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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem’s R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. Near 20 years DayangChem has provided dif

High purity 2-Aminoacetophenone hydrochloride 98% TOP1 supplier in China

Cas:5468-37-1

Min.Order:100 Gram

FOB Price: $3.0

Type:Lab/Research institutions

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality Α-Amino Acetophenone Hydrochloride supplier in China

Cas:5468-37-1

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

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Henan Allgreen Chemical Co.,Ltd

high quality Appearance:white powder Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai

2-Aminoacetophenone hydrochloride

Cas:5468-37-1

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

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Enke Pharma-tech Co.,Ltd. (Cangzhou, China )

Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api, intermedi

2-Aminoacetophenone hydrochloride

Cas:5468-37-1

Min.Order:1 Kilogram

FOB Price: $5.0

Type:Manufacturers

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

2-Aminoacetophenone hydrochloride

Cas:5468-37-1

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Henan Tianfu Chemical Co., Ltd.

TIANFUCHEM--5468-37-1 -- 2-Aminoacetophenone hydrochloride factory price Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stabl

TIANFUCHEM--5468-37-1 -- 2-Aminoacetophenone hydrochloride factory price

Cas:5468-37-1

Min.Order:1 Metric Ton

FOB Price: $2000.0

Type:Lab/Research institutions

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LIDE PHARMACEUTICALS LIMITED

Advantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&amp

2-Aminoacetophenone hydrochloride / LIDE PHARMA- Factory supply / Best price

Cas:5468-37-1

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Jinan Finer Chemical Co., Ltd

Product Description Product website: http://www.finerchem.com Product Name 2-Aminoacetophenone hydrochloride CAS No. 5468-37-1

2-Aminoacetophenone hydrochloride

Cas:5468-37-1

Min.Order:1 Gram

FOB Price: $22.0

Type:Lab/Research institutions

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Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

2-Aminoacetophenone hydrochloride

Cas:5468-37-1

Min.Order:1 Kilogram

FOB Price: $9.0 / 99.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Top PureCAS 5468-37-1 with best price

Cas:5468-37-1

Min.Order:10 Gram

FOB Price: $146.0 / 176.0

Type:Trading Company

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Ethanone,2-amino-1-phenyl-, hydrochloride (1:1) 5468-37-1

Cas:5468-37-1

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Ethanone,2-amino-1-phenyl-, hydrochloride (1:1)

Cas:5468-37-1

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Ethanone,2-amino-1-phenyl-, hydrochloride (1:1)

Cas:5468-37-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

Α-Amino Acetophenone Hydrochloride

Cas:5468-37-1

Min.Order:0

Negotiable

Type:Manufacturers

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Triumph International Development Limilted

Appearance:white or light yellow crystalline powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:By Se

2-Aminoacetophenone hydrochloride

Cas:5468-37-1

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

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SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

2H-1,4-benzoxazin-3(4H)-one

Cas:5468-37-1

Min.Order:4 Kilogram

Negotiable

Type:Lab/Research institutions

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 2-AMINOACETOPHENONE HYDROCHLORIDE

Cas:5468-37-1

Min.Order:0 Metric Ton

Negotiable

Type:Other

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Ethanone,2-amino-1-phenyl-, hydrochloride (1:1)

Cas:5468-37-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

2-Aminoacetophenone hydrochloride/High quality/Best price

Cas:5468-37-1

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

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Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

High purity 2-Aminoacetophenone hydrochloride

Cas:5468-37-1

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Shanghai Minstar Chemical Co., Ltd

Product Name: 2-Aminoacetophenone hydrochloride Synonyms: 2-AMinoacetophenone hydrochloride, 96% 1GR;OMEGA-AMINOACETOPHENONE HYDROCHLORIDE (CA. 4% NACL);2-AMINOACETOPHENONE HYDROCHLORIDE 99%;O-aminoacetophenone HCl ,1-(o-aminophenyl)ethanone;&o

2-Aminoacetophenone hydrochloride

Cas:5468-37-1

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

5468-37-1 CAS NO.5468-37-1

Cas:5468-37-1

Min.Order:1 Metric Ton

FOB Price: $7.0 / 8.0

Type:Trading Company

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Hangzhou Zhongqi chem Co.,Ltd.

Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service and h

Ethanone,2-amino-1-phenyl-, hydrochloride (1:1)

Cas:5468-37-1

Min.Order:0

Negotiable

Type:Other

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

2-Aminoacetophenone HCl

Cas:5468-37-1

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

2-Aminoacetophenone hydrochloride

Cas:5468-37-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

SAGECHEM LIMITED

SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe

2-Aminoacetophenone hydrochloride

Cas:5468-37-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Golden Pharma Co., Limited

GOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation

2-Aminoacetophenone Hydrochloride

Cas:5468-37-1

Min.Order:1 Kilogram

Negotiable

Type:Other

inquiry

Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

2-Aminoacetophenone Hydrochloride cas no. 5468-37-1 98%

Cas:5468-37-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

2-Aminoacetophenone Hydrochloride

Cas:5468-37-1

Min.Order:0

Negotiable

Type:Other

inquiry

Hangzhou Dingyan Chem Co., Ltd

R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou

2-AMino-1-phenylethanone hydrochloride

Cas:5468-37-1

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Synthetic route

α-bromoacetophenone
70-11-1

α-bromoacetophenone

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

Conditions
ConditionsYield
Stage #1: α-bromoacetophenone With hexamethylenetetramine In chloroform at 50℃; for 2h; Delepine Amine Synthesis;
Stage #2: With hydrogenchloride In ethanol for 2h; Reflux;
99%
Stage #1: α-bromoacetophenone With hexamethylenetetramine In diethyl ether at 20℃; for 12h; Delepine Amine Synthesis;
Stage #2: With hydrogenchloride; water In ethanol for 3h; Reflux;
97%
Stage #1: α-bromoacetophenone With hexamethylenetetramine In chloroform at 20℃;
Stage #2: With hydrogenchloride In ethanol; water at 20℃; for 16h;
94%
2-nitroacetophenone
614-21-1

2-nitroacetophenone

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

Conditions
ConditionsYield
With hydrogen; sulfided platinum on carbon In hydrogenchloride; ethanol at 50℃; under 760 Torr; for 2h;98%
C6H9NO4
128038-38-0

C6H9NO4

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

Conditions
ConditionsYield
With hydrogenchloride In ethanol; water for 48h; Ambient temperature;96%
2-diformylamino-1-phenylethanone
127118-86-9

2-diformylamino-1-phenylethanone

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

Conditions
ConditionsYield
With hydrogenchloride; ethanol for 48h; Ambient temperature;95%
With hydrogenchloride In ethanol for 48h; Ambient temperature; Yield given;
L-2-methyl-4-N-benzoylpentaphenone
191104-42-4

L-2-methyl-4-N-benzoylpentaphenone

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

Conditions
ConditionsYield
With hydrogenchloride In methanol Heating; 1;95%
2-azido-1-phenylethan-1-one
1816-88-2

2-azido-1-phenylethan-1-one

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

Conditions
ConditionsYield
Stage #1: 2-azido-1-phenylethan-1-one With tin(II) chloride dihdyrate In methanol at 20℃; Inert atmosphere;
Stage #2: With hydrogenchloride In methanol for 12h; Inert atmosphere;
92%
With hydrogenchloride; hydrogen; palladium on activated charcoal In methanol under 2327.2 Torr; for 5h; Ambient temperature;86%
α-Phenylacyl amino acid methyl ester hydrochloride
38061-23-3, 81202-39-3

α-Phenylacyl amino acid methyl ester hydrochloride

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

Conditions
ConditionsYield
With hydrogenchloride92%
(R)-N-tert-butanesulfinyl 2-oxo-2-phenylethylamine
1386376-82-4

