Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:4547-02-8
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inquiryBENZP-DINITRIDE-THIO-KETONE Basic information Product Name: BENZP-DINITRIDE-THIO-KETONE Synonyms: BENZP-DINITRIDE-THIO-KETONE;7-Chloro-5-phenyl-1H-benzo[e][1,4]diaz
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufactu
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiryBENZP-DINITRIDE-THIO-KETONE CAS:4547-02-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organi
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inquirySuperiority We can customize and synthesize products that other suppliers may not be able to provide. Advantage cof, mof ligand manufacturer Product Detail bes
Cas:4547-02-8
Min.Order:100 Kilogram
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:4547-02-8
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inquiryProduct Name: BENZP-DINITRIDE-THIO-KETONE Synonyms: BENZP-DINITRIDE-THIO-KETONE;7-Chloro-5-phenyl-1H-benzo[e][1,4]diazepine-2(3H)-thione;Thionordiazepam;7-Chloro-5-phenyl-1H-benzo[e][1,4]diazepine-2(3H);Benzodiazepines Intermediate 1 CAS: 4547
Cas:4547-02-8
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inquiry1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s
Cas:4547-02-8
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryOur Advantage 1. Rich experience We specialize in this filed for many years, our APIs exported to all over the world and and we established long friendly relations of cooperation with our clients. 2. Great quality,purity and favorable Good qual
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inquiryAppearance:white or yellowish white flaky crystal Storage:Keep the sun from direct sunlight ;prevention against high temperature Package:As customer request Application:Used for research and industrial manufacture. Transportatio
Cas:4547-02-8
Min.Order:100 Metric Ton
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:4547-02-8
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:4547-02-8
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:4547-02-8
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inquiry7-Chloro-5-phenyl-1H-benzo[e]-[1,4]diazepine-2(3H)-thioneAppearance:white powder Storage:Store in dry, dark and ventilated place Package:according to customers' requirements Application:chemical research Transportation:By air(EMS or EUB or FedEx or T
Cas:4547-02-8
Min.Order:1 Gram
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inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:4547-02-8
Min.Order:100 Gram
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inquirySuperior quality, moderate price & quick delivery. Appearance:light yellow crystal solid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:100g/bottle,1kg/bottle,25kg/drum or as per your request Application:Hypn
Cas:4547-02-8
Min.Order:1 Gram
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Type:Trading Company
inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:4547-02-8
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inquiryProduct name: 7-Chloro-1,3-dihydro-5-Phenyl-2H-1,4-Benzodiazepine-2-Thione CAS No.:4547-02-8 Molecule Formula:C15H11ClN2S Molecule Weight:286.78 Purity: 99.0% Package: 25kg/drum Description:White crystalline powder Manufacture Standar
Cas:4547-02-8
Min.Order:1 Kilogram
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Type:Trading Company
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:4547-02-8
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inquiryOur Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:4547-02-8
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inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
Cas:4547-02-8
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:4547-02-8
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:4547-02-8
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inquiryConditions | Yield |
