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inquiryHigh quality and best price of 2-Octyl-1-dodecanol from Henan Tianfu Chemical: Henan Tianfu Chemical Co.,LTD was built in 2009 with an ISO certificate in the past 5 years, we have grown up as a famous fine chemicals supplier in china and we had e
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inquiryProduct Name 2-Octyl-1-dodecanol; octyldodecanol CAS No. 5333-42-6 MF C20H42O Appearance Colorless Liquid Content
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2-Octyl-1-dodecanol Chemical Properties Melting point −1-1 °C(lit.) Boiling point 234-238 °C/33 mmHg(lit.) density 0.838 g/mL at 25 °C(lit.) refractive index n20/D 1.453(lit.) Fp 113 °C solubility Practic
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryConditions | Yield |
---|---|
With sodium hydroxide | 90% |
2-octyldodecan-1-ol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran at 20℃; for 2h; Cooling with ice; | 86% |
Conditions | Yield |
---|---|
With cesium hydroxide; C33H48IIr2N6(1+)*F6P(1-) In toluene at 120℃; for 16h; Guerbet Reaction; Sealed tube; | A 76% B 3% |
Conditions | Yield |
---|---|
With cesium hydroxide; C33H48IIr2N6(1+)*F6P(1-) In toluene at 120℃; for 8h; Reagent/catalyst; Guerbet Reaction; Sealed tube; | 69% |
With dichloro(pentamethylcyclopentadienyl) iridium; potassium tert-butylate; 1,7-Octadiene In para-xylene at 120℃; for 4h; Guerbet reaction; | 43% |
With heptanal; potassium hydroxide at 230 - 245℃; under 760 Torr; for 6h; Guerbet Reaction; Dean-Stark; |
1-Decanol
hexan-1-ol
A
2-(n-butyl)octanol
B
2-hexyldecan-1-ol
C
5-hydroxymethyl-pentadecane
D
2-octyldodecan-1-ol
Conditions | Yield |
---|---|
With potassium hydroxide at 255℃; for 6h; Reagent/catalyst; Dean-Stark; Inert atmosphere; | A 8.4% B n/a C n/a D 39.1% |
Conditions | Yield |
---|---|
With nickel at 220 - 250℃; Hydrogenation; | |
With nickel; decalin at 220 - 250℃; Hydrogenation; | |
With potassium hydroxide; benzyl alcohol |
caprinaldehyde
benzyl alcohol
A
2-octyldodecan-1-ol
B
(±)-2-benzyl-1-decanol
Conditions | Yield |
---|---|
With potassium hydroxide |
Conditions | Yield |
---|---|
at 220 - 250℃; under 36775.4 Torr; Hydrogenation; |
Conditions | Yield |
---|---|
at 220 - 250℃; under 36775.4 Torr; Hydrogenation; |
octanol
1-Decanol
A
2-hexyldecan-1-ol
B
2-octyl-1-decanol
C
2-hexyl-1-dodecanol
D
2-octyldodecan-1-ol
Conditions | Yield |
---|---|
With potassium hydroxide at 190 - 225℃; for 3h; Dean-Stark; Inert atmosphere; Overall yield = 89.4 %; |
Conditions | Yield |
---|---|
Stage #1: 1-Decene; trimethylaluminum With rac-[(C2H4)(η5-C9H10)2]ZrCl2 In toluene at 20℃; for 72h; Inert atmosphere; Stage #2: With oxygen In toluene at 0℃; for 26h; |
1-Decene
triethylaluminum
A
2-ethyldecane-1-ol
B
2-octyldodecan-1-ol
Conditions | Yield |
---|---|
Stage #1: 1-Decene; triethylaluminum With rac-[(C2H4)(η5-C9H10)2]ZrCl2 In dichloromethane at 20℃; for 72h; Inert atmosphere; Stage #2: With oxygen In dichloromethane at 0℃; for 26h; Solvent; |
