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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

Iminodibenzylcarbonyl chloride Manufacturer/High quality/Best price/In stock

Cas:33948-19-5

Min.Order:1 Kilogram

FOB Price: $3.0

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality Iminodibenzyl Carbonyl Chloride supplier in China

Cas:33948-19-5

Min.Order:0 Metric Ton

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Hebei yanxi chemical co.,LTD.

Hebei Yanxi Chemical Co., Ltd. is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low car

Factory supply Iminodibenzy Carbonyl Chloride

Cas:33948-19-5

Min.Order:1 Metric Ton

FOB Price: $1.0 / 2.0

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

Iminodibenzyl-5-carbonyl chloride

Cas:33948-19-5

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

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Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

Iminodibenzylcarbonyl chloride CAS 33948-19-5

Cas:33948-19-5

Min.Order:1 Kilogram

FOB Price: $9.0 / 99.0

Type:Trading Company

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Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

TIANFU CHEM-- Iminodibenzylcarbonyl chloride

Cas:33948-19-5

Min.Order:1 Kilogram

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Factory direct supplyCAS 33948-19-5 with competitive price

Cas:33948-19-5

Min.Order:10 Gram

FOB Price: $146.0 / 176.0

Type:Trading Company

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

Hot Sell Factory Supply Raw Material CAS 33948-19-5 Iminodibenzy Carbonyl Chloride

Cas:33948-19-5

Min.Order:10 Kilogram

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Type:Trading Company

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Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W

Iminodibenzylcarbonyl chloride CAS33948-19-5

Cas:33948-19-5

Min.Order:1 Kilogram

FOB Price: $7.0 / 9.0

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Hubei Langyou International Trading Co., Ltd

Advantages: Hubei XinRunde Chemical Co., Ltd is a renowned pharmaceutical manufacturer. We can offer high quality products at competitive price in quick delivery with 100% custom pass guaranteed. Never stop striving to offer our best s

Iminodibenzylcarbonyl Chloride 33948-19-5 API Manufacturer

Cas:33948-19-5

Min.Order:10 Gram

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Type:Other

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Iminodibenzylcarbonyl chloride 33948-19-5

Cas:33948-19-5

Min.Order:1 Kilogram

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Iminodibenzylcarbonyl chloride

Cas:33948-19-5

Min.Order:1 Kilogram

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Hubei Jiutian Bio-medical Technology Co., Ltd

1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie

cas 33948-19-5 CAS 33948-19-5 Iminodibenzylcarbonyl chloride

Cas:33948-19-5

Min.Order:1 Kilogram

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Iminodibenzylcarbonyl chloride

Cas:33948-19-5

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

Iminodibenzyl Carbonyl Chloride

Cas:33948-19-5

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

Iminodibenzylcarbonyl chloride

Cas:33948-19-5

Min.Order:0 Metric Ton

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Afine Chemicals Limited

Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments

IMINODIBENZYL CARBONYL CHLORIDE

Cas:33948-19-5

Min.Order:1 Gram

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Iminodibenzylcarbonyl chloride

Cas:33948-19-5

Min.Order:0

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SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

Iminodibenzylcarbonylchloride 10,11-dihydro-dibenzo[b,f]azep ine-5-carbonyl chloride

Cas:33948-19-5

Min.Order:4 Kilogram

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Iminodibenzyl-5-Carbonyl Chloride

Cas:33948-19-5

Min.Order:0 Metric Ton

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Hangzhou Fonlynn Health Technology Co., Ltd.

Packing: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Transportation:Express/Sea/Air Port:Ningbo/Shanghai/Qingd

iminodibenzyl carbonyl chloride

Cas:33948-19-5

Min.Order:0

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Chemlyte Solutions

Chemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff

Featured products Iminodibenzylcarbonyl chloride

Cas:33948-19-5

Min.Order:100 Gram

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SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

Factory supply Iminodibenzy Carbonyl Chloride

Cas:33948-19-5

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

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Siwei Development Group Ltd.

