 5h;93%
With hydrogenchloride; sodium tungstate; phosphoric acid; dihydrogen peroxide at 90℃; for 5h; other 1,2-diols, other catalysts;93%
With potassium carbonate at 20℃; for 3.3h; electrolysis: nickel(III) oxide hydroxide electrode, 0.3 A;70%
hept-6-ynoic acid
30964-00-2

hept-6-ynoic acid

6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

Conditions
ConditionsYield
With [RhCl2(p-cymene)]2; water at 20℃; for 12h;88%
With platinum catalyst In water at 37℃; for 96h;58%
C15H20O5

C15H20O5

6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

Conditions
ConditionsYield
With iron(III) chloride In dichloromethane at 20℃; for 0.0833333h; Inert atmosphere; Green chemistry;75%
1-trimethylsilyloxy-2-methyl-1-cyclohexene
19980-35-9

1-trimethylsilyloxy-2-methyl-1-cyclohexene

A

6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

B

2-hydroxy-2-methylcyclohexanone
96304-02-8, 96304-40-4, 144178-58-5, 3476-78-6

2-hydroxy-2-methylcyclohexanone

Conditions
ConditionsYield
With tert.-butylhydroperoxide; titanium silicate for 24h; Heating;A 73%
B 6%
methyl cyclohexane
82166-21-0

methyl cyclohexane

A

6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

B

1-Methylcyclohexanol
590-67-0

1-Methylcyclohexanol

Conditions
ConditionsYield
With ozone In neat (no solvent) at 20℃; for 5h; UV-irradiation;A 70%
B 10%
1,2-epoxy-1-methylcyclohexane
1713-33-3

1,2-epoxy-1-methylcyclohexane

6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

Conditions
ConditionsYield
With dodecyltrimethylammonium phosphotungstate; water; dihydrogen peroxide In toluene at 80℃; for 12h; chemoselective reaction;69%
With dihydrogen peroxide In water; tert-butyl alcohol at 80℃; for 24h;
Conditions
ConditionsYield
With tert.-butylhydroperoxide; bis(acetylacetonato)dioxidomolybdenum(VI) In chlorobenzene at 60℃; for 24h;62%
percarbonate de O,O-tert-butyle et O-isopropyle
65700-06-3

percarbonate de O,O-tert-butyle et O-isopropyle

butyric acid
107-92-6

butyric acid

6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

Conditions
ConditionsYield
at 130℃; for 2.5h;54%
2-Methylcyclohexanol
583-59-5

2-Methylcyclohexanol

A

6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

B

2-methylhexane-1,6-dioic acid
626-70-0

2-methylhexane-1,6-dioic acid

Conditions
ConditionsYield
With oxygen; sodium nitrite In trifluoroacetic acid at 0 - 20℃; for 5h;A 52%
B 14%
2-Methylcyclohexanol
583-59-5

2-Methylcyclohexanol

6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

Conditions
ConditionsYield
With sulfuric acid24%
With chromium(VI) oxide; sulfuric acid at 30℃;
1-acetoxy-2-methylcyclohexene
1196-73-2

1-acetoxy-2-methylcyclohexene

A

6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

B

2-methyl-2-nitrocyclohexan-1-one
80594-87-2

2-methyl-2-nitrocyclohexan-1-one

Conditions
ConditionsYield
With nitric acid; acetic anhydride at 15 - 22℃; for 2h;A 17.3%
B 21%
(Z)-Cyclooctene
931-88-4, 931-87-3

(Z)-Cyclooctene

A

Adipic acid
124-04-9

Adipic acid

B

heptanedioic acid
111-16-0

heptanedioic acid

C

octane-1,8-dioic acid
505-48-6

octane-1,8-dioic acid

D

6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

Conditions
ConditionsYield
With dihydrogen peroxide; methyltrioctylammonium tetrakis(oxodiperoxotungsto)phos In water at 85℃; for 7h; Further byproducts given;A 7%
B 2.6%
C 24 % Chromat.
D 4%
1-methylcyclohex-1-ene
591-49-1

