CAS No.4695-13-0,2,2-DIPHENYLACETAMIDE Suppliers

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Henan Tianfu Chemical Co., Ltd.

Benzeneacetamide, a-phenyl- 2,2-diphenylethanamide; Acetamide, 2,2-diphenyl; Diphenylacetic acid amide; CAS No.: 4695-13-0 Molecular formula: C14H13NO Molecular weight: 211.25900 Exact quality: 211.10000 PSA: 43.09000 LogP: 3.00410 Ph

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Benzeneacetamide, a-phenyl- cas 4695-13-0Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

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Nanjing Raymon Biotech Co., Ltd.

1-((4'-chloro-5,5-dimethyl-3,4,5,6-tetrahydro-[1,1'-biphenyl]-2-yl)methyl)piperazine dihydrochloride Storage:keep in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/pharma intermediate Transportation

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Benzeneacetamide, a-phenyl-Appearance:Off white to slight yellow solid Storage:Stored in shaded, cool and dry places Package:1L 5L 10L 25L bottle Application:pharma intermediate Transportation:Handle with cares to avoid damaging the packages. Protect

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Synthetic route

: 117-34-0
2,2-diphenylacetic acid

: 4695-13-0
2,2-diphenylacetamide

Conditions

Conditions	Yield
With pyridine; di-tert-butyl dicarbonate; ammonium bicarbonate In 1,4-dioxane at 20℃; for 12h;	95%
With magnesium(II) nitrate hexahydrate; urea In octane at 120℃; for 24h; Reagent/catalyst;	92%
Stage #1: 2,2-diphenylacetic acid With thionyl chloride In tetrahydrofuran at 50℃; for 1h; Stage #2: With ammonium hydroxide In tetrahydrofuran at 0℃; for 0.0833333h;	86%

: 86-29-3
Diphenylacetonitrile

: 4695-13-0
2,2-diphenylacetamide

Conditions

Conditions	Yield
With sodium hydroxide; poly(ethylene glycol)-400 for 0.025h; microwave irradiation;	94%
With tetra(n-butyl)ammonium hydroxide In ethanol; water at 80℃; for 12h; Green chemistry; chemoselective reaction;	92%
With Os(hydride)6(triisopropylphosphine)2; water In tetrahydrofuran-d8 at 100℃; for 4h; Inert atmosphere;	79%

: 182318-00-9
1-(1H-benzo[d][1,2,3]triazol-1-yl)-2,2-diphenylethan-1-one

: 4695-13-0
2,2-diphenylacetamide

Conditions

Conditions	Yield
With ammonium hydroxide In tetrahydrofuran; ethanol at 20℃; for 4h;	90%

: 1309976-99-5
C19H21N3O

: 4695-13-0
2,2-diphenylacetamide

Conditions

Conditions	Yield
With lithium aluminium tetrahydride In tetrahydrofuran at 0℃; for 0.166667h;	85%
With lithium aluminium tetrahydride In tetrahydrofuran at 0℃; for 0.166667h;	85%

: 1871-76-7
diphenylacetic acid chloride

: 4695-13-0
2,2-diphenylacetamide

Conditions

Conditions	Yield
With ammonia In methanol at 55℃; for 0.5h;	80%
With diethyl ether; ammonia
With ammonia

: 97320-51-9
2-diphenylmethyleneoxazolidine-4,5-dione

: 4695-13-0
2,2-diphenylacetamide

Conditions

Conditions	Yield
With phosphorous acid trimethyl ester In benzene for 8h; Heating;	80%

: 626-34-6
ethyl 3-aminobut-2-enoate

: 3469-17-8
2-diazo-1,2-diphenylethan-1-one

A: 4695-13-0
2,2-diphenylacetamide

B: 128999-98-4
(Z)-3-Amino-2-diphenylacetyl-but-2-enoic acid ethyl ester

C: 129000-01-7
(Z)-3-Diphenylacetylamino-but-2-enoic acid ethyl ester

Conditions

Conditions	Yield
In dichloromethane for 168h; Ambient temperature;	A 23% B 42% C 16%

