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Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
superior quality moderate price & quick delivery Appearance:yellow to brown-yellow powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Us
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A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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6-Nitroindole from China CAS NO.4769-96-4Appearance:detailed see specifications Storage:Store in dry, dark and ventilated place. Package:according to customers' requirements Application:It is an important raw material and intermediates used in Organi
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inquiry6-Nitroindole, 96%; 6-Nitroindole, 96% 1GR; 1H-Indole, 6-nitro-; 6-NITRO-1H-INDOLE; 6-NITROINDOLE; 6-NITROINDLE; 6-Nitroindole, 97% CAS No.: 4769-96-4 Molecular formula: C8H6N2O2 Molecular weight: 162.15 6-nitroguanidine Melting point
Product name: 6-Nitroindole CAS No.:4769-96-4 Molecule Formula:C8H6N2O2 Molecule Weight:162.15 Purity: 99.0% Package: 25kg/drum Description:Yellow crystalline powder Manufacture Standards:Enterprise Standard TESTIN
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inquiryProduct Name: 6-Nitroindole Synonyms: 6-Nitroindole,96%;6-Nitroindole, 96% 1GR;1H-Indole, 6-nitro-;6-NITROINDLE;6-Nitroindole,97%;6-NITRO-1H-INDOLE;6-NITROINDOLE;6-Nitroindole in stock Factory CAS: 4769-96-4 MF: C8H6N2O2 MW: 162.15 EIN
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
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Shanghai Lonwin Chemical company is a subsidiary of Lonwin Industry Group Limited, was established in 2011 and is headquartered in Shanghai, adjacent to China National Convention and Exhibition Center and Hongqiao transportation hub.Lonwinchem is
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Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
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inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as
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6-nitroindoline
6-nitroindole
Conditions | Yield |
---|---|
With oxygen; salcomine In methanol at 25℃; for 5h; | 92% |
With manganese(IV) oxide In dichloromethane at 0 - 20℃; for 12h; Inert atmosphere; | 92% |
With isolated cobalt single atom sites stabilized on an ordered porous nitrogen doped carbon matrix In 1,3,5-trimethyl-benzene at 120℃; for 8h; Schlenk technique; | 92% |
6-nitroindole
Conditions | Yield |
---|---|
In ethylene glycol at 170℃; Retro Diels-Alder reaction; Inert atmosphere; | 92% |
2-ethynyl-5-nitroaniline
6-nitroindole
Conditions | Yield |
---|---|
With [cyclopentadienylruthenium(II) bis-(2-diphenylphosphino-6-t-butylpyridine)(acetonitrile)]hexafluorophosphate In tetrahydrofuran-d8 at 70℃; for 2h; Sealed tube; | 92% |
Conditions | Yield |
---|---|
With sodium tungstate; dihydrogen peroxide In methanol; water at 20℃; for 7h; | A 7% B 79% |
6-nitroindole
Conditions | Yield |
---|---|
With Amberlyst 15 In 2-methyltetrahydrofuran at 100℃; for 0.75h; Microwave irradiation; | 70% |
Conditions | Yield |
---|---|
In methanol; N,N-dimethyl-formamide for 0.0833333h; Heating; | A 57% B 22% C 6% |
Conditions | Yield |
---|---|
In water; N,N-dimethyl-formamide for 1h; Heating; | A 54% B 13% |