1-methylcyclohex-1-ene

A

1,5-pentanedioic acid
110-94-1

1,5-pentanedioic acid

B

Adipic acid
124-04-9

Adipic acid

C

6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

D

5-ketohexanoic acid
3128-06-1

5-ketohexanoic acid

Conditions
ConditionsYield
With dihydrogen peroxide; methyltrioctylammonium tetrakis(oxodiperoxotungsto)phos In water at 85℃; for 6h; Yield given; Further byproducts given;A 0.4%
B 0.3%
C n/a
D 0.5%
ethyl 6-chloro-6-oxohexanoate
1071-71-2

ethyl 6-chloro-6-oxohexanoate

sodium diethylmalonate
996-82-7

sodium diethylmalonate

6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

Conditions
ConditionsYield
With toluene Kochen des Reaktionsprodukts mit 20prozentig. HCl;
diethyl adipate
141-28-6

diethyl adipate

6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

1-ethynyl-2-methyl-cyclohexene
32591-08-5

1-ethynyl-2-methyl-cyclohexene

6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

Conditions
ConditionsYield
Ozonolyse;
ethylmagnesium bromide
925-90-6

ethylmagnesium bromide

2-ethoxycarbonyl-1-cyclopentanone
611-10-9

2-ethoxycarbonyl-1-cyclopentanone

6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

Conditions
ConditionsYield
With diethyl ether Erwaermen des Reaktionsgemisches mit Acetylchlorid und Erhitzen des Reaktionsprodukts mit wss. Natriumcarbonat-Loesung;
ethyl 2-propylacetoacetate
1540-28-9

ethyl 2-propylacetoacetate

6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

Conditions
ConditionsYield
Verseifung;
6-Acetoxy-heptadien-(3,5)-saeure-(1)
1571-01-3

6-Acetoxy-heptadien-(3,5)-saeure-(1)

6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

Conditions
ConditionsYield
(i) H2, Pd-C, (ii) KOH, MeOH, (iii) H2SO4, CrO3; Multistep reaction;
diethyl 2-acetylhexanedioate
90124-78-0

diethyl 2-acetylhexanedioate

6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

Conditions
ConditionsYield
With hydrogenchloride
carbon dioxide
124-38-9

carbon dioxide

2-(4-chlorobutyl)-2-methyl[1,3]dioxolane
57558-50-6

2-(4-chlorobutyl)-2-methyl[1,3]dioxolane

6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

Conditions
ConditionsYield
(i) Mg, THF, (ii) /BRN= 1900390/, Et2O, (iii) aq. HCl; Multistep reaction;
(E)-2-Diethylamino-7-oxo-oct-2-enenitrile
73185-97-4

(E)-2-Diethylamino-7-oxo-oct-2-enenitrile

6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

Conditions
ConditionsYield
With hydrogenchloride
1-Methyl-2-methylselanyl-cyclohexene
66030-48-6

1-Methyl-2-methylselanyl-cyclohexene

6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

Conditions
ConditionsYield
With dihydrogen peroxide In tetrahydrofuran
formic acid
64-18-6

formic acid

1-hexen-5-one
109-49-9

1-hexen-5-one

A

6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

B

α-methyl-δ-oxocaproic acid
54248-02-1

α-methyl-δ-oxocaproic acid

Conditions
ConditionsYield
With carbon monoxide; palladium on activated charcoal; 1,4-di(diphenylphosphino)-butane In 1,2-dimethoxyethane at 150℃; under 5168 Torr; for 24h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
1-methylcyclohex-1-ene
591-49-1

1-methylcyclohex-1-ene

A

1,5-pentanedioic acid
110-94-1

1,5-pentanedioic acid

B

6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

C

6-oxoheptanal
19480-04-7

6-oxoheptanal

D

n-hexan-2-one
591-78-6

n-hexan-2-one

E

5-ketohexanoic acid
3128-06-1

5-ketohexanoic acid

F

Glutaraldehyde
111-30-8

Glutaraldehyde

Conditions
ConditionsYield
With ozone at 30℃; Mechanism; Product distribution; multistep reaction;
2-methyl-2-decene
23381-92-2

