Dayangchem’s R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. Near 20 years DayangChem has provided dif
Cas:5468-37-1
Min.Order:100 Gram
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Type:Lab/Research institutions
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryhigh quality Appearance:white powder Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
Cas:5468-37-1
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inquiryCangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api, intermedi
Cas:5468-37-1
Min.Order:1 Kilogram
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Type:Manufacturers
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:5468-37-1
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FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryTIANFUCHEM--5468-37-1 -- 2-Aminoacetophenone hydrochloride factory price Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stabl
Cas:5468-37-1
Min.Order:1 Metric Ton
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
Cas:5468-37-1
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryProduct Description Product website: http://www.finerchem.com Product Name 2-Aminoacetophenone hydrochloride CAS No. 5468-37-1
Cas:5468-37-1
Min.Order:1 Gram
FOB Price: $22.0
Type:Lab/Research institutions
inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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Min.Order:10 Gram
FOB Price: $146.0 / 176.0
Type:Trading Company
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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Min.Order:1 Kilogram
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:5468-37-1
Min.Order:1 Kilogram
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
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Cas:5468-37-1
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:5468-37-1
Min.Order:4 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:5468-37-1
Min.Order:0 Metric Ton
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Type:Other
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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Min.Order:0
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Type:Lab/Research institutions
inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:5468-37-1
Min.Order:1 Gram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:5468-37-1
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryProduct Name: 2-Aminoacetophenone hydrochloride Synonyms: 2-AMinoacetophenone hydrochloride, 96% 1GR;OMEGA-AMINOACETOPHENONE HYDROCHLORIDE (CA. 4% NACL);2-AMINOACETOPHENONE HYDROCHLORIDE 99%;O-aminoacetophenone HCl ,1-(o-aminophenyl)ethanone;&o
Cas:5468-37-1
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:5468-37-1
Min.Order:1 Metric Ton
FOB Price: $7.0 / 8.0
Type:Trading Company
inquiryLocated in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service and h
Cas:5468-37-1
Min.Order:0
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Type:Other
inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
Cas:5468-37-1
Min.Order:0
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Type:Lab/Research institutions
inquirySAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe
Cas:5468-37-1
Min.Order:0
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Type:Lab/Research institutions
inquiryGOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation
Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:5468-37-1
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Type:Lab/Research institutions
inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou
Cas:5468-37-1
Min.Order:0
Negotiable
Type:Manufacturers
inquiryConditions | Yield |
---|---|
Stage #1: α-bromoacetophenone With hexamethylenetetramine In chloroform at 50℃; for 2h; Delepine Amine Synthesis; Stage #2: With hydrogenchloride In ethanol for 2h; Reflux; | 99% |
Stage #1: α-bromoacetophenone With hexamethylenetetramine In diethyl ether at 20℃; for 12h; Delepine Amine Synthesis; Stage #2: With hydrogenchloride; water In ethanol for 3h; Reflux; | 97% |
Stage #1: α-bromoacetophenone With hexamethylenetetramine In chloroform at 20℃; Stage #2: With hydrogenchloride In ethanol; water at 20℃; for 16h; | 94% |
Conditions | Yield |
---|---|
With hydrogen; sulfided platinum on carbon In hydrogenchloride; ethanol at 50℃; under 760 Torr; for 2h; | 98% |
C6H9NO4
2-aminoacetophenone hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol; water for 48h; Ambient temperature; | 96% |
2-diformylamino-1-phenylethanone
2-aminoacetophenone hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride; ethanol for 48h; Ambient temperature; | 95% |
With hydrogenchloride In ethanol for 48h; Ambient temperature; Yield given; |
L-2-methyl-4-N-benzoylpentaphenone
2-aminoacetophenone hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In methanol Heating; 1; | 95% |