...Expand

: 1118-66-7
4-Aminopent-3-en-2-one

: 3469-17-8
2-diazo-1,2-diphenylethan-1-one

A: 4695-13-0
2,2-diphenylacetamide

B: 128999-95-1
3-[1-Amino-eth-(E)-ylidene]-1,1-diphenyl-pentane-2,4-dione

Conditions

Conditions	Yield
In dichloromethane for 168h; Mechanism; Ambient temperature; other primary and secondary enaminones;	A 10% B 40%
In dichloromethane for 168h; Ambient temperature;	A 10% B 40%
In dichloromethane for 168h; Ambient temperature;	A 10% B 10%

...Expand

: 5344-88-7
benzil monohydrazone

A: 4695-13-0
2,2-diphenylacetamide

B: 3893-33-2
benzil monoazine

C: 78813-05-5
benzil-mono-benzhydrylidenehydrazone

D: 4057-61-8
3,4-diphenyl-1,2,5-thiadiazole

Conditions

Conditions	Yield
With tetrasulphur tetranitride In toluene for 24h; Heating;	A 3% B 5% C 20% D 8%
With tetrasulphur tetranitride In toluene for 24h; Mechanism; Heating;	A 3% B 5% C 20% D 8%

...Expand

: 530-48-3
1,1-Diphenylethylene

: 4695-13-0
2,2-diphenylacetamide

Conditions

Conditions	Yield
With pyridine; ammonium hydroxide; sulfur at 230℃;
Multi-step reaction with 3 steps 1: glacial acetic acid; concentrated nitric acid 2: hydrochloride of tin dichloride; alcohol 3: KOH; alcohol View Scheme

: 64-17-5
ethanol

: 43002-68-2
2,2-diphenyl-acetimidic acid ethyl ester; hydrochloride

A: 4695-13-0
2,2-diphenylacetamide

B: 3468-99-3
ethyl diphenylacetate

C: 86-29-3
Diphenylacetonitrile

...Expand

: 10425-22-6
Benzil dicyanohydrin

: 4695-13-0
2,2-diphenylacetamide

Conditions

Conditions	Yield
With sulfuric acid

: 43002-68-2
2,2-diphenyl-acetimidic acid ethyl ester; hydrochloride

A: 75-00-3
chloroethane

B: 4695-13-0
2,2-diphenylacetamide

Conditions

Conditions	Yield
at 128 - 130℃;

: 525-06-4
diphenyl ketene

: 4695-13-0
2,2-diphenylacetamide

Conditions

Conditions	Yield
With diethyl ether; ammonia

: 117-34-0
2,2-diphenylacetic acid

: 17356-08-0
thiourea

: 4695-13-0
2,2-diphenylacetamide

: 117-34-0
2,2-diphenylacetic acid

: 57-13-6
urea

: 4695-13-0
2,2-diphenylacetamide

: 97080-43-8
diethyl 2,2-diphenylmalonate

: 141-52-6
sodium ethanolate

: 57-13-6
urea

A: 4695-13-0
2,2-diphenylacetamide

B: 117-34-0
2,2-diphenylacetic acid

Conditions

Conditions	Yield
at 106 - 108℃; unter Druck;

...Expand

: 3469-17-8
2-diazo-1,2-diphenylethan-1-one

: 4695-13-0
2,2-diphenylacetamide

Conditions

Conditions	Yield
With hydrogen sulfide; ammonia
With ammonia for 2h; Heating;	4.81 g

: 525-06-4
diphenyl ketene

A: 4695-13-0
2,2-diphenylacetamide

B: 117-34-0
2,2-diphenylacetic acid

Conditions

Conditions	Yield
With ammonia; water at 25℃; Mechanism; bimolecular rate constants of reaction of diphenylketene with var. bases; other bases;

: N-Methoxy-2,2-diphenyl-acetamide

: 4695-13-0
2,2-diphenylacetamide

Conditions

Conditions	Yield
With titanium(III) chloride; air 1) H2O, EtOH, 0.5 h, 40 deg C; Yield given. Multistep reaction;