2-methyl-2-decene

A

6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

B

2-hydroxy-2-methylcyclohexanone
96304-02-8, 96304-40-4, 144178-58-5, 3476-78-6

2-hydroxy-2-methylcyclohexanone

Conditions
ConditionsYield
With cobalt(II); oxygen; 2-Methylcyclohexanone
methanol
67-56-1

methanol

6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

methyl 6-oxoheptanoate
2046-21-1

methyl 6-oxoheptanoate

Conditions
ConditionsYield
iron(III) chloride100%
With sulfuric acid In 1,2-dichloro-ethane Fisher esterification;100%
With sulfuric acid In 1,2-dichloro-ethane for 12h; Heating;100%
6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

methyl iodide
74-88-4

methyl iodide

methyl 6-oxoheptanoate
2046-21-1

methyl 6-oxoheptanoate

Conditions
ConditionsYield
Stage #1: 6-oxoheptanoic acid With 1,8-diazabicyclo[5.4.0]undec-7-ene In acetone at 23℃; for 0.25h;
Stage #2: methyl iodide In acetone for 1h;
95%
6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

aniline
62-53-3

aniline

2-methyl-1-phenylazepane

2-methyl-1-phenylazepane

Conditions
ConditionsYield
With phenylsilane; C9H8FeN2O8S2 In neat (no solvent) at 100℃; for 20h; Schlenk technique; Inert atmosphere; Glovebox; Irradiation;92%
6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

isobutene
115-11-7

isobutene

tert-butyl 6-oxoheptanoate
116666-94-5

tert-butyl 6-oxoheptanoate

Conditions
ConditionsYield
In dichloromethane for 96h; Ambient temperature;90%
6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

(R)-2'-[3-(2-Methoxyethoxy)propoxy]-1,1'-binaphthalen-2-ol

(R)-2'-[3-(2-Methoxyethoxy)propoxy]-1,1'-binaphthalen-2-ol

6-oxo-heptanoic acid 2'-[3-(2-methoxy-ethoxy)-propoxy]-[1,1']binaphthalenyl-2-yl ester

6-oxo-heptanoic acid 2'-[3-(2-methoxy-ethoxy)-propoxy]-[1,1']binaphthalenyl-2-yl ester

Conditions
ConditionsYield
With 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide In dichloromethane90%
6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

4-methoxy-aniline
104-94-9

4-methoxy-aniline

2-methyl-1-(4-methoxyphenyl)azepane

2-methyl-1-(4-methoxyphenyl)azepane

Conditions
ConditionsYield
With phenylsilane; C9H8FeN2O8S2 In neat (no solvent) at 100℃; for 20h; Schlenk technique; Inert atmosphere; Glovebox; Irradiation;90%
6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

dicyclohexyl-carbodiimide
538-75-0

dicyclohexyl-carbodiimide

4-(tri-n-butylstannyl)-but-3-en-1-ol
107399-01-9, 212783-03-4, 107711-42-2

4-(tri-n-butylstannyl)-but-3-en-1-ol

4-(tri-n-butylstannyl)-3(E)-butenyl 6-oxoheptanoate
134311-32-3

4-(tri-n-butylstannyl)-3(E)-butenyl 6-oxoheptanoate

Conditions
ConditionsYield
In dichloromethane catalyst: (dimethylamino)pyridine, stirred at room temp. for 2 days; filtrated, concd., chromy. (silica gel, hexane/EtOAc), elem. anal.;89%
6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

p-toluidine
106-49-0

p-toluidine

6-oxoheptanoic acid p-methylanilide
83086-06-0

6-oxoheptanoic acid p-methylanilide

Conditions
ConditionsYield
With 4-methyl-morpholine; isobutyl chloroformate In tetrahydrofuran for 8h; Ambient temperature;87%
With dicyclohexyl-carbodiimide In tetrahydrofuran70%
6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