Conditions | Yield |
---|---|
Stage #1: 2-azido-1-phenylethan-1-one With tin(II) chloride dihdyrate In methanol at 20℃; Inert atmosphere; Stage #2: With hydrogenchloride In methanol for 12h; Inert atmosphere; | 92% |
With hydrogenchloride; hydrogen; palladium on activated charcoal In methanol under 2327.2 Torr; for 5h; Ambient temperature; | 86% |
α-Phenylacyl amino acid methyl ester hydrochloride
2-aminoacetophenone hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride | 92% |
(R)-N-tert-butanesulfinyl 2-oxo-2-phenylethylamine
2-aminoacetophenone hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In methanol at 20℃; for 1h; | 92% |
(R)-N-tert-butanesulfinyl 2,2-dimethoxy-2-phenylethylamine
2-aminoacetophenone hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In methanol at 20℃; for 1h; | 90% |
Multi-step reaction with 2 steps 1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.5 h / -78 °C 2: hydrogenchloride / methanol / 1 h / 20 °C View Scheme |
2,2,2-trifluoro-N-(2-oxo-2-phenylethyl)acetamide
2-aminoacetophenone hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In water; isopropyl alcohol at 40℃; | 89% |
With potassium hydroxide at 20℃; for 0.25h; | 84% |
(R)-N-tert-butanesulfinyl 2,2-diethoxy-2-phenylethylamine
2-aminoacetophenone hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In methanol at 20℃; for 1h; | 89% |
Multi-step reaction with 2 steps 1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.5 h / -78 °C 2: hydrogenchloride / methanol / 1 h / 20 °C View Scheme |
2-aminoacetophenone hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol at 20℃; for 72h; Hydrolysis; | 85% |
2-nitroacetophenone
A
2-aminoacetophenone hydrochloride
B
2-amino-1-phenylethanol hydrochloride
Conditions | Yield |
---|---|
With hydrogen; platinum on activated charcoal In hydrogenchloride; ethanol at 50℃; under 760 Torr; Product distribution; further catalyst, variation of the amount of hydrogen; | A 63% B n/a |
C17H26NO6P
2-aminoacetophenone hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In benzene Ambient temperature; | 62% |
hexamethylenetetramine
1-chloroacetophenone
2-aminoacetophenone hydrochloride
Conditions | Yield |
---|---|
at 20℃; aus der additionellen Verbindung, durch Einw. von alkoh. Salzsaeure; |
hexamethylene tetramine salt of ω-bromoacetophenone
2-aminoacetophenone hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol |
Conditions | Yield |
---|---|
With hydrogenchloride; hexamethylenetetramine; sodium iodide 1.) ethanol, chloroform, room temp., 20 h; 2.) ethanol, 50-52 deg C, 3 h; Yield given. Multistep reaction; | |
Multi-step reaction with 2 steps 1: 84.7 percent / CH2Cl2 / 1 h / 20 °C 2: 85 percent / aq. HCl / ethanol / 72 h / 20 °C View Scheme | |
Stage #1: 1-chloroacetophenone With hexamethylenetetramine In chloroform at 20℃; for 4h; Delepine Amine Synthesis; Stage #2: With hydrogenchloride In methanol for 4h; Delepine Amine Synthesis; Reflux; |
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol at 50 - 55℃; Yield given; |
sodium diformamide
α-bromoacetophenone
2-aminoacetophenone hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride 1a) EtOH, RT, 2h, 1b) 50 deg C, 30 min, 2) 30 min, reflux; Yield given. Multistep reaction; | |
1.) EtOH, 2 h; 2.) HCl, room temp., 2 d,; Yield given. Multistep reaction; |
A
2-aminoacetophenone hydrochloride
B
α-Aminoacetophenone hydrobromide
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol for 72h; Ambient temperature; Title compound not separated from byproducts; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 20 percent / n-BuLi / tetrahydrofuran; hexane; formic acid / -78 - 20 °C 2: 95 percent / 6N aq.HCl / methanol / Heating; 1 View Scheme |
methyl 5-phenyl-4-oxazolecarboxylate
A
2-aminoacetophenone hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 80 percent / HCl 2: 92 percent / HCl View Scheme |
2-aminoacetophenone hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride; water In ethanol for 1.5h; Reflux; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: bromine / dichloromethane / 20 °C 2.1: hexamethylenetetramine / chloroform / 2 h / 50 °C 2.2: 2 h / Reflux View Scheme | |
Multi-step reaction with 2 steps 1.1: bromine / diethyl ether / 1.17 h / 0 - 5 °C 2.1: hexamethylenetetramine / chloroform / 4 h / 20 °C 2.2: 3 h / Reflux View Scheme | |
Multi-step reaction with 2 steps 1.1: copper(ll) bromide / ethyl acetate; chloroform / Reflux 2.1: hexamethylenetetramine / chloroform / 2 h / 20 °C 2.2: 48 h / 20 °C View Scheme |
2-aminoacetophenone hydrochloride
benzoyl chloride
N-(2-oxo-2-phenylethyl)benzamide
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In dichloromethane; water at 20℃; Cooling with ice; | 100% |
With sodium hydrogencarbonate In ethyl acetate Ambient temperature; | 90% |
With sodium carbonate for 4h; | 