(R)-N-tert-butanesulfinyl 2-oxo-2-phenylethylamine

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

Conditions
ConditionsYield
With hydrogenchloride In methanol at 20℃; for 1h;92%
(R)-N-tert-butanesulfinyl 2,2-dimethoxy-2-phenylethylamine
1386376-70-0

(R)-N-tert-butanesulfinyl 2,2-dimethoxy-2-phenylethylamine

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

Conditions
ConditionsYield
With hydrogenchloride In methanol at 20℃; for 1h;90%
Multi-step reaction with 2 steps
1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.5 h / -78 °C
2: hydrogenchloride / methanol / 1 h / 20 °C
View Scheme
2,2,2-trifluoro-N-(2-oxo-2-phenylethyl)acetamide
91994-49-9

2,2,2-trifluoro-N-(2-oxo-2-phenylethyl)acetamide

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

Conditions
ConditionsYield
With hydrogenchloride In water; isopropyl alcohol at 40℃;89%
With potassium hydroxide at 20℃; for 0.25h;84%
(R)-N-tert-butanesulfinyl 2,2-diethoxy-2-phenylethylamine
1386376-71-1

(R)-N-tert-butanesulfinyl 2,2-diethoxy-2-phenylethylamine

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

Conditions
ConditionsYield
With hydrogenchloride In methanol at 20℃; for 1h;89%
Multi-step reaction with 2 steps
1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.5 h / -78 °C
2: hydrogenchloride / methanol / 1 h / 20 °C
View Scheme
1-(2-oxo-2-phenyl-ethyl)-3,5,7-triaza-1-azonia-tricyclo[3.3.1.13,7]decane chloride

1-(2-oxo-2-phenyl-ethyl)-3,5,7-triaza-1-azonia-tricyclo[3.3.1.13,7]decane chloride

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

Conditions
ConditionsYield
With hydrogenchloride In ethanol at 20℃; for 72h; Hydrolysis;85%
2-nitroacetophenone
614-21-1

2-nitroacetophenone

A

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

B

2-amino-1-phenylethanol hydrochloride
4561-43-7

2-amino-1-phenylethanol hydrochloride

Conditions
ConditionsYield
With hydrogen; platinum on activated charcoal In hydrogenchloride; ethanol at 50℃; under 760 Torr; Product distribution; further catalyst, variation of the amount of hydrogen;A 63%
B n/a
C17H26NO6P
85231-97-6

C17H26NO6P

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

Conditions
ConditionsYield
With hydrogenchloride In benzene Ambient temperature;62%
hexamethylenetetramine
100-97-0

hexamethylenetetramine

1-chloroacetophenone
532-27-4

1-chloroacetophenone

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

Conditions
ConditionsYield
at 20℃; aus der additionellen Verbindung, durch Einw. von alkoh. Salzsaeure;
hexamethylene tetramine salt of ω-bromoacetophenone
37394-52-8

hexamethylene tetramine salt of ω-bromoacetophenone

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

Conditions
ConditionsYield
With hydrogenchloride In ethanol
1-chloroacetophenone
532-27-4

1-chloroacetophenone

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

Conditions
ConditionsYield
With hydrogenchloride; hexamethylenetetramine; sodium iodide 1.) ethanol, chloroform, room temp., 20 h; 2.) ethanol, 50-52 deg C, 3 h; Yield given. Multistep reaction;
Multi-step reaction with 2 steps
1: 84.7 percent / CH2Cl2 / 1 h / 20 °C
2: 85 percent / aq. HCl / ethanol / 72 h / 20 °C
View Scheme
Stage #1: 1-chloroacetophenone With hexamethylenetetramine In chloroform at 20℃; for 4h; Delepine Amine Synthesis;
Stage #2: With hydrogenchloride In methanol for 4h; Delepine Amine Synthesis; Reflux;
2-Aminoacetophenone
613-89-8