4-trifluoromethylphenylamine
455-14-1

4-trifluoromethylphenylamine

6-oxo-N-<4-(trifluoromethyl)phenyl>heptanamide
84417-40-3

6-oxo-N-<4-(trifluoromethyl)phenyl>heptanamide

Conditions
ConditionsYield
With 4-methyl-morpholine; isobutyl chloroformate In tetrahydrofuran86%
With 4-methyl-morpholine; isobutyl chloroformate 1.) THF, -15 deg C, 15 min, 2.) THF, RT, overnight; Yield given. Multistep reaction;
6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

heptane-1,6-diol
13175-27-4

heptane-1,6-diol

Conditions
ConditionsYield
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 20℃;85%
With lithium aluminium tetrahydride In tetrahydrofuran at 20℃; for 1h; Inert atmosphere;81%
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 25℃; Inert atmosphere;70%
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 20℃; Inert atmosphere; Schlenk technique;35%
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 20℃; Inert atmosphere;
6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

4-butoxy-benzoic acid N-(4-methoxy-phenyl)-hydrazide
764658-26-6

4-butoxy-benzoic acid N-(4-methoxy-phenyl)-hydrazide

4-[1-(4-butoxy-benzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]-butyric acid

4-[1-(4-butoxy-benzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]-butyric acid

Conditions
ConditionsYield
With acetic acid at 80℃; for 2h;84%
With acetic acid
6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

bis[(2-pyridyl)methyl]amine
1539-42-0

bis[(2-pyridyl)methyl]amine

6-oxo-N,N-bis(pyridin-2-ylmethyl)heptanamide

6-oxo-N,N-bis(pyridin-2-ylmethyl)heptanamide

Conditions
ConditionsYield
With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 0.166667h;84%
6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

Propargylamine
2450-71-7

Propargylamine

6-oxo-N-(prop-2-yn-1-yl)heptanamide
280577-92-6

6-oxo-N-(prop-2-yn-1-yl)heptanamide

Conditions
ConditionsYield
Stage #1: 6-oxoheptanoic acid With 4-methyl-morpholine; isobutyl chloroformate In tetrahydrofuran at 0℃; for 0.25h; Substitution;
Stage #2: Propargylamine In tetrahydrofuran at 20℃; for 0.5h; Substitution;
80%
With 4-methyl-morpholine In tetrahydrofuran at 0 - 20℃; for 0.5h;80%
Stage #1: 6-oxoheptanoic acid With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In dichloromethane for 0.0333333h;
Stage #2: With benzotriazol-1-ol In dichloromethane for 0.0333333h;
Stage #3: Propargylamine In dichloromethane at 20℃; for 16h;
52%
6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

2-Phenoxyethanol
122-99-6

2-Phenoxyethanol

2-phenoxyethyl 6-oxoheptanoate

2-phenoxyethyl 6-oxoheptanoate

Conditions
ConditionsYield
Stage #1: 6-oxoheptanoic acid With thionyl chloride In N,N-dimethyl-formamide at 30℃; for 1h;
Stage #2: 2-Phenoxyethanol In pentane at 20℃; for 1h;
80%
oxalyl dichloride
79-37-8

oxalyl dichloride

6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

6-oxoheptanoic acid chloride
56721-54-1

6-oxoheptanoic acid chloride

Conditions
ConditionsYield
In benzene at 50℃; for 1h;79.7%
6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

