As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:317374-08-6
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Colorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on
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inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:317374-08-6
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:317374-08-6
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
Cas:317374-08-6
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the
Cas:317374-08-6
Min.Order:1 Kilogram
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inquiryProduct Name: 2-methyl-4-(2-methyl-benzoylamino)-benzoic acid CAS: 317374-08-6 MF: C16H15NO3 MW: 269.3 EINECS: 1312995-182-4 Mol File: Mol File 2-methyl-4-(2-methyl-benzoylamino)-benzoic acid Structure 2-methyl-4-(2-methyl-benzoy
Cas:317374-08-6
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiry2-methyl-4-(2-methyl-benzoylamino)-benzoic acid CAS:317374-08-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing
Cas:317374-08-6
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:317374-08-6
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Type:Lab/Research institutions
inquiryProduct Name: 2-methyl-4-(2-methyl-benzoylamino)-benzoic acid Synonyms: 4-(2-MethylbenzaMido)-2-Methyl-benzoic acid;2-Methyl-4-(2-methylbenzamido);2-methyl-4-(2-methyl-benzoylamino)-benzoic acid;2-methyl-4-(2-methyl-p-nitrobenzoic acid benzoyl p
Cas:317374-08-6
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:317374-08-6
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Type:Lab/Research institutions
inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Cas:317374-08-6
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Type:Manufacturers
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:317374-08-6
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:317374-08-6
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryHenan Tianfu Chemical Co., Ltd. is located in Zhengzhou High-tech Development Zone with import and export license. We passed ISO 9001:2008 in 2009, and won "High-tech Enterprise" by provincial government in 2013.The objective of the com
Cas:317374-08-6
Min.Order:1 Kilogram
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inquiryProduct name: 2-Methyl-4-(2-Methylbenzoylamino)Benzoic Acid CAS No.: 317374-08-6 Molecule Formula:C16H15NO3 Molecule Weight:269.30 Purity: 99.0% Package: 25kg/drum Description:White to off-white powder Manufacture Standards:Enterprise
Cas:317374-08-6
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryHuarong Industrial Group Limited established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World.
Cas:317374-08-6
Min.Order:1 Gram
FOB Price: $1.0 / 2.0
Type:Trading Company
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:317374-08-6
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inquiryHANGZHOU THINK CHEMICAL CO., LTD. (THINKCHEM) is an integrative corporation of trade, research and contract manufacture. With about ten years of business experiences on the marketing & distribution, thinkchem specializes in exp
factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:317374-08-6
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:317374-08-6
Min.Order:1 Gram
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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Type:Trading Company
inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
Cas:317374-08-6
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Negotiable
Type:Manufacturers