Product name: Iminodibenzyl Carbonyl Chloride CAS No.:33948-19-5 Molecule Formula:C15H12ClNO Molecule Weight:257.71 Purity: 99.0% Package: 25kg/drum Description:Light brown or pale yellow powder Manufacture Standards:Enterprise Standa

High Quality Iminodibenzyl Carbonyl Chloride

Cas:33948-19-5

Min.Order:1 Kilogram

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EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

Iminodibenzylcarbonyl chloride

Cas:33948-19-5

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

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Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

Iminodibenzylcarbonyl chloride

Cas:33948-19-5

Min.Order:1 Gram

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KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

Iminodibenzylcarbonyl chloride

Cas:33948-19-5

Min.Order:1 Metric Ton

FOB Price: $1.5

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Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

Iminodibenzyl-5-carbonyl chloride

Cas:33948-19-5

Min.Order:0

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Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

Iminodibenzylcarbonyl chloride Cas no.33948-19-5 98%

Cas:33948-19-5

Min.Order:0

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Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

Factory supply Iminodibenzy Carbonyl Chloride

Cas:33948-19-5

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Synthetic route

phosgene
75-44-5

phosgene

9,10-dihydrodibenzazepine
494-19-9

9,10-dihydrodibenzazepine

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride
33948-19-5

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride

Conditions
ConditionsYield
In toluene at 90 - 95℃; for 3.5h;90%
With sodium hydroxide In chlorobenzene at 100 - 115℃; for 4h;80%
With toluene
With toluene
n-butyllithium
109-72-8, 29786-93-4

n-butyllithium

6-fluoro-3-[1-(3-hydroxypropyl)-4-piperidinyl]-1,2-benzisoxazole
150332-87-9

6-fluoro-3-[1-(3-hydroxypropyl)-4-piperidinyl]-1,2-benzisoxazole

A

1-[3-((10,11-dihydro-5H-dibenz[b,f]azepin-5-yl)carbonyloxy)propyl]-4-(6-fluoro-1,2-benzisoxazol-3-yl)piperidine, oxalate

1-[3-((10,11-dihydro-5H-dibenz[b,f]azepin-5-yl)carbonyloxy)propyl]-4-(6-fluoro-1,2-benzisoxazol-3-yl)piperidine, oxalate

B

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride
33948-19-5

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride

Conditions
ConditionsYield
In hexane
9,10-dihydrodibenzazepine
494-19-9

9,10-dihydrodibenzazepine

bis(trichloromethyl) carbonate
32315-10-9

bis(trichloromethyl) carbonate

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride
33948-19-5

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride

Conditions
ConditionsYield
With pyridine In 1,2-dichloro-ethane at 75℃; for 3h; Inert atmosphere;
With sodium hydroxide In chlorobenzene at 100 - 115℃; for 4.5h;
In chlorobenzene at 110℃; for 5h; Temperature;
With sodium hydrogencarbonate In dichloromethane at 0 - 20℃; for 12.5h;
5,10-bis(2-nitrobenzenesulfonyl)-5,10-diaza-1,14-tetradecanediamine
951010-97-2

5,10-bis(2-nitrobenzenesulfonyl)-5,10-diaza-1,14-tetradecanediamine

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride
33948-19-5

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride

C39H47N7O9S2

C39H47N7O9S2

Conditions
ConditionsYield
In dichloromethane at 20℃; for 19h;95%
In dichloromethane at 20℃;
10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride
33948-19-5

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride

5H-dibenz[b,f]azepine-5-carbonylchloride
33948-22-0

5H-dibenz[b,f]azepine-5-carbonylchloride

Conditions
ConditionsYield
With sodium bromate; N-benzyl-N,N,N-triethylammonium chloride; bromine; dibenzoyl peroxide In chlorobenzene at 92 - 97℃; for 8.5h; Temperature; Reagent/catalyst;90.5%
Multi-step reaction with 2 steps
1: Br2 / chlorobenzene / 1.5 h / 145 - 150 °C
2: chlorobenzene / 2 h / 150 - 155 °C
View Scheme
With bromine In chlorobenzene at 80℃; for 6h; Temperature; Inert atmosphere;
10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride
33948-19-5

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride

9,10-dihydrodibenzazepine
494-19-9

9,10-dihydrodibenzazepine

Conditions
ConditionsYield
In acetonitrile electrolysis (Et4NClO4, Hg-dropelectrode);90%
Methyl-(1-methyl-[4]piperidyl)-amin
73579-08-5

Methyl-(1-methyl-[4]piperidyl)-amin

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride
33948-19-5

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride

N-methyl-N-(1-methylpiperodin-4-yl)-10,11-dihydro-5H-dibenzo[b,f]azepine-5-carboxamide

N-methyl-N-(1-methylpiperodin-4-yl)-10,11-dihydro-5H-dibenzo[b,f]azepine-5-carboxamide

Conditions
ConditionsYield
With triethylamine In dichloromethane for 2h; Heating;90%
10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride
33948-19-5

