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inquiryProduct Name: 5-Acetylindole Synonyms: Ethanone, 1-(1H-indol-5-yl)- (9CI);5-ACETYLINDOLE 97+%;1-(1H-Indol-5-yl)ethan-1-one;Ethanone, 1-(1H-indol-5-yl)-;1-(1H-Indol-5-yl)ethan-1-one, 5-Ethanoyl-1H-indole;Acetyl-5-indole [French];ketone,
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
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inquiryWe are committed to providing our customers with the best products and services at the most competitive prices.Appearance:White to beige crystals Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use a
5-Acetylindole cas 53330-94-2Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiryfactory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
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inquiry1. Subsidiary of Institute of Chemistry, Henan Academy of Sciences, national research platform;2. About 30 years’ experience in this field since 1983;3. An experienced R&D team consisting of Doctors and Masters;4. Various types of analytical instrume
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inquiryCompound sourcing ServicesAgency of testing serviceFactory audit serviceFounded in Dec. 1999, Nanjing Chemlin Chemical Industrial Co.,Ltd(CHEMLIN) has been covering the business scope from trading of chemicals to custom-synthesis & Manufacturing. Co
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inquiry1-(4-amino-3-ethynylphenyl)ethanone
1-(1H-indol-5-yl)ethanone
Conditions | Yield |
---|---|
With P(p-C6H4F)3; chloro(1,5-cyclooctadiene)rhodium(I) dimer In N,N-dimethyl-formamide at 85℃; for 2h; | 93% |
5-Acetyl-2,3-dihydro-1H-indole
1-(1H-indol-5-yl)ethanone
Conditions | Yield |
---|---|
With acetone for 70h; Irradiation; | 90% |
With rhodium(III) chloride hydrate; C13H19N4(1+)*Br(1-) In toluene at 110℃; for 24h; Schlenk technique; Inert atmosphere; | 85% |
With oxygen; 1-(2,2-diphenyl-2λ4,3λ4-[1,3,2]diazaborolo[4,5,1-ij]quinolin-1(2H)-yl)-3-phenylpropan-1-one In 1-methyl-pyrrolidin-2-one at 20℃; for 5h; Irradiation; Green chemistry; | 74% |
With chloranil; xylene | |
With chloranil |
Conditions | Yield |
---|---|
In tetrahydrofuran at 0℃; for 12h; Inert atmosphere; | 87.97% |
In tetrahydrofuran at 0 - 20℃; | 80% |
In tetrahydrofuran; diethyl ether at 0 - 20℃; Inert atmosphere; | 72.9% |
5-acetylindole-3-carboxylic acid
1-(1H-indol-5-yl)ethanone
Conditions | Yield |
---|---|
With quinoline; 5-acetylindole-3-carboxylic acid cupric(II) salt at 155℃; for 2h; | 86% |
5-ethynyl-1H-indole
1-(1H-indol-5-yl)ethanone
Conditions | Yield |
---|---|
With 4-cyanobenzaldehyde oxime; bis-[(trifluoroacetoxy)iodo]benzene In methanol; water at 20℃; | 84% |
Conditions | Yield |
---|---|
With tert.-butyl lithium; potassium hydride Yield given. Multistep reaction; |
indole
acetyl chloride
N,N-dimethyl-formamide
A
1-(1H-indol-5-yl)ethanone
B
1-(1H-indol-6-yl)ethan-1-one
Conditions | Yield |
---|---|
Yield given. Multistep reaction. Yields of byproduct given; |
C11H14SiNCH3CO
1-(1H-indol-5-yl)ethanone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: potassium carbonate / methanol / 25 °C 2: 93 percent / tris(4-fluorophenyl)phosphine / [Rh(COD)Cl]2 / dimethylformamide / 2 h / 85 °C View Scheme |
4-Aminoacetophenone
1-(1H-indol-5-yl)ethanone
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: benzyltrimethylammonium iodine dichloride; CaCO3 / CH2Cl2; methanol / 25 °C 2: CuI; diethylamine / PdCl2(PPh3)2 / 25 °C 3: potassium carbonate / methanol / 25 °C 4: 93 percent / tris(4-fluorophenyl)phosphine / [Rh(COD)Cl]2 / dimethylformamide / 2 h / 85 °C View Scheme |
4-acetyl-2-iodoaniline
1-(1H-indol-5-yl)ethanone