2-Aminoacetophenone

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

Conditions
ConditionsYield
With hydrogenchloride In ethanol at 50 - 55℃; Yield given;
sodium diformamide
18197-26-7

sodium diformamide

α-bromoacetophenone
70-11-1

α-bromoacetophenone

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

Conditions
ConditionsYield
With hydrogenchloride 1a) EtOH, RT, 2h, 1b) 50 deg C, 30 min, 2) 30 min, reflux; Yield given. Multistep reaction;
1.) EtOH, 2 h; 2.) HCl, room temp., 2 d,; Yield given. Multistep reaction;
1-(2-oxo-2-phenylethyl)-3,5,7-triaza-1-azoniatricyclo[3.3.1.1(3,7)]decane bromide

1-(2-oxo-2-phenylethyl)-3,5,7-triaza-1-azoniatricyclo[3.3.1.1(3,7)]decane bromide

A

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

B

α-Aminoacetophenone hydrobromide
37394-53-9

α-Aminoacetophenone hydrobromide

Conditions
ConditionsYield
With hydrogenchloride In ethanol for 72h; Ambient temperature; Title compound not separated from byproducts;
phenylmagnesium bromide
100-58-3

phenylmagnesium bromide

A

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

B

hydrobromide of ω-amino-acetophenone

hydrobromide of ω-amino-acetophenone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 20 percent / n-BuLi / tetrahydrofuran; hexane; formic acid / -78 - 20 °C
2: 95 percent / 6N aq.HCl / methanol / Heating; 1
View Scheme
methyl 5-phenyl-4-oxazolecarboxylate
38061-18-6

methyl 5-phenyl-4-oxazolecarboxylate

A

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

B

5-phenyl-oxazole-2-carbonyl chloride

5-phenyl-oxazole-2-carbonyl chloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 80 percent / HCl
2: 92 percent / HCl
View Scheme
1-(2-oxo-2-phenylethyl)-3,5,7-triaza-1-azoniatricyclo[3.3.1.1(3,7)]decane bromide

1-(2-oxo-2-phenylethyl)-3,5,7-triaza-1-azoniatricyclo[3.3.1.1(3,7)]decane bromide

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

Conditions
ConditionsYield
With hydrogenchloride; water In ethanol for 1.5h; Reflux;
acetophenone
98-86-2

acetophenone

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: bromine / dichloromethane / 20 °C
2.1: hexamethylenetetramine / chloroform / 2 h / 50 °C
2.2: 2 h / Reflux
View Scheme
Multi-step reaction with 2 steps
1.1: bromine / diethyl ether / 1.17 h / 0 - 5 °C
2.1: hexamethylenetetramine / chloroform / 4 h / 20 °C
2.2: 3 h / Reflux
View Scheme
Multi-step reaction with 2 steps
1.1: copper(ll) bromide / ethyl acetate; chloroform / Reflux
2.1: hexamethylenetetramine / chloroform / 2 h / 20 °C
2.2: 48 h / 20 °C
View Scheme
2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

benzoyl chloride
98-88-4

benzoyl chloride

N-(2-oxo-2-phenylethyl)benzamide
4190-14-1

N-(2-oxo-2-phenylethyl)benzamide

Conditions
ConditionsYield
With sodium hydrogencarbonate In dichloromethane; water at 20℃; Cooling with ice;100%
With sodium hydrogencarbonate In ethyl acetate Ambient temperature;90%
With sodium carbonate for 4h;84%
4-ethoxy-1,1,1-trifluoro-3-butene-2-one
59938-06-6, 17129-06-5

4-ethoxy-1,1,1-trifluoro-3-butene-2-one

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

(Z)-1,1,1-Trifluoro-4-(2-oxo-2-phenyl-ethylamino)-but-3-en-2-one
142991-64-8

(Z)-1,1,1-Trifluoro-4-(2-oxo-2-phenyl-ethylamino)-but-3-en-2-one

Conditions
ConditionsYield
With triethylamine In acetonitrile for 4h; Ambient temperature;100%
2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