: 24037-64-7
2-Benzoyl-2.2-diphenyl-acetamid

: 4695-13-0
2,2-diphenylacetamide

Conditions

Conditions	Yield
With potassium hydroxide In methanol

: 19962-73-3
4,4-diphenyl-[1,3]oxathiolan-5-one

: ammonium hydroxide

A: 4695-13-0
2,2-diphenylacetamide

B: 117-34-0
2,2-diphenylacetic acid

C: 7783-06-4
hydrogen sulfide

Conditions

Conditions	Yield
at 100℃; im Rohr;

...Expand

: 7664-41-7
ammonia

: 525-06-4
diphenyl ketene

: 4695-13-0
2,2-diphenylacetamide

: 110-86-1
pyridine

: 530-48-3
1,1-Diphenylethylene

: 7664-41-7
ammonia

sulfur: sulfur

: 4695-13-0
2,2-diphenylacetamide

Conditions

Conditions	Yield
at 230℃;

...Expand

etheric α-diazo-deoxybenzoin: etheric α-diazo-deoxybenzoin

: 4695-13-0
2,2-diphenylacetamide

Conditions

Conditions	Yield
With ammonium hydroxide; silver nitrate

: 110-86-1
pyridine

: 599-67-7
1,1-diphenylethanol

: 7664-41-7
ammonia

sulfur: sulfur

: 4695-13-0
2,2-diphenylacetamide

Conditions

Conditions	Yield
at 210℃;

...Expand

: 693-65-2
dipentyl ether

: 4746-87-6
benzilamide

: 7553-56-2
iodine

: 6749-78-6
4-methylphenylmagnesium iodide

: 4695-13-0
2,2-diphenylacetamide

...Expand

: 7664-93-9
sulfuric acid

: 10425-22-6
Benzil dicyanohydrin

: 4695-13-0
2,2-diphenylacetamide

: 86-29-3
Diphenylacetonitrile

A: 4695-13-0
2,2-diphenylacetamide

B: 117-34-0
2,2-diphenylacetic acid

Conditions

Conditions	Yield
With PEG-400; sodium hydroxide; water microwave irradiation;

: 4695-13-0
2,2-diphenylacetamide

: 2154-71-4
bis-trifluoromethyl-aminooxyl

: α-(bistrifluoromethylamino-oxy)diphenylacetamide

Conditions

Conditions	Yield
In tetrachloromethane for 15h; Ambient temperature;	100%

: 4695-13-0
2,2-diphenylacetamide

: 86-29-3
Diphenylacetonitrile

Conditions

Conditions	Yield
With copper diacetate; 1,2-bis-(dicyclohexylphosphino)ethane In tetrahydrofuran at 20℃; for 12h; Catalytic behavior; Mechanism; Reagent/catalyst; Solvent; Temperature; Inert atmosphere;	99%
With bis(trichloromethyl) carbonate; triethylamine In chloroform at 50℃; for 2h;	87%
With palladium diacetate; Selectfluor; acetonitrile at 20℃; for 18h;	84%

: 4695-13-0
2,2-diphenylacetamide

: 119-61-9
benzophenone

Conditions

Conditions	Yield
With tetraethylammonium bromide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In acetonitrile at 20 - 60℃;	96%
Multi-step reaction with 2 steps 1: phosphorus pentachloride; phosphorus oxychloride 2: nickel; acetic acid ester; aqueous alcohol / Hydrogenation View Scheme

: 4695-13-0
2,2-diphenylacetamide

: 117-34-0
2,2-diphenylacetic acid

Conditions

Conditions	Yield
With titanium tetrachloride In 1,4-dioxane; water for 24h; Heating;	92%

: 4695-13-0
2,2-diphenylacetamide

: 3963-62-0
2,2-Diphenylethylamine

Conditions

Conditions	Yield
With lithium aluminium tetrahydride In diethyl ether at 20℃; for 4h;	91%
Multi-step reaction with 2 steps 1: thionyl chloride 2: Raney nickel; ethanol; liquid ammonia / 100 °C / 117681 Torr / Hydrogenation View Scheme
Multi-step reaction with 2 steps 1: phosphorus pentachloride; phosphorus oxychloride 2: nickel; alcohol; acetic acid ester / Hydrogenation.Reagens: Wasser View Scheme