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: CuI; diethylamine / PdCl2(PPh3)2 / 25 °C 2: potassium carbonate / methanol / 25 °C 3: 93 percent / tris(4-fluorophenyl)phosphine / [Rh(COD)Cl]2 / dimethylformamide / 2 h / 85 °C View Scheme |
2,2,2-trifluoro-1-(1H-indol-3-yl)ethanone
1-(1H-indol-5-yl)ethanone
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 62 percent / AlCl3 / nitromethane / 4 h / 20 °C 2: 98 percent / aq. KOH / Heating 3: 86 percent / quinoline; 5-acetylindole-3-carboxylic acid cupric(II) salt / 2 h / 155 °C View Scheme |
5-acetyl-3-trifluoroacetylindole
1-(1H-indol-5-yl)ethanone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 98 percent / aq. KOH / Heating 2: 86 percent / quinoline; 5-acetylindole-3-carboxylic acid cupric(II) salt / 2 h / 155 °C View Scheme |
1-Acetyl-2,3-dihydro-1H-indole
1-(1H-indol-5-yl)ethanone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 12 percent / acetone / 24 h / Irradiation 2: 90 percent / acetone / 70 h / Irradiation View Scheme | |
Multi-step reaction with 3 steps 1: AlCl3 2: H3O(1+) 3: chloranile View Scheme | |
Multi-step reaction with 3 steps 1: aluminium chloride; carbon disulfide 2: hydrochloric acid; water 3: tetrachloro-<1,4>benzoquinone; xylene View Scheme |
1-indoline
1-(1H-indol-5-yl)ethanone
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 2: AlCl3 3: H3O(1+) 4: chloranile View Scheme |
1-(1-acetylindolin-5-yl)ethanone
1-(1H-indol-5-yl)ethanone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: H3O(1+) 2: chloranile View Scheme | |
Multi-step reaction with 2 steps 1: hydrochloric acid; water 2: tetrachloro-<1,4>benzoquinone; xylene View Scheme |
1-(1H-indol-5-yl)ethanone
Conditions | Yield |
---|---|
With hydrogenchloride at 20℃; |
5-bromo-1H-indole
1-(1H-indol-5-yl)ethanone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: potassium hydride / tetrahydrofuran; mineral oil / 0.25 h / 0 °C 1.2: 0.33 h / -78 °C 2.1: tetrahydrofuran; mineral oil; pentane / -78 - 20 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / acetonitrile / 6 h / 50 °C 1.2: 3 h / 20 °C 2.1: bis-[(trifluoroacetoxy)iodo]benzene; 4-cyanobenzaldehyde oxime / methanol; water / 20 °C View Scheme |
Conditions | Yield |
---|---|
In tetrahydrofuran; mineral oil; pentane at -78 - 20℃; |
N-methoxy-N-methyl-1H-indole-5-carboxamide
methylmagnesium bromide
1-(1H-indol-5-yl)ethanone
Conditions | Yield |
---|---|
In tetrahydrofuran; toluene at 20 - 50℃; for 1h; | 323 mg |
1H-Indole-5-carboxylic acid
1-(1H-indol-5-yl)ethanone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 4 h / 20 °C 2: tetrahydrofuran; toluene / 1 h / 20 - 50 °C View Scheme |
1-(1H-indol-5-yl)ethanone
Conditions | Yield |
---|---|
Stage #1: 4-methoxy-6-methyl-7,8-dihydro[1,3]dioxolo[4,5-g]isoquinolin-6-ium bromide With potassium hydroxide In methanol at 25℃; for 0.0333333h; Stage #2: 1-(1H-indol-5-yl)ethanone In methanol at 25℃; chemoselective reaction; | 90% |
1-(1H-indol-5-yl)ethanone
methyl iodide
1-(1-methyl-1H-indol-5-yl)ethan-1-one
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran at 0℃; for 1h; | 89.71% |
1-(1H-indol-5-yl)ethanone
Conditions | Yield |
---|---|
With potassium hydroxide In dimethyl sulfoxide for 1h; Ambient temperature; | 88% |
1-(1H-indol-5-yl)ethanone
oxalic acid diethyl ester
Conditions | Yield |
---|---|
In ethanol for 3h; Inert atmosphere; Reflux; | 83% |
1-(1H-indol-5-yl)ethanone
di-tert-butyl dicarbonate
5-acetylindole-1-carboxylic acid tert-butyl ester
Conditions | Yield |
---|---|
dmap In tetrahydrofuran at 0℃; for 1.08333h; | 81% |
Stage #1: 1-(1H-indol-5-yl)ethanone With sodium hydride In tetrahydrofuran for 0.25h; Stage #2: di-tert-butyl dicarbonate In tetrahydrofuran at 20℃; for 1h; | 79.9% |
Stage #1: 1-(1H-indol-5-yl)ethanone With sodium hydrogencarbonate In tetrahydrofuran at 0℃; for 0.5h; Stage #2: di-tert-butyl dicarbonate In tetrahydrofuran at 20℃; for 0.333333h; | 61.7% |