1,1,1-trifluoro-4-methoxypent-3-en-2-one
135351-20-1, 102145-82-4

1,1,1-trifluoro-4-methoxypent-3-en-2-one

(Z)-1,1,1-Trifluoro-4-(2-oxo-2-phenyl-ethylamino)-pent-3-en-2-one
142991-70-6

(Z)-1,1,1-Trifluoro-4-(2-oxo-2-phenyl-ethylamino)-pent-3-en-2-one

Conditions
ConditionsYield
With triethylamine In acetonitrile for 4h; Ambient temperature;100%
2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

(S)-2-Amino-1-phenyl-1-ethanol
56613-81-1

(S)-2-Amino-1-phenyl-1-ethanol

Conditions
ConditionsYield
With hydrogen; triethylamine; (2S,4S)-BCPM-rhodium In methanol at 50℃; under 15200 Torr; for 20h;100%
Multi-step reaction with 4 steps
1: pyridine / 10 h / Ambient temperature
2: 88 percent / NaBH4 / ethanol / 6 h / 0 °C
3: 42 percent / 4 Angstroem sieves / hexane; tetrahydrofuran / 240 h / 25 °C / lipase from Pseudomonas cepacia
4: 10percent aq. HCl / methanol
View Scheme
Multi-step reaction with 4 steps
1: pyridine / 10 h / Ambient temperature
2: 84 percent / NaBH4 / ethanol / 6 h / 0 °C
3: 43 percent / 4 Angstroem sieves / diisopropyl ether / 36 h / 25 °C / lipase from Pseudomonas cepacia
4: 10percent aq. HCl / methanol
View Scheme
Multi-step reaction with 4 steps
1: pyridine / 10 h / Ambient temperature
2: 90 percent / NaBH4 / ethanol / 6 h / 0 °C
3: 4 Angstroem sieves / hexane; tetrahydrofuran / 120 h / 25 °C / lipase from Pseudomonas cepacia
4: 10percent aq. HCl / methanol
View Scheme
Multi-step reaction with 4 steps
1: pyridine / 10 h / Ambient temperature
2: 93 percent / NaBH4 / ethanol / 6 h / 0 °C
3: 39 percent / 4 Angstroem sieves / hexane; tetrahydrofuran / 48 h / 25 °C / lipase from Pseudomonas cepacia
4: 10percent aq. HCl / methanol
View Scheme
2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

4-methyl-benzoyl chloride
874-60-2

4-methyl-benzoyl chloride

4-Methyl-N-[1-(2-oxo-2-phenylethyl)]benzamide
82221-14-5

4-Methyl-N-[1-(2-oxo-2-phenylethyl)]benzamide

Conditions
ConditionsYield
With sodium hydrogencarbonate In ethyl acetate Ambient temperature;100%
With sodium carbonate at 20℃; for 2h; Acylation;82%
2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

4-Chloro-N-[1-(2-oxo-2-phenylethyl)]benzamide
82221-13-4

4-Chloro-N-[1-(2-oxo-2-phenylethyl)]benzamide

Conditions
ConditionsYield
With sodium hydrogencarbonate In ethyl acetate Ambient temperature;100%
With pyridine Acylation; Heating;78.5%
With sodium acetate for 4h;42%
2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

4-chlorobenzoyl chloride
586-75-4

4-chlorobenzoyl chloride

4-Bromo-N-[1-(2-oxo-2-phenylethyl)]benzamide
37611-23-7

4-Bromo-N-[1-(2-oxo-2-phenylethyl)]benzamide

Conditions
ConditionsYield
With sodium hydrogencarbonate In ethyl acetate Ambient temperature;99%
With pyridine Acylation; Heating;77.4%
With sodium acetate for 4h;48%
With pyridine for 0.5h; Heating;
2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