2-octyldodecan-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: sodium methylate / N,N-dimethyl-formamide / 0.5 h / 80 °C / Large scale 1.2: 2 h / 120 °C / Large scale 2.1: lithium chloride / N,N-dimethyl-formamide; water / 24 h / 160 °C / Large scale 3.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 20 °C / Cooling with ice View Scheme |
2-octyldodecan-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: lithium chloride / N,N-dimethyl-formamide; water / 24 h / 160 °C / Large scale 2: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 20 °C / Cooling with ice View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: sodium methylate / N,N-dimethyl-formamide / 0.5 h / 80 °C / Large scale 1.2: 2 h / 120 °C / Large scale 2.1: sodium methylate / N,N-dimethyl-formamide / 0.5 h / 80 °C / Large scale 2.2: 2 h / 120 °C / Large scale 3.1: lithium chloride / N,N-dimethyl-formamide; water / 24 h / 160 °C / Large scale 4.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 20 °C / Cooling with ice View Scheme |
2-octyldodecan-1-ol
9-(bromomethyl)nonadecane
Conditions | Yield |
---|---|
With N-Bromosuccinimide; triphenylphosphine In dichloromethane at 0 - 20℃; | 99% |
With N-Bromosuccinimide; triphenylphosphine In dichloromethane at 20℃; for 24h; | 98% |
With bromine; triphenylphosphine In dichloromethane at 0 - 20℃; Inert atmosphere; | 97% |
2-octyldodecan-1-ol
2-octyl-dodecanoic acid
Conditions | Yield |
---|---|
With periodic acid; pyridinium chlorochromate In acetonitrile at 0℃; | 99% |
With periodic acid; pyridinium chlorochromate In acetonitrile at 0 - 20℃; | 86% |
With potassium permanganate; sulfuric acid In dichloromethane; water for 4h; | 74% |
Conditions | Yield |
---|---|
With p-toluenesulfonic acid monohydrate | 99% |
Conditions | Yield |
---|---|
With p-toluenesulfonic acid monohydrate | 98% |
5-bromothiophene-2-carboxylic acid
2-octyldodecan-1-ol
2-octyl-dodecyl 5-bromothiophene-2-carboxylate
Conditions | Yield |
---|---|
With 4-(dimethylamino)pyridinium tosylate; diisopropyl-carbodiimide In dichloromethane at 20℃; | 97% |
Conditions | Yield |
---|---|
With (1S)-10-camphorsulfonic acid at 60℃; for 24h; | 97% |
2-octyldodecan-1-ol
9-(iodomethyl)nonadecane
Conditions | Yield |
---|---|
With 1H-imidazole; iodine; triphenylphosphine In dichloromethane at 0 - 20℃; for 2.25h; | 97% |
Stage #1: 2-octyldodecan-1-ol With 1H-imidazole; triphenylphosphine In dichloromethane at 0℃; Inert atmosphere; Stage #2: With iodine In dichloromethane at 0 - 20℃; for 2h; Inert atmosphere; | 93% |
With phosphoric acid; hydrogen iodide at 130℃; Inert atmosphere; | 91% |
2-octyldodecan-1-ol
2-decyltetradecanoic acid
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid at 80 - 83℃; for 24h; | 96% |
Conditions | Yield |
---|---|
Stage #1: 2-octyldodecan-1-ol With sodium hydride In N,N-dimethyl-formamide; paraffin oil at 0℃; for 1h; Stage #2: 5,6-difluorobenzo[c]1,2,5thiadiazole In N,N-dimethyl-formamide; paraffin oil at 20℃; for 12h; | 95% |
Conditions | Yield |
---|---|
With p-toluenesulfonic acid monohydrate | 95% |
With toluene-4-sulfonic acid at 20 - 100℃; for 18h; |
2-octyldodecan-1-ol
2-octydodecyl aldehyde
Conditions | Yield |
---|---|