Conditions | Yield |
---|---|
With tetra-(n-butyl)ammonium iodide; potassium hydroxide In N,N-dimethyl-formamide at 20℃; Inert atmosphere; | 78% |
1-(1H-indol-5-yl)ethanone
carbonic acid dimethyl ester
Conditions | Yield |
---|---|
With sodium hydride In mineral oil Reflux; | 78% |
1-(1H-indol-5-yl)ethanone
p-toluenesulfonyl chloride
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; for 2h; Inert atmosphere; | 68% |
1,4-dibromo-butane
1-(1H-indol-5-yl)ethanone
1-[1-(4-bromobutyl)indol-5-yl]-ethanone
Conditions | Yield |
---|---|
Stage #1: 1-(1H-indol-5-yl)ethanone With tetra-(n-butyl)ammonium iodide; potassium hydroxide In N,N-dimethyl-formamide at 20℃; for 0.75h; Stage #2: 1,4-dibromo-butane In N,N-dimethyl-formamide at 0 - 20℃; for 1.25h; | 67% |
1-(1H-indol-5-yl)ethanone
sodium 4-methylbenzenesulfinate
Conditions | Yield |
---|---|
With iodine; triphenylphosphine In water Reflux; Inert atmosphere; Schlenk technique; Green chemistry; | 60% |
1-(1H-indol-5-yl)ethanone
ethyl 3-[4-(2-chloroethoxy)-phenyl]-2-ethoxy-propionate
ethyl 3-{4-[2-(5-acetylindol-1-yl)ethoxy]phenyl}-2-ethoxypropionate
Conditions | Yield |
---|---|
Stage #1: 1-(1H-indol-5-yl)ethanone With potassium carbonate In N,N-dimethyl-formamide at 100℃; for 1h; Stage #2: ethyl 3-[4-(2-chloroethoxy)-phenyl]-2-ethoxy-propionate In N,N-dimethyl-formamide for 15h; Reflux; | 56% |
1-(1H-indol-5-yl)ethanone
Conditions | Yield |
---|---|
With chloro-trimethyl-silane; phosphonic acid diethyl ester In toluene at 85℃; for 3h; Sealed tube; | 54% |
1-(1H-indol-5-yl)ethanone
5-(1-hydroxyethyl)-1H-indole
Conditions | Yield |
---|---|
With sodium tetrahydroborate In ethanol | 49% |
1-Methyl-4-piperidone
1-(1H-indol-5-yl)ethanone
Conditions | Yield |
---|---|
With sodium methylate In methanol for 48h; Heating; | 36% |
1-(1H-indol-5-yl)ethanone
2-Chloro-N,N-diethylacetamide
2-chloro-1,1'-indole-3,5-diyl-bis-ethanone
Conditions | Yield |
---|---|
With trichlorophosphate at 65℃; for 2h; | 35% |
1-(1H-indol-5-yl)ethanone
carbonic acid dimethyl ester
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran; mineral oil | 27% |
1-(1H-indol-5-yl)ethanone
5-Nitrosalicylaldehyde
methyl iodide
1-(1',3',3'-trimethyl-6-nitro-1',3'-dihydro-spiro[chromene-2,2'-indol]-5'-yl)-ethanone
Conditions | Yield |
---|---|
(i) MeOH, (ii) NaOH, (iii) /BRN= 512565/, EtOH; Multistep reaction; |
1-(1H-indol-5-yl)ethanone
5-nitro-o-vanilline
methyl iodide
1-(8-methoxy-1',3',3'-trimethyl-6-nitro-1',3'-dihydro-spiro[chromene-2,2'-indol]-5'-yl)-ethanone
Conditions | Yield |
---|---|
(i) MeOH, (ii) NaOH, (iii) /BRN= 613271/, EtOH; Multistep reaction; |
3,5-dinitrosalicylaldehyde
1-(1H-indol-5-yl)ethanone
methyl iodide
1-(1',3',3'-trimethyl-6,8-dinitro-1',3'-dihydro-spiro[chromene-2,2'-indol]-5'-yl)-ethanone
Conditions | Yield |
---|---|
(i) MeOH, (ii) NaOH, (iii) /BRN= 1121900/, EtOH; Multistep reaction; |
1-(1H-indol-5-yl)ethanone
3-bromo-5-nitrosalicylaldehyde
methyl iodide
1-(8-bromo-1',3',3'-trimethyl-6-nitro-1',3'-dihydro-spiro[chromene-2,2'-indol]-5'-yl)-ethanone
Conditions | Yield |
---|---|
(i) MeOH, (ii) NaOH, (iii) /BRN= 1213613/, EtOH; Multistep reaction; |
1-(1H-indol-5-yl)ethanone
diethoxyphosphoryl-acetic acid ethyl ester
ethyl (E)-(indol-5-yl)-2-butenoate
Conditions | Yield |
---|---|
With ethanol; sodium hydride 1.) THF, 0 deg C, 30 min, 2.) THF, b.) RT, 30 min, b.) reflux, 8 h; Yield given. Multistep reaction; |
1-(1H-indol-5-yl)ethanone
Bromodiphenylmethane
5-acetyl-1-(diphenylmethyl)indole
Conditions | Yield |
---|---|
With potassium tert-butylate 1.) DMF, 0 deg C, 30 min, 2.) DMF, a.) 0 deg C, 1 h, b.) RT, 3 h; Yield given. Multistep reaction; |
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