2,4-dinitrotoluene
N,N-dimethyl-formamide dimethyl acetal
6-nitroindole
Conditions | Yield |
---|---|
Stage #1: 2,4-dinitrotoluene; N,N-dimethyl-formamide dimethyl acetal With pyrrolidine In 1,4-dioxane at 102℃; for 5h; Leimgruber-Batcho Indole Synthesis; Reflux; Inert atmosphere; Stage #2: With hydrazine hydrate In 1,4-dioxane at 45℃; for 1h; Leimgruber-Batcho Indole Synthesis; | 52% |
diethyl malonate
1-methoxy-6-nitroindole
A
6-nitroindole
B
diethyl 2-(6-nitroindol-3-yl)methylmalonate
Conditions | Yield |
---|---|
With potassium hydride In N,N-dimethyl-formamide for 0.0833333h; Heating; | A 20% B 40% C 5% |
Conditions | Yield |
---|---|
In water; N,N-dimethyl-formamide for 1h; Heating; | A 4% B 15% |
6-Nitro-1H-indole-2-carboxylic Acid
6-nitroindole
Conditions | Yield |
---|---|
With quinoline; copper(II) oxide |
6-nitro-1H-indole-3-carboxylic acid
6-nitroindole
Conditions | Yield |
---|---|
With quinoline at 180℃; |
N-chloromethylsulfonyl-6-nitroindoline
6-nitroindole
Conditions | Yield |
---|---|
With sodium hydroxide In dimethyl sulfoxide at 20 - 25℃; for 0.5h; |
acetaldehyde-(3-nitro-phenylhydrazone)
A
6-nitroindole
B
4-nitro-1H-indoIe
Conditions | Yield |
---|---|
GIPKh-115 In acetonitrile at 200 - 320℃; (g) phase; | |
GIPKh-115 In acetonitrile at 180 - 320℃; (g) phase. Object of study: effect of electronic factors; |
1-hydroxy-6-introindole
6-nitroindole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 96 percent / methanol / 20 °C 2: 4 percent / dimethylformamide; H2O / 1 h / Heating View Scheme | |
Multi-step reaction with 2 steps 1: 96 percent / methanol / 20 °C 2: 57 percent / dimethylformamide; methanol / 0.08 h / Heating View Scheme | |
Multi-step reaction with 2 steps 1: 96 percent / methanol / 20 °C 2: 20 percent / KH (35 percent in mineral oil) / dimethylformamide / 0.08 h / Heating View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: concentrated sulfuric acid; nitric acid / <5 2: maleic acid-anhydride; palladium; water View Scheme | |
Multi-step reaction with 2 steps 1: concentrated sulfuric acid; nitric acid / <5 2: tetrachloro-<1,4>benzoquinone; xylene View Scheme | |
Multi-step reaction with 2 steps 1: nitric acid; sulfuric acid / 0 - 20 °C 2: manganese(IV) oxide / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1: nitric acid; sulfuric acid / 0 - 20 °C 2: manganese(IV) oxide / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: acetic acid; HNO3 2: aqueous KOH 3: quinoline / 180 °C View Scheme |
6-nitro-1H-indole-2-carboxylic acid ethyl ester
6-nitroindole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aq.-ethanolic KOH 2: copper (II)-oxide; quinoline View Scheme |
6-nitro-indole-3-carboxylic acid ethyl ester
6-nitroindole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aqueous KOH 2: quinoline / 180 °C View Scheme |
ethyl 2-[2-(3-nitrophenyl)hydrazinylidene]propanoate
6-nitroindole
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: polyphosphoric acid 2: aq.-ethanolic KOH 3: copper (II)-oxide; quinoline View Scheme |
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In ethyl acetate under 2587.7 Torr; | 100% |
100% | |
With silver tetrafluoroborate; 4,4'-Dimethoxy-2,2'-bipyridin; potassium tert-butylate; hydrogen In 1,4-dioxane at 80℃; under 30003 Torr; for 48h; Autoclave; | 94% |
Conditions | Yield |