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride

10,11-Dihydrocarbamazepin
3564-73-6

10,11-Dihydrocarbamazepin

Conditions
ConditionsYield
With ammonia In methanol; water at 57 - 59℃; for 1.5h;85.35%
With ethanol; ammonia
With ethanol; ammonia
pyrrolidine
123-75-1

pyrrolidine

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride
33948-19-5

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride

(10,11-dihydro-5H-dibenzo[b,f]azepin-5-yl)(pyrrolidin-1-yl)methanone
294194-09-5

(10,11-dihydro-5H-dibenzo[b,f]azepin-5-yl)(pyrrolidin-1-yl)methanone

Conditions
ConditionsYield
With triethylamine In benzene85%
4-phenyl-1-piperazine
92-54-6

4-phenyl-1-piperazine

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride
33948-19-5

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride

(11,12-dihydro-5H-dibenzo[b,f]azepin-5-yl)(4-phenylpiperazin-1-yl)methanone
1250430-98-8

(11,12-dihydro-5H-dibenzo[b,f]azepin-5-yl)(4-phenylpiperazin-1-yl)methanone

Conditions
ConditionsYield
With triethylamine In 1,4-dioxane83%
10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride
33948-19-5

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride

Propargylamine
2450-71-7

Propargylamine

N-(prop-2-ynyl)-10,11-dihydro-5H-dibenzo[b,f]azepine-5-carboxamide
127025-48-3

N-(prop-2-ynyl)-10,11-dihydro-5H-dibenzo[b,f]azepine-5-carboxamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0℃; for 24h; Reflux;76%
1-phenylmethylpiperazine
2759-28-6

1-phenylmethylpiperazine

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride
33948-19-5

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride

5-[(4-benzylpiperazin-1-yl)carbonyl]-10,11-dihydro-5H-dibenzo[b,f]azepine

5-[(4-benzylpiperazin-1-yl)carbonyl]-10,11-dihydro-5H-dibenzo[b,f]azepine

Conditions
ConditionsYield
With triethylamine In dichloromethane for 2h; Heating;75%
10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride
33948-19-5

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride

methyl 3,5-diaminobenzoate
1949-55-9

methyl 3,5-diaminobenzoate

N,N'-bis(iminodibenzyl-5-carbonyl)-3,5-diaminobenzoic methyl ester
175085-87-7

N,N'-bis(iminodibenzyl-5-carbonyl)-3,5-diaminobenzoic methyl ester

Conditions
ConditionsYield
With dmap; triethylamine In dichloromethane for 24h; Heating;72%
10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride
33948-19-5

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride

2-propynyl 3-hydroxy-9β,13α-dimethyl-2-oxo-24,25,26-trinoroleana-1(10),3,5,7-tetraen-29-oate

2-propynyl 3-hydroxy-9β,13α-dimethyl-2-oxo-24,25,26-trinoroleana-1(10),3,5,7-tetraen-29-oate

(6bS,8aS,11R,12bS,14aR)-4,6b,8a,11,12b,14a-hexamethyl-2-oxo-11-((prop-2-yn-1-yloxy)carbonyl)-2,6b,7,8,8a,9,10,11,12,12a,12b,13,14,14a-tetradecahydropicen-3-yl 10,11-dihydro-5H-dibenzo[b,f]azepine-5-carboxylate

(6bS,8aS,11R,12bS,14aR)-4,6b,8a,11,12b,14a-hexamethyl-2-oxo-11-((prop-2-yn-1-yloxy)carbonyl)-2,6b,7,8,8a,9,10,11,12,12a,12b,13,14,14a-tetradecahydropicen-3-yl 10,11-dihydro-5H-dibenzo[b,f]azepine-5-carboxylate

Conditions
ConditionsYield
With dmap; triethylamine In dichloromethane at 0 - 25℃; for 12h;62%
10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride
33948-19-5

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride

(2S)-2-[(10,11-dihydro-5H-dibenzo[b,f]azepin-5-ylcarbonyl)amino]-3-(1H-indol-3-yl)propionic acid methyl ester

(2S)-2-[(10,11-dihydro-5H-dibenzo[b,f]azepin-5-ylcarbonyl)amino]-3-(1H-indol-3-yl)propionic acid methyl ester

Conditions
ConditionsYield
With N-ethylmorpholine; In N,N-dimethyl-formamide at 0 - 40℃;30.3%
10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride
33948-19-5

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride

N,N',N'-trimethylenediamine
142-25-6

N,N',N'-trimethylenediamine

10,11-dihydro-dibenz[b,f]azepine-5-carboxylic acid-[(2-dimethylamino-ethyl)-methyl-amide]

10,11-dihydro-dibenz[b,f]azepine-5-carboxylic acid-[(2-dimethylamino-ethyl)-methyl-amide]