---|---|
With n-butyllithium; tetraphosphorus decasulfide In tetrahydrofuran; hexane for 16h; Heating; | 87% |
With tetraphosphorus decasulfide In pyridine Heating; 1.) 30 min. reflux, 2.) 1 h; | 67% |
With tetraphosphorus decasulfide; sodium hydrogencarbonate In acetonitrile for 24h; Heating; | |
With Lawessons reagent In 1,2-dimethoxyethane at 75℃; | |
With tetraphosphorus decasulfide; triethylamine In toluene at 75℃; for 8h; Solvent; Temperature; Inert atmosphere; | 175 g |
2,3-dihydro-5-phenyl-1H-1,4-benzodiazepin-2-one
7-chloro-1,3-dihydro-5-phenyl-2H-1,4-benzodiazepin-2-thione
Conditions | Yield |
---|---|
Stage #1: 2,3-dihydro-5-phenyl-1H-1,4-benzodiazepin-2-one With aluminum (III) chloride; chlorine In dichloromethane at 10 - 20℃; Stage #2: With sodiumsulfide nonahydrate; tetrabutylammomium bromide; dihydrogen peroxide for 2h; Reflux; | 78.7% |
di-morpholin-4-yl-phosphinic acid 7-chloro-5-phenyl-3H-benzo[e][1,4]diazepin-2-yl ester
7-chloro-1,3-dihydro-5-phenyl-2H-1,4-benzodiazepin-2-thione
Conditions | Yield |
---|---|
In tetrahydrofuran |
2-Amino-5-chlorobenzophenone
7-chloro-1,3-dihydro-5-phenyl-2H-1,4-benzodiazepin-2-thione
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: cyclohexane / 4 h / 60 - 81 °C 2: hexamethylenetetramine; ammonium bicarbonate / ethanol / 6 h / 40 - 50 °C 3: triethylamine; tetraphosphorus decasulfide / toluene / 8 h / 75 °C / Inert atmosphere View Scheme |
(2-Aminomethyl-[1,3]dioxolan-2-yl)-methanol
7-chloro-1,3-dihydro-5-phenyl-2H-1,4-benzodiazepin-2-thione
{2-[(7-chloro-5-phenyl-3H-benzo[e][1,4]diazepin-2-ylamino)-methyl]-[1,3]dioxolan-2-yl}-methanol
Conditions | Yield |
---|---|
In ethanol at 100℃; for 3h; | 90% |
N-Methylhydroxylamine
7-chloro-1,3-dihydro-5-phenyl-2H-1,4-benzodiazepin-2-thione
N-(7-Chlor-5-phenyl-3H-1,4-benzodiazepin-2-yl)-N-methylhydroxylamin
Conditions | Yield |
---|---|
In methanol for 1.5h; Heating; | 87% |
(3-azidoacetonyl)amine, ethylene ketal
7-chloro-1,3-dihydro-5-phenyl-2H-1,4-benzodiazepin-2-thione
(2-azidomethyl-[1,3]dioxolan-2-ylmethyl)-(7-chloro-5-phenyl-3H-benzo[e][1,4]diazepin-2-yl)-amine
Conditions | Yield |
---|---|
In ethanol | 87% |
In ethanol; water |
2-(methanesulfonamido)propionhydrazide
7-chloro-1,3-dihydro-5-phenyl-2H-1,4-benzodiazepin-2-thione
N-[1-(8-Chloro-6-phenyl-4H-2,3,5,10b-tetraaza-benzo[e]azulen-1-yl)-ethyl]-methanesulfonamide
Conditions | Yield |
---|---|
Heating; | 84% |
7-chloro-1,3-dihydro-5-phenyl-2H-1,4-benzodiazepin-2-thione
ethylhydrazine carboxylate
3-(7-chloro-5-phenyl-3H-1,4-benzodiazepin-2-yl)carbazic acid ethyl ester
Conditions | Yield |
---|---|
In ethanol for 24h; Heating; | 77% |
glycine
7-chloro-1,3-dihydro-5-phenyl-2H-1,4-benzodiazepin-2-thione
N-(7-chloro-5-phenyl-3H-benzo[e][1,4]diazepin-2-yl)-glycine
Conditions | Yield |
---|---|
With sodium carbonate In ethanol; water | 77% |
7-chloro-1,3-dihydro-5-phenyl-2H-1,4-benzodiazepin-2-thione
4-methyl-1-piperazinylacetic acid hydrazide
8-chloro-1-(4-methyl-piperazin-1-ylmethyl)-6-phenyl-4H-benzo[f][1,2,4]triazolo[4,3-a][1,4]diazepine
Conditions | Yield |
---|---|
In butan-1-ol for 4h; Heating; | 72% |
ethyl(methylthio)acetic hydrazide
7-chloro-1,3-dihydro-5-phenyl-2H-1,4-benzodiazepin-2-thione
8-Chloro-1-methylsulfanylmethyl-6-phenyl-4H-2,3,5,10b-tetraaza-benzo[e]azulene
Conditions | Yield |
---|---|
In butan-1-ol Heating; | 65% |
2-[2-(2-Aminomethyl-[1,3]dioxolan-2-yl)-ethyl]-isoindole-1,3-dione
7-chloro-1,3-dihydro-5-phenyl-2H-1,4-benzodiazepin-2-thione
A
2-{2-[2-(7-Chloro-5-phenyl-3H-benzo[e][1,4]diazepin-2-ylamino)-ethyl]-[1,3]dioxolan-2-ylmethyl}-isoindole-1,3-dione
B
N-(2-{2-[(7-chloro-5-phenyl-3H-benzo[e][1,4]diazepin-2-ylamino)-methyl]-[1,3]dioxolan-2-yl}-ethyl)-phthalimide
Conditions | Yield |
---|---|
In ethanol at 60℃; | A 36% B 65% |
In ethanol at 60℃; overnight; | A 36% B 58% |
2-(ethanesulfonamido)propionhydrazide
7-chloro-1,3-dihydro-5-phenyl-2H-1,4-benzodiazepin-2-thione