methanesulfonyl chloride
124-63-0

methanesulfonyl chloride

N-(2-oxo-2-phenylethyl)methanesulfonamide
56062-81-8

N-(2-oxo-2-phenylethyl)methanesulfonamide

Conditions
ConditionsYield
With triethylamine In N,N-dimethyl-formamide at 0 - 20℃; for 12h;98%
With triethylamine In N,N-dimethyl-formamide at 0 - 20℃; for 12h;98%
With 4-methyl-morpholine In 1-methyl-pyrrolidin-2-one at 0℃; for 1h;85%
2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

isobutyryl chloride
79-30-1

isobutyryl chloride

C12H15NO2
218768-05-9

C12H15NO2

Conditions
ConditionsYield
With sodium hydrogencarbonate In dichloromethane; water at 20℃; Cooling with ice;96%
With sodium carbonate In dichloromethane; water at 0 - 20℃;
2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

4-methoxy-N-(2-oxo-2-phenylethyl)benzamide
30252-15-4

4-methoxy-N-(2-oxo-2-phenylethyl)benzamide

Conditions
ConditionsYield
With sodium hydrogencarbonate In ethyl acetate Ambient temperature;95%
With sodium carbonate
2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

1,3,4,6-Tetra-O-acetyl-2-deoxy-2-isothiocyanato-α-D-glucopyranose
109947-42-4

1,3,4,6-Tetra-O-acetyl-2-deoxy-2-isothiocyanato-α-D-glucopyranose

1,3,4,6-tetra-O-acetyl-2-deoxy-2-(3-phenacylthioureido)-α-D-glucopyranose
112290-68-3

1,3,4,6-tetra-O-acetyl-2-deoxy-2-(3-phenacylthioureido)-α-D-glucopyranose

Conditions
ConditionsYield
With sodium hydrogencarbonate In water; acetone for 2h; Ambient temperature;95%
2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

1,1-Diphenyl-2-iodoethyl isocyanate
135104-02-8

1,1-Diphenyl-2-iodoethyl isocyanate

N-(2-Iodo-1,1-diphenylethyl)-N'-phenacylurea
135104-00-6

N-(2-Iodo-1,1-diphenylethyl)-N'-phenacylurea

Conditions
ConditionsYield
With sodium hydrogencarbonate In water; acetone for 0.5h; Ambient temperature;95%
potassium (4-fluorobenzoyl)trifluoroborate
1590389-14-2

potassium (4-fluorobenzoyl)trifluoroborate

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

4-Fluoro-N-[1-(2-oxo-2-phenylethyl)]benzamide
2368-16-3

4-Fluoro-N-[1-(2-oxo-2-phenylethyl)]benzamide

Conditions
ConditionsYield
With 1,3-dichloro-5,5-dimethylhydantoin In tetrahydrofuran at 20℃; for 1.5h; pH=3; chemoselective reaction;95%
4-(trifluoromethyl)phenyl isothiocyanate
1645-65-4

4-(trifluoromethyl)phenyl isothiocyanate

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

5-phenyl-N-(4-(trifluoromethyl)phenyl)oxazol-2-amine

5-phenyl-N-(4-(trifluoromethyl)phenyl)oxazol-2-amine

Conditions
ConditionsYield
Stage #1: 4-(trifluoromethyl)phenyl isothiocyanate; 2-aminoacetophenone hydrochloride With potassium carbonate In acetonitrile at 0 - 25℃; for 2h;
Stage #2: With iodine; potassium carbonate In acetonitrile at 60℃; for 1h;
95%
With tetra-(n-butyl)ammonium iodide; triethylamine In methanol; acetonitrile at 0℃; for 5h; Electrolysis;78%
2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

p-nitrophenyl isothiocyanate
2131-61-5

p-nitrophenyl isothiocyanate

N-(4-nitrophenyl)-5-phenyloxazol-2-amine

N-(4-nitrophenyl)-5-phenyloxazol-2-amine

Conditions
ConditionsYield
Stage #1: 2-aminoacetophenone hydrochloride; p-nitrophenyl isothiocyanate With potassium carbonate In acetonitrile at 0 - 25℃; for 1h;
Stage #2: With iodine; potassium carbonate In acetonitrile at 60℃; for 0.5h;
95%
With tetra-(n-butyl)ammonium iodide; triethylamine In methanol; acetonitrile at 0℃; for 5h; Electrolysis;82%
3,5-bistrifluoromethylphenylisothiocyanate
23165-29-9