inquiryProduct Name: 2-methyl-4-(2-methyl-benzoylamino)-benzoic acid Synonyms: 2-methyl-4-(2-methyl-benzoylamino)-benzoic acid;2-methyl-4-(2-methyl-p-nitrob…Appearance:Solid powder Storage:Sealed,light and oxygen resistant Package:aluminum foil bag,carton
Cas:317374-08-6
Min.Order:0
Negotiable
Type:Other
inquiryHigh quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
Cas:317374-08-6
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Type:Lab/Research institutions
inquiryGOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation
Cas:317374-08-6
Min.Order:1 Kilogram
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Type:Other
inquiryWe are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
Cas:317374-08-6
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Type:Trading Company
inquiry4-amino-2-methylbenzoic acid
ortho-toluoyl chloride
2-methyl-4-(2-methylbenzoylamino)benzoic acid
Conditions | Yield |
---|---|
With pyridine In chloroform at 0 - 40℃; for 8h; Reagent/catalyst; Solvent; Temperature; | 95.6% |
carbon monoxide
2-bromo-5-(2-methylbenzoylamino)toluene
2-methyl-4-(2-methylbenzoylamino)benzoic acid
Conditions | Yield |
---|---|
Stage #1: carbon monoxide; 2-bromo-5-(2-methylbenzoylamino)toluene With palladium diacetate; tributyl-amine; cesium acetate; triphenylphosphine In N,N-dimethyl-formamide at 120℃; for 3h; carbonylation; Hydrolysis; Stage #2: With sodium hydroxide In N,N-dimethyl-formamide; toluene at 20℃; for 0.5h; | 81% |
2-methyl-4-(2-methylbenzoylamino)acetophenone
2-methyl-4-(2-methylbenzoylamino)benzoic acid
Conditions | Yield |
---|---|
Stage #1: 2-methyl-4-(2-methylbenzoylamino)acetophenone With sodium hypochlorite; water In isopropyl alcohol at 5 - 60℃; for 1h; Stage #2: With hydrogenchloride In water at 20℃; Product distribution / selectivity; | 77.2% |
carbon monoxide
7-chloro-1,2,3,4-tetrahydro-5H-benzo[b]azepin-5-one
2-bromo-5-(2-methylbenzoylamino)toluene
A
MOP-21826
B
2-methyl-4-(2-methylbenzoylamino)benzoic acid
Conditions | Yield |
---|---|
With cesium acetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triphenylphosphine; palladium diacetate In N,N-dimethyl-formamide Heating; | A n/a B 75% |
oxalyl dichloride
2-methyl-4-(2-methylbenzoylamino)benzoic acid
Conditions | Yield |
---|---|
Stage #1: 2-methyl-N-m-tolylbenzamide; aluminum (III) chloride In dichloromethane at 3℃; for 0.166667h; Stage #2: oxalyl dichloride In dichloromethane at 2 - 7℃; for 5h; Stage #3: With hydrogenchloride; sodium hydroxide; water Product distribution / selectivity; more than 3 stages; | 65.8% |
1-{2-[4-methyl-2-(2-methylbenzoylamino)phenyl]-2-oxoethyl}pyridinium chloride
2-methyl-4-(2-methylbenzoylamino)benzoic acid
Conditions | Yield |
---|---|
Stage #1: 1-{2-[2-methyl-4-(2-methylbenzoyl-amino)phenyl]-2-oxoethyl}pyridinium chloride; 1-{2-[4-methyl-2-(2-methylbenzoylamino)phenyl]-2-oxoethyl}pyridinium chloride With sodium hydroxide; water In methanol at 60 - 76℃; for 4h; Stage #2: With hydrogenchloride In methanol; water at 60 - 76℃; pH=1; Product distribution / selectivity; | 60.5% |
2-chloro-2'-methyl-4'-(2-methylbenzoylamino)-acetophenone
2-chloro-4'-methyl-2'-(2-methylbenzoylamino)aceto-phenone
2-methyl-4-(2-methylbenzoylamino)benzoic acid
Conditions | Yield |
---|---|
Stage #1: 2-chloro-2'-methyl-4'-(2-methylbenzoylamino)-acetophenone; 2-chloro-4'-methyl-2'-(2-methylbenzoylamino)aceto-phenone With sodium hypochlorite; water In isopropyl alcohol at 10 - 20℃; for 0.5 - 1h; Stage #2: With hydrogenchloride In water; isopropyl alcohol Product distribution / selectivity; | 57% |
tolvaptan
A