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride
33948-19-5

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride

10-bromo-10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride
33948-20-8

10-bromo-10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride

Conditions
ConditionsYield
With bromine In chlorobenzene at 145 - 150℃; for 1.5h;
10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride
33948-19-5

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride

NG-tosylargine
4353-32-6

NG-tosylargine

Nα-(10,11-dihydroo-5H-dibenz[b.f]azepine-5-carbonyl)toluenesulfonyl-L-arginine

Nα-(10,11-dihydroo-5H-dibenz[b.f]azepine-5-carbonyl)toluenesulfonyl-L-arginine

Conditions
ConditionsYield
With sodium carbonate In 1,4-dioxane
Spermine
71-44-3

Spermine

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride
33948-19-5

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride

C25H37N5O

C25H37N5O

Conditions
ConditionsYield
In dichloromethane at 20℃;
C23H34N6O8S2
951010-96-1

C23H34N6O8S2

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride
33948-19-5

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride

C38H45N7O9S2

C38H45N7O9S2

Conditions
ConditionsYield
In dichloromethane at 20℃;
10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride
33948-19-5

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride

carbamazepin
298-46-4

carbamazepin

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: Br2 / chlorobenzene / 1.5 h / 145 - 150 °C
2: chlorobenzene / 2 h / 150 - 155 °C
3: 25percent NH4OH / methanol / 5 h / 75 - 85 °C
View Scheme
10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride
33948-19-5

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride

(S)-1-(10,11-Dihydro-5H-dibenz[b,f]azepine-5-carbonyl)-4-(benzyloxycarbonyl)piperazine-2-carboxylic acid

(S)-1-(10,11-Dihydro-5H-dibenz[b,f]azepine-5-carbonyl)-4-(benzyloxycarbonyl)piperazine-2-carboxylic acid

Conditions
ConditionsYield
284 mg (24%)
10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride
33948-19-5

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride

benzylamine
100-46-9

benzylamine

10,11-dihydro-dibenzo[b,f]azepine-5-carboxylic acid benzylamide

10,11-dihydro-dibenzo[b,f]azepine-5-carboxylic acid benzylamide

Conditions
ConditionsYield
In dichloromethane at 20℃; for 27h;
C17H22N2O3*ClH
1131679-43-0

C17H22N2O3*ClH

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride
33948-19-5

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride

C32H33N3O4
1131680-29-9

C32H33N3O4

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran
C17H22N2O3*ClH
1131679-47-4

C17H22N2O3*ClH

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride
33948-19-5

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride

C32H33N3O4
1131680-31-3

C32H33N3O4

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran
10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride
33948-19-5

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride

10,11-Dihydro-dibenzo[b,f]azepine-5-carboxylic acid hydrazide
1676-31-9

10,11-Dihydro-dibenzo[b,f]azepine-5-carboxylic acid hydrazide

Conditions
ConditionsYield
With hydrazine hydrate In diethyl ether; ethanol for 0.5h; Schlenk technique; Inert atmosphere;
10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride
33948-19-5

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride

[ReBr(CO)3(H2BF)]
1417342-96-1

[ReBr(CO)3(H2BF)]

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: hydrazine hydrate / diethyl ether; ethanol / 0.5 h / Schlenk technique; Inert atmosphere
2: toluene-4-sulfonic acid / toluene / 0.5 h / 20 °C / Schlenk technique; Inert atmosphere
3: toluene / 5 h / Schlenk technique; Inert atmosphere; Reflux
View Scheme
10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride
33948-19-5

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride

C22H19N3O2
1417342-90-5

C22H19N3O2

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: hydrazine hydrate / diethyl ether; ethanol / 0.5 h / Schlenk technique; Inert atmosphere
2: toluene-4-sulfonic acid / toluene / 0.5 h / 20 °C / Schlenk technique; Inert atmosphere
View Scheme
10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride
33948-19-5

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride

(R)-Phenylglycinol
56613-80-0

(R)-Phenylglycinol

C23H22N2O2

C23H22N2O2

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0℃; for 12h; Inert atmosphere;
10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride
33948-19-5

10,11-dihydro-dibenzo[b,f]azepine-5-carbonyl chloride

(R)-Phenylglycinol
56613-80-0

(R)-Phenylglycinol

C33H43N3O6Si

C33H43N3O6Si

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: triethylamine / dichloromethane / 12 h / 0 °C / Inert atmosphere
2: triethylamine / benzene / 72 h / 111 °C / Inert atmosphere
View Scheme

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