: 302-17-0
chloral hydrate

: 4695-13-0
2,2-diphenylacetamide

: 924637-59-2
2,2-diphenyl-N-(2,2,2-trichloro-1-hydroxy-ethyl)-acetamide

Conditions

Conditions	Yield
In benzene for 12h; Heating / reflux;	91%

: 4695-13-0
2,2-diphenylacetamide

: 433-27-2
Trifluoroacetaldehyde ethyl hemiacetal

: 924637-61-6
2,2-diphenyl-N-(2,2,2-trifluoro-1-hydroxy-ethyl)-acetamide

Conditions

Conditions	Yield
In 1,4-dioxane for 48h; Heating / reflux;	91%

: 67-56-1
methanol

: 4695-13-0
2,2-diphenylacetamide

: 3469-00-9
methyl 2,2-diphenylacetate

Conditions

Conditions	Yield
With potassium hydrogensulfate at 65℃; for 48h;	88%

: 4695-13-0
2,2-diphenylacetamide

: 100-46-9
benzylamine

: 5022-26-4
N-benzyl-2,2-diphenylacetamide

Conditions

Conditions	Yield
With Ce(III) immobilised on an aminated epichlorohydrin-activated agarose matrix at 140℃; for 22h; Green chemistry;	80%

: 4695-13-0
2,2-diphenylacetamide

: 17518-50-2
2,2-diphenylthioacetamide

Conditions

Conditions	Yield
With tetraphosphorus decasulfide In dichloromethane at 20℃; for 4h;	71%

: 4695-13-0
2,2-diphenylacetamide

: 144-62-7
oxalic acid

A: 91-01-0
1,1-Diphenylmethanol

B: C14H15NO*C2H2O4

Conditions

Conditions	Yield
Stage #1: 2,2-diphenylacetamide With oxygen; sodium bis(2-methoxyethoxy)aluminium dihydride In tetrahydrofuran; toluene at 0 - 25℃; under 760.051 Torr; for 3h; Stage #2: oxalic acid In methanol; diethyl ether	A 53% B 26%

...Expand

: 64-17-5
ethanol

: 4695-13-0
2,2-diphenylacetamide

: 3468-99-3
ethyl diphenylacetate

Conditions

Conditions	Yield
With hydrogenchloride; titanium tetrachloride for 40h; Heating;	52%

: 4695-13-0
2,2-diphenylacetamide

: 103-71-9
phenyl isocyanate

: 1-Diphenylacetyl-3-phenyl-urea

Conditions

Conditions	Yield
In 1,4-dioxane for 2h; Heating;	26.9%

: 4695-13-0
2,2-diphenylacetamide

: 67402-86-2
3,3-dimethylglutardialdehyde

: 115932-92-8
1-diphenylacetyl-1,4-dihydro-4,4-dimethylpyridine

Conditions

Conditions	Yield
With toluene-4-sulfonic acid In benzene for 3h; Heating;	26%

: 1871-76-7
diphenylacetic acid chloride

: 4695-13-0
2,2-diphenylacetamide

: tris-diphenylacetyl-amine

Conditions

Conditions	Yield
With pyridine

: 79-37-8
oxalyl dichloride

: 4695-13-0
2,2-diphenylacetamide

: 97320-51-9
2-diphenylmethyleneoxazolidine-4,5-dione

: 60-29-7
diethyl ether

: 4695-13-0
2,2-diphenylacetamide

: 925-90-6
ethylmagnesium bromide

: 6336-52-3
1,1-diphenylbutan-2-one

...Expand

: 4695-13-0
2,2-diphenylacetamide

: 925-90-6
ethylmagnesium bromide

: 6336-52-3
1,1-diphenylbutan-2-one

Conditions

Conditions	Yield
With diethyl ether

: 4695-13-0
2,2-diphenylacetamide

: 141-52-6
sodium ethanolate

: 5457-53-4
Benzhydryl-carbamidsaeure-ethylester

Conditions

Conditions	Yield
With ethanol; bromine

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Risk Statements	22
Safety Statements	22-36/37
RTECS	AB8135000

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