3,5-bistrifluoromethylphenylisothiocyanate

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

N-(3,5-bis(trifluoromethyl)phenyl)-5-phenyloxazol-2-amine

N-(3,5-bis(trifluoromethyl)phenyl)-5-phenyloxazol-2-amine

Conditions
ConditionsYield
With tetra-(n-butyl)ammonium iodide; triethylamine In methanol; acetonitrile at 0℃; for 5h; Electrolysis;95%
methyl 4-(chlorocarbonyl)butyrate
1501-26-4

methyl 4-(chlorocarbonyl)butyrate

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

N-(4-Carbomethoxybutanoyl)-2-aminoacetophenone
133602-35-4

N-(4-Carbomethoxybutanoyl)-2-aminoacetophenone

Conditions
ConditionsYield
In pyridine94%
trans-1-iodo-2-isocyanatocyclohexane
38765-81-0, 89877-27-0, 137575-61-2

trans-1-iodo-2-isocyanatocyclohexane

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

N-(trans-2-Iodocyclohexyl)-N'-phenacylurea
135103-96-7

N-(trans-2-Iodocyclohexyl)-N'-phenacylurea

Conditions
ConditionsYield
With sodium hydrogencarbonate In water; acetone for 0.5h; Ambient temperature;94%
2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

phenyl isocyanate
103-71-9

phenyl isocyanate

2-oxo-3,4-diphenyl-2,3-dihydro-imidazole-1-carboxylic acid phenylamide

2-oxo-3,4-diphenyl-2,3-dihydro-imidazole-1-carboxylic acid phenylamide

Conditions
ConditionsYield
In toluene Heating;94%
2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

p-chlorphenylisocyanate
104-12-1

p-chlorphenylisocyanate

N-(4-Chlorophenyl)carbamoyl-α-aminoacetophenone
109130-44-1

N-(4-Chlorophenyl)carbamoyl-α-aminoacetophenone

Conditions
ConditionsYield
With sodium carbonate In water at 20℃; for 24h;94%
2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

cyclopropanecarboxylic acid chloride
4023-34-1

cyclopropanecarboxylic acid chloride

N-(2-oxo-2-phenylethyl)cyclopropanecarboxamide

N-(2-oxo-2-phenylethyl)cyclopropanecarboxamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃;94%
1-isothiocyanato-4-(trifluoromethoxy)benzene
64285-95-6

1-isothiocyanato-4-(trifluoromethoxy)benzene

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

5-phenyl-N-(4-(trifluoromethoxy)phenyl)oxazol-2-amine

5-phenyl-N-(4-(trifluoromethoxy)phenyl)oxazol-2-amine

Conditions
ConditionsYield
With tetra-(n-butyl)ammonium iodide; triethylamine In methanol; acetonitrile at 0℃; for 5h; Electrolysis;93%
ethyl 3-(chloroformyl)propionate
14794-31-1

ethyl 3-(chloroformyl)propionate

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

N-(3-Carbethoxypropanoyl)-ω-aminoacetophenone
133602-34-3

N-(3-Carbethoxypropanoyl)-ω-aminoacetophenone

Conditions
ConditionsYield
In pyridine at 25℃; for 96h;92%
di-tert-butyl dicarbonate
24424-99-5

di-tert-butyl dicarbonate

2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

(2-Oxo-2-phenylethyl)carbamic acid tert-butyl ester
76477-26-4

(2-Oxo-2-phenylethyl)carbamic acid tert-butyl ester

Conditions
ConditionsYield
With sodium hydrogencarbonate In ethanol at 20℃; for 48h;92%
With sodium hydrogencarbonate In methanol for 20h;91%
With sodium hydrogencarbonate In methanol; water for 20h;91%

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