Ethanesulfonic acid [1-(8-chloro-6-phenyl-4H-2,3,5,10b-tetraaza-benzo[e]azulen-1-yl)-ethyl]-amide
Conditions | Yield |
---|---|
Heating; | 63% |
(ethanesulfonamido)acethydrazide
7-chloro-1,3-dihydro-5-phenyl-2H-1,4-benzodiazepin-2-thione
Ethanesulfonic acid (8-chloro-6-phenyl-4H-2,3,5,10b-tetraaza-benzo[e]azulen-1-ylmethyl)-amide
Conditions | Yield |
---|---|
Heating; | 61% |
4-hydroxy-but-2-ynamine
7-chloro-1,3-dihydro-5-phenyl-2H-1,4-benzodiazepin-2-thione
4-(7-chloro-5-phenyl-3H-benzo[e][1,4]diazepin-2-ylamino)-but-2-yn-1-ol
Conditions | Yield |
---|---|
In tetrahydrofuran Ambient temperature; | 57% |
(methanesulfonamido)acethydrazide
7-chloro-1,3-dihydro-5-phenyl-2H-1,4-benzodiazepin-2-thione
N-(8-Chloro-6-phenyl-4H-2,3,5,10b-tetraaza-benzo[e]azulen-1-ylmethyl)-methanesulfonamide
Conditions | Yield |
---|---|
Heating; | 57% |
N-<<2-(aminomethyl)-1,3-dioxolan-2-yl>methyl>phthalimide
7-chloro-1,3-dihydro-5-phenyl-2H-1,4-benzodiazepin-2-thione
A
C21H16N2O6
B
N-<<2-<<7-chloro-5-phenyl-3H-1,4-benzodiazepin-2-yl>amino>methyl>-1,3-dioxolan-2-yl>methylphthalimide
Conditions | Yield |
---|---|
In ethanol at 60℃; for 18h; | A 1.9 g B 52.8% |
N-benzyl hydroxylalmine
7-chloro-1,3-dihydro-5-phenyl-2H-1,4-benzodiazepin-2-thione
N-Benzyl-N-(7-chlor-5-phenyl-3H-1,4-benzodiazepin-2-yl)-hydroxylamin
Conditions | Yield |
---|---|
In methanol for 1.5h; Heating; | 48% |
1-chloro-2-(4-methyl-1-piperazinyl)ethane dihydrochloride
(2E)-but-2-enedioic acid
7-chloro-1,3-dihydro-5-phenyl-2H-1,4-benzodiazepin-2-thione
Conditions | Yield |
---|---|
In tetrahydrofuran; ethanol | 42% |
5-methyl-1H-imidazole-4-carboxylic acid hydrazide
7-chloro-1,3-dihydro-5-phenyl-2H-1,4-benzodiazepin-2-thione
8-chloro-1-(5-methyl-4-imidazolyl)-6-phenyl-4H-s-triazolo<4,3-a>-1,4-benzodiazepine
Conditions | Yield |
---|---|
In butan-1-ol for 8h; Heating; | 38% |
3-ethyl-2-methylsulfanyl-benzothiazolium; toluene-4-sulfonate
7-chloro-1,3-dihydro-5-phenyl-2H-1,4-benzodiazepin-2-thione
7-chloro-3-(3-ethyl-3H-benzothiazol-2-ylidene)-5-phenyl-1,3-dihydro-benzo[e][1,4]diazepine-2-thione
Conditions | Yield |
---|---|
With triethylamine In ethanol |
(2-chloroethyl)dimethylamine hydrochloride
7-chloro-1,3-dihydro-5-phenyl-2H-1,4-benzodiazepin-2-thione
2-(2-dimethylaminoethylthio)-5-phenyl-7-chloro-3H-1,4-benzodiazepine
Conditions | Yield |
---|---|
With potassium hydroxide In tetrahydrofuran; water for 1.5h; Ambient temperature; Yield given; |
C-(2-Dimethylaminomethyl-[1,3]dioxolan-2-yl)-methylamine
7-chloro-1,3-dihydro-5-phenyl-2H-1,4-benzodiazepin-2-thione
7-chloro-5-phenyl-2-[[3-(dimethylamino)acetonyl]amino]-3H-1,4-benzodiazepine, ethylene ketal
Conditions | Yield |
---|---|
In butan-1-ol at 60℃; for 0.5h; |
2-[2-(2-Aminomethyl-[1,3]dioxolan-2-yl)-ethyl]-isoindole-1,3-dione
7-chloro-1,3-dihydro-5-phenyl-2H-1,4-benzodiazepin-2-thione
A
2-[4-(7-Chloro-5-phenyl-3H-benzo[e][1,4]diazepin-2-ylamino)-2-oxo-butyl]-isoindole-1,3-dione
B
2-[4-(7-Chloro-5-phenyl-3H-benzo[e][1,4]diazepin-2-ylamino)-3-oxo-butyl]-isoindole-1,3-dione
C
N-[2-(8-chloro-6-phenyl-4H-benzo[f]imidazo[1,5-a][1,4]diazepin-1-yl)-ethyl]-phthalimide
Conditions | Yield |
---|---|
With sulfuric acid 1.) EtOH, 60 deg C, 2.) RT; Yield given. Multistep reaction. Yields of byproduct given; | |
With sulfuric acid 1.) EtOH, 60 deg C 2.) RT; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; |
methylamine
7-chloro-1,3-dihydro-5-phenyl-2H-1,4-benzodiazepin-2-thione
(7-chloro-5-phenyl-1,3-dihydro-benzo[e][1,4]diazepin-2-ylidene)-methyl-amine
Conditions | Yield |
---|---|
In water; acetonitrile at 20℃; for 3h; |
7-chloro-1,3-dihydro-5-phenyl-2H-1,4-benzodiazepin-2-thione
7-chloro-2-(N-nitrosomethylamino)-5-phenyl-3H-1,4-benzodiazepine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: acetonitrile; H2O / 3 h / 20 °C 2: 0.55 g / sodium nitrite; AcOH / 3 h / 20 °C View Scheme |
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