With pyridinium chlorochromate In dichloromethane at 27℃; for 3h; | 94% |
With magnesium sulfate; pyridinium chlorochromate In dichloromethane | 92% |
With silica gel; pyridinium chlorochromate In dichloromethane at 20℃; | 90.8% |
2-octyldodecan-1-ol
2-[2-(2-methoxyethoxy)etoxy]acetic acid
Conditions | Yield |
---|---|
With p-toluenesulfonic acid monohydrate | 94% |
succinic acid anhydride
2-octyldodecan-1-ol
4-(2-octyldodecyloxy)-4-oxobutanoic acid
Conditions | Yield |
---|---|
With pyridine In toluene for 5h; Reflux; | 93% |
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 12h; Inert atmosphere; | 92% |
2-octyldodecan-1-ol
Conditions | Yield |
---|---|
With potassium 2-(difluoro(trifluoromethoxy)methoxy)-2,2-difluoroacetate; tetramethylammonium fluoride at 150℃; for 5h; Glovebox; Inert atmosphere; Schlenk technique; Sealed tube; | 92% |
With potassium 2-(difluoro(trifluoromethoxy)methoxy)-2,2-difluoroacetate; tetramethylammonium fluoride at 150℃; for 5h; Schlenk technique; Glovebox; Inert atmosphere; | 92% |
Conditions | Yield |
---|---|
With pyridine at 0 - 20℃; for 3h; Inert atmosphere; | 90% |
With pyridine In dichloromethane at 0 - 20℃; | 87% |
With pyridine at 20℃; for 3h; | 83% |
With pyridine In dichloromethane at 20℃; for 48h; Cooling with ice; | 80% |
With pyridine at -10℃; for 6h; | 74% |
2-octyldodecan-1-ol
Conditions | Yield |
---|---|
With hydrogenchloride In dichloromethane at 20℃; for 36h; | 89.7% |
2-octyldodecan-1-ol
Conditions | Yield |
---|---|
With titanium(IV) acetylacetone In toluene for 40h; Reflux; | 88% |
With dmap; oxo[hexa(trifluoroacetato)]tetrazinc In toluene at 100℃; Inert atmosphere; Molecular sieve; Schlenk technique; Sealed tube; | 83.8% |
2-octyldodecan-1-ol
4,7-dibromo-5,6-difluorobenzo[c]1,2,5thiadiazole
Conditions | Yield |
---|---|
With potassium tert-butylate In tetrahydrofuran Inert atmosphere; Reflux; | 87% |
2-octyldodecan-1-ol
Conditions | Yield |
---|---|
tin(II) trifluoromethanesulfonate at 180℃; | 86.8% |
Conditions | Yield |
---|---|
With pentafluorophenylboronic acid In nitromethane at 40℃; for 6h; Ferrier Carbohydrate Rearrangement; stereoselective reaction; | 86% |
2-octyldodecan-1-ol
Conditions | Yield |
---|---|
With diphenyl phosphoryl azide; triethylamine at 90℃; Curtius Rearrangement; Inert atmosphere; | 85% |
N-(1-oxododecyl)alanine
2-octyldodecan-1-ol
Conditions | Yield |
---|---|
With sodium bicarbonate; magnesium sulfate; toluene-4-sulfonic acid | 82% |
Conditions | Yield |
---|---|
Stage #1: 2-octyldodecan-1-ol; C30H36N2O6 In dichloromethane; N,N-dimethyl-formamide at 0℃; for 0.25h; Stage #2: With 1,2-dichloro-ethane In dichloromethane; N,N-dimethyl-formamide at 20℃; for 24h; | 78% |
2-octyldodecan-1-ol
4-bromomethylbenzoic Acid
(2-octyldodecyl) 4-bromomethylbenzoate
Conditions | Yield |
---|---|
With 4-(dimethylamino)pyridinium tosylate; diisopropyl-carbodiimide In dichloromethane at 20℃; | 76% |
2-bromothiophene-4-carboxylic acid
2-octyldodecan-1-ol
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 24h; Inert atmosphere; | 76% |
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