7-chloro-2,3-dihydro-1H-benzo[b]azepine
D
2-methyl-4-(2-methylbenzoylamino)benzoic acid
Conditions | Yield |
---|---|
With hydrogenchloride; water In acetonitrile at 80℃; for 24h; |
tolvaptan
C
2-methyl-4-(2-methylbenzoylamino)benzoic acid
Conditions | Yield |
---|---|
With sodium hydroxide In acetonitrile at 80℃; for 17h; |
methanol
tolvaptan
A
7-chloro-2,3-dihydro-1H-benzo[b]azepine
G
2-methyl-4-(2-methylbenzoylamino)benzoic acid
Conditions | Yield |
---|---|
With hydrogenchloride; water at 80℃; for 24h; |
Conditions | Yield |
---|---|
With sodium hydroxide at 80℃; for 17h; |
2-methyl-4-aminobenzaldehyde
2-methyl-4-(2-methylbenzoylamino)benzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: hydroxylamine hydrochloride; sodium formate; formic acid / 3 h / 100 °C 2: water; sodium hydroxide / ethylene glycol / 6 h / 100 °C 3: pyridine / chloroform / 8 h / 0 - 40 °C View Scheme |
1-amino-3-methylbenzene
2-methyl-4-(2-methylbenzoylamino)benzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: trichlorophosphate / 6 h / 0 - 60 °C 2: hydroxylamine hydrochloride; sodium formate; formic acid / 3 h / 100 °C 3: water; sodium hydroxide / ethylene glycol / 6 h / 100 °C 4: pyridine / chloroform / 8 h / 0 - 40 °C View Scheme |
(4R,5R)-4,5-bis(methoxymethoxy)-7-chloro-2,3,4,5-tetrahydro-1H-1-benzazepine
2-methyl-4-(2-methylbenzoylamino)benzoic acid
(4R,5R)-4,5-bis(methoxymethoxy)-7-chloro-1-[2-methyl-4-(2-methylbenzoylamino)benzoyl]-2,3,4,5-tetrahydro-1H-1-benzazepine
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 20℃; | 81% |
2-methyl-4-(2-methylbenzoylamino)benzoic acid
2-methyl-4-(2-methylbenzoylamino)benzoic acid chloride
Conditions | Yield |
---|---|
With 1-methyl-pyrrolidin-2-one; thionyl chloride In dichloromethane for 0.5h; Heating; | |
With thionyl chloride; N,N-dimethyl-formamide In dichloromethane for 3h; Reflux; | |
With thionyl chloride In N,N-dimethyl acetamide at 0 - 25℃; for 2h; Reagent/catalyst; Temperature; |
2-methyl-4-(2-methylbenzoylamino)benzoic acid
(4S,5S)-4,5-bis(methoxymethoxy)-7-chloro-1-[2-methyl-4-(2-methylbenzoylamino)benzoyl]-2,3,4,5-tetrahydro-1H-1-benzazepine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: SOCl2; NMP / CH2Cl2 / 0.5 h / Heating 2: 85 percent / pyridine / CH2Cl2 / 20 °C View Scheme |
2-methyl-4-(2-methylbenzoylamino)benzoic acid
(4S,5R)-4,5-bis(methoxymethoxy)-7-chloro-1-[2-methyl-4-(2-methylbenzoylamino)benzoyl]-2,3,4,5-tetrahydro-1H-1-benzazepine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: SOCl2; NMP / CH2Cl2 / 0.5 h / Heating 2: 86 percent / pyridine / CH2Cl2 / 20 °C View Scheme |
2-methyl-4-(2-methylbenzoylamino)benzoic acid
(4R,5S)-4,5-bis(methoxymethoxy)-7-chloro-1-[2-methyl-4-(2-methylbenzoylamino)benzoyl]-2,3,4,5-tetrahydro-1H-1-benzazepine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: SOCl2; NMP / CH2Cl2 / 0.5 h / Heating 2: 83 percent / pyridine / CH2Cl2 / 20 °C View Scheme |
2-methyl-4-(2-methylbenzoylamino)benzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: SOCl2; NMP / CH2Cl2 / 0.5 h / Heating 2: 85 percent / pyridine / CH2Cl2 / 20 °C 3: 82 percent / conc. HCl / methanol / 3.5 h / 60 °C View Scheme |
2-methyl-4-(2-methylbenzoylamino)benzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: SOCl2; NMP / CH2Cl2 / 0.5 h / Heating 2: 86 percent / pyridine / CH2Cl2 / 20 °C 3: 87 percent / conc. HCl / methanol / 60 °C View Scheme |
2-methyl-4-(2-methylbenzoylamino)benzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: SOCl2; NMP / CH2Cl2 / 0.5 h / Heating 2: 83 percent / pyridine / CH2Cl2 / 20 °C 3: 89 percent / conc. HCl / methanol / 60 °C View Scheme |