5-(3-methyl-3H-diazirin-3-yl)pentanoic acid
25080-63-1

5-(3-methyl-3H-diazirin-3-yl)pentanoic acid

Conditions
ConditionsYield
Stage #1: 6-oxoheptanoic acid With ammonia; hydroxylamine-O-sulfonic acid at -75 - 20℃; for 12h; Sealed tube;
Stage #2: With potassium tert-butylate at -75 - 20℃; for 2h; Sealed tube;
79%
Multi-step reaction with 2 steps
1: hydroxylamine-O-sulfonic acid / ammonia / 12 h / -78 - 20 °C / Sealed tube; liquid NH3
2: potassium hydroxide / ammonia / 2 h / -78 - 20 °C / Sealed tube; liquid NH3
View Scheme
6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

6-methyl-hept-6-enoic acid
5212-67-9

6-methyl-hept-6-enoic acid

Conditions
ConditionsYield
Stage #1: Methyltriphenylphosphonium bromide With n-butyllithium In hexanes; dimethyl sulfoxide at 0 - 20℃; for 1h; Wittig Reaction;
Stage #2: 6-oxoheptanoic acid With n-butyllithium In tetrahydrofuran; hexanes; dimethyl sulfoxide at 20℃; for 48h;
Stage #3: With hydrogenchloride; water more than 3 stages;
78%
6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

Methyltriphenylphosphonium bromide
1779-49-3

Methyltriphenylphosphonium bromide

6-methyl-hept-6-enoic acid
5212-67-9

6-methyl-hept-6-enoic acid

Conditions
ConditionsYield
Stage #1: Methyltriphenylphosphonium bromide With n-butyllithium In hexane; dimethyl sulfoxide at 20℃; for 1h;
Stage #2: 6-oxoheptanoic acid With n-butyllithium In tetrahydrofuran; hexane; dimethyl sulfoxide at 20℃; for 48h; Wittig olefination; Further stages.;
78%
Stage #1: Methyltriphenylphosphonium bromide With n-butyllithium In hexanes; dimethyl sulfoxide at 0 - 20℃; for 1h;
Stage #2: 6-oxoheptanoic acid In tetrahydrofuran; hexanes; dimethyl sulfoxide at 40℃; for 48h;
Stage #3: With hydrogenchloride; water In tetrahydrofuran; hexanes; dimethyl sulfoxide
78%
sodium cyanide
773837-37-9

sodium cyanide

6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

C16H24N4O4
1144115-64-9

C16H24N4O4

Conditions
ConditionsYield
Stage #1: sodium cyanide; 6-oxoheptanoic acid With sodium carbonate; hydrazinium sulfate In water for 44h;
Stage #2: With hydrogenchloride In water
Stage #3: With bromine In water for 1h;
78%
6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

ethanol
64-17-5

ethanol

2-bromophenylhydrazine hydrochloride
50709-33-6

2-bromophenylhydrazine hydrochloride

ethyl 4-(7-bromo-2-methyl-1H-indol-3-yl)butanoate
1232860-64-8

ethyl 4-(7-bromo-2-methyl-1H-indol-3-yl)butanoate

Conditions
ConditionsYield
With sulfuric acid at 100℃; for 1.5h; Fischer Indole Synthesis;76%
Stage #1: 6-oxoheptanoic acid; 2-bromophenylhydrazine hydrochloride In ethanol at 50℃; for 0.666667h;
Stage #2: ethanol With sulfuric acid for 16h; Reflux;
15 g
6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

acetone
67-64-1

acetone

2-oxopropyl 6-oxoheptanoate

2-oxopropyl 6-oxoheptanoate

Conditions
ConditionsYield
With tert.-butylhydroperoxide; tetrabutylammomium bromide In acetone at 120℃; under 33753.4 Torr; for 0.5h; Inert atmosphere; Microwave irradiation;75%
6-oxoheptanoic acid
3128-07-2

6-oxoheptanoic acid

2-cyano-6-hydroxybenzothiazole
939-69-5

2-cyano-6-hydroxybenzothiazole

2-cyanobenzo[d]thiazol-6-yl 6-oxoheptanoate

2-cyanobenzo[d]thiazol-6-yl 6-oxoheptanoate

Conditions
ConditionsYield
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane at 20℃; for 2h;74%

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