---|---|
Stage #1: 6-nitroindole With sodium hydride In N,N-dimethyl-formamide for 0.166667h; Stage #2: methyl iodide In N,N-dimethyl-formamide at 0℃; | 100% |
Stage #1: 6-nitroindole With sodium hydride In N,N-dimethyl-formamide for 0.166667h; Stage #2: methyl iodide In N,N-dimethyl-formamide at 20℃; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; | 98% |
6-nitroindole
p-toluenesulfonyl chloride
N-[4-(methylphenyl)sulfonyl]-6-nitro-1H-indole
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide | 99% |
6-nitroindole
(2-trimethylethylsilylethoxy)methyl chloride
6-nitro-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-indole
Conditions | Yield |
---|---|
Stage #1: 6-nitroindole With sodium hydride In tetrahydrofuran; mineral oil for 0.5h; Inert atmosphere; Stage #2: (2-trimethylethylsilylethoxy)methyl chloride In tetrahydrofuran; mineral oil at 20℃; for 16h; Inert atmosphere; | 98.7% |
Stage #1: 6-nitroindole With potassium hydroxide In N,N-dimethyl-formamide at 0℃; for 0.25h; Stage #2: (2-trimethylethylsilylethoxy)methyl chloride In N,N-dimethyl-formamide at 0℃; for 10h; | 38% |
6-nitroindole
t-butyl 4-bromomethyl-3-methoxybenzoate
tert-butyl 3-methoxy-4-<(6-nitroindol-1-yl)methyl>benzoate
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 48h; Heating; | 98% |
6-nitroindole
1-chloro 4-iodobutane
1-(4-chlorobutyl)-6-nitro-1H-indole
Conditions | Yield |
---|---|
Stage #1: 6-nitroindole With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; for 0.0833333h; Stage #2: 1-chloro 4-iodobutane In N,N-dimethyl-formamide at 20℃; for 0.5h; | 97.6% |
With sodium hydride In N,N-dimethyl-formamide |
6-nitroindole
ethyl bromoacetate
(6-nitro-indol-1-yl)-acetic acid ethyl ester
Conditions | Yield |
---|---|
Stage #1: 6-nitroindole With sodium hydride In N,N-dimethyl-formamide for 0.416667h; Stage #2: ethyl bromoacetate In N,N-dimethyl-formamide at 20℃; for 26h; | 97% |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 36h; | 88% |
Stage #1: 6-nitroindole With sodium hydride In N,N-dimethyl-formamide at 0 - 25℃; Stage #2: ethyl bromoacetate In N,N-dimethyl-formamide at 0 - 25℃; Product distribution / selectivity; | 57% |
6-nitroindole
1-methyl-6-nitro-indole
Conditions | Yield |
---|---|
With CH3I; NaH In dimethylformamide [DMF]; water | 97% |
With potassium carbonate; methyl iodide In N,N-dimethyl-formamide |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide for 12h; Inert atmosphere; Reflux; | 97% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 126℃; for 2h; Concentration; Reflux; Green chemistry; | 96% |
With potassium carbonate In n-heptane; water; ethyl acetate; N,N-dimethyl-formamide | 96.1% |
6-nitroindole
trifluoroacetic anhydride
2,2,2-trifluoro-1-(6-nitro-1H-indol-3-yl)-ethanone
Conditions | Yield |
---|---|
Stage #1: 6-nitroindole; trifluoroacetic anhydride In N,N-dimethyl-formamide at 60℃; for 3h; Stage #2: With water; sodium hydrogencarbonate In ethyl acetate; N,N-dimethyl-formamide | 96% |
In tetrahydrofuran at 0 - 25℃; for 18h; | 40% |
6-nitroindole
benzenesulfonyl chloride
6-nitro-1-(phenylsulfonyl)-1H-indole
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 0 - 20℃; for 24h; | 96% |
Stage #1: 6-nitroindole With sodium hydride In tetrahydrofuran; mineral oil at 20℃; for 1h; Inert atmosphere; Stage #2: benzenesulfonyl chloride In tetrahydrofuran; mineral oil for 1h; Inert atmosphere; | 77% |
6-nitroindole
methyl 4-(bromomethyl)-3-methoxybenzoate
methyl 3-methoxy-4-<(6-nitroindol-1-yl)methyl>benzoate
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 48h; Heating; | 95% |
With potassium carbonate In N,N-dimethyl-formamide for 12h; Inert atmosphere; Reflux; | 38% |
With potassium carbonate In dichloromethane; ethyl acetate; acetone |
Conditions | Yield |
---|---|
With copper(l) iodide; metformin hydrochloride; caesium carbonate In N,N-dimethyl-formamide at 130℃; for 6h; Inert atmosphere; | 95% |
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; | 95% |
Conditions | Yield |
---|---|
With 4,4'-sulfonediphenol In acetic acid butyl ester at 80℃; for 2h; Friedel-Crafts Alkylation; Sealed tube; Green chemistry; | 95% |
Conditions | Yield |
---|---|
Stage #1: 6-nitroindole With sodium hydride In N,N-dimethyl-formamide; mineral oil at 20℃; for 0.666667h; Stage #2: ethyl bromide With sodium iodide In N,N-dimethyl-formamide; mineral oil | 94.5% |
6-nitroindole
1-bromomethyl-3,5-difluoro-benzene
1-(3,5-difluoro-benzyl)-6-nitro-1H-indole
Conditions | Yield |
---|---|
Stage #1: 6-nitroindole With sodium hydride In DMF (N,N-dimethyl-formamide) at 20℃; for 0.25h; Stage #2: 1-bromomethyl-3,5-difluoro-benzene In DMF (N,N-dimethyl-formamide) | 94% |
Stage #1: 6-nitroindole With 1-methyl-pyrrolidin-2-one; cesium carbonate at 0℃; for 0.5h; Stage #2: 1-bromomethyl-3,5-difluoro-benzene at 20℃; for 18h; | |
Stage #1: 6-nitroindole With sodium hydride In DMF (N,N-dimethyl-formamide) for 0.5h; Stage #2: 1-bromomethyl-3,5-difluoro-benzene In DMF (N,N-dimethyl-formamide) for 1h; |
Conditions | Yield |
---|---|
In water at 80℃; for 24h; Friedel-Crafts reaction; | 93% |
cyclopropyl trifluoromethyl ketone
6-nitroindole
Conditions | Yield |
---|---|
With caesium carbonate In acetonitrile at 20℃; for 8h; | 93% |
Conditions | Yield |
---|---|
With aluminium(III) chloride hexahydrate; sodium dodecyl-sulfate; silica gel In neat (no solvent) at 20℃; for 0.5h; Milling; Green chemistry; | 93% |
6-nitroindole
Conditions | Yield |
---|---|
In 2,2,2-trifluoroethanol at 40℃; for 12h; Inert atmosphere; Schlenk technique; Sealed tube; | 93% |
Conditions | Yield |
---|---|
With dichloro bis(acetonitrile) palladium(II) In water at 120℃; for 16h; Sealed tube; | 92% |
Conditions | Yield |
---|---|
With Pf0A9 E104G enzyme In aq. phosphate buffer; water; dimethyl sulfoxide at 75℃; for 12h; pH=8; Reagent/catalyst; Enzymatic reaction; | 91% |
Conditions | Yield |
---|---|
With N,N,N,N,-tetramethylethylenediamine; boron trifluoride diethyl etherate; oxygen; copper(II) bis(trifluoromethanesulfonate) In dimethyl sulfoxide at 80℃; for 12h; regioselective reaction; | 91% |
6-nitroindole
4-bromomethyl-3-methoxybenzonitrile
1-(4-cyano-2-methoxybenzyl)-6-nitroindole
Conditions | Yield |
---|---|
With potassium carbonate In acetone Heating; | 90% |
6-nitroindole
1-iodo-3-chloro-propane
1-(3-chloropropyl)-6-nitro-1H-indole
Conditions | Yield |
---|---|
Stage #1: 6-nitroindole With sodium hydride In N,N-dimethyl-formamide at 0℃; for 0.25h; Stage #2: 1-iodo-3-chloro-propane In N,N-dimethyl-formamide at 20℃; for 3h; | 90% |
With sodium hydride In N,N-dimethyl-formamide |
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