2-methyl-4-(2-methylbenzoylamino)benzoic acid
N-(4-(7-chloro-5-hydroxy-2,2-dideutero-3,4,5-trihydro-1H-benzo[b]azepine-1-carbonyl)-3-methylphenyl)-2-methylbenzamide
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: thionyl chloride / N,N-dimethyl-formamide / dichloromethane / 3 h / Reflux 2.1: triethylamine / dichloromethane / 4 h / 0 °C 3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C 3.2: 0 °C View Scheme |
2-methyl-4-(2-methylbenzoylamino)benzoic acid
N-(4-(5-(tert-butyldimethylsilyloxy)-7-chloro-2,2-dideutero-3,4,5-trihydro-1H-benzo[b]azepine-1-carbonyl)-3-methylphenyl)-2-methylbenzamide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: thionyl chloride / N,N-dimethyl-formamide / dichloromethane / 3 h / Reflux 2: triethylamine / dichloromethane / 4 h / 0 °C View Scheme |
2-methyl-4-(2-methylbenzoylamino)benzoic acid
N-(4-(7-chloro-5-oxo-2,2-dideutero-3,4-dihydro-1H-benzo[b]azepine-1-carbonyl)-3-methylphenyl)-2-methylbenzamide
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: thionyl chloride / N,N-dimethyl-formamide / dichloromethane / 3 h / Reflux 2.1: triethylamine / dichloromethane / 4 h / 0 °C 3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C 3.2: 0 °C 4.1: manganese(IV) oxide / dichloromethane / 8 h / Reflux View Scheme |
2-methyl-4-(2-methylbenzoylamino)benzoic acid
N-(4-(7-chloro-2,3-dihydro-5-hydroxy-2,2,4,4,5-pentadeutero-1H-benzo[b]azepine-1-carbonyl)-3-methylphenyl)-2-methylbenzamide
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1.1: thionyl chloride / N,N-dimethyl-formamide / dichloromethane / 3 h / Reflux 2.1: triethylamine / dichloromethane / 4 h / 0 °C 3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C 3.2: 0 °C 4.1: manganese(IV) oxide / dichloromethane / 8 h / Reflux 5.1: d(4)-methanol; sodium hydroxide / 18 h / 20 °C / Inert atmosphere 6.1: d(4)-methanol; sodium borodeuteride / 2 h / 0 °C View Scheme |
2-methyl-4-(2-methylbenzoylamino)benzoic acid
N-(4-(7-chloro-2,3-dihydro-5-oxo-2,2,4,4-tetradeutero-1H-benzo[b]azepine-1-carbonyl)-3-methylphenyl)-2-methylbenzamide
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: thionyl chloride / N,N-dimethyl-formamide / dichloromethane / 3 h / Reflux 2.1: triethylamine / dichloromethane / 4 h / 0 °C 3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C 3.2: 0 °C 4.1: manganese(IV) oxide / dichloromethane / 8 h / Reflux 5.1: d(4)-methanol; sodium hydroxide / 18 h / 20 °C / Inert atmosphere View Scheme |
2-methyl-4-(2-methylbenzoylamino)benzoic acid
tolvaptan
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: thionyl chloride / N,N-dimethyl acetamide / 2 h / 0 - 25 °C 2: 2,6-dimethylpyridine / N,N-dimethyl acetamide; water / 2 h / 0 °C View Scheme |
2-methyl-4-(2-methylbenzoylamino)benzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: thionyl chloride / toluene / 3 h / Reflux 1.2: 1 h 2.1: thionyl chloride / dichloromethane / 4 h / Reflux 3.1: pyridine / ethyl acetate / 20 °C 4.1: potassium borohydride; ethanol / 1 h / 25 - 35 °C View Scheme |
2-methyl-4-(2-methylbenzoylamino)benzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: thionyl chloride / toluene / 3 h / Reflux 1.2: 1 h 2.1: thionyl chloride / dichloromethane / 4 h / Reflux View Scheme |
2-methyl-4-(2-methylbenzoylamino)benzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: thionyl chloride / toluene / 3 h / Reflux 1.2: 1 h 2.1: thionyl chloride / dichloromethane / 4 h / Reflux 3.1: pyridine / ethyl acetate / 20 °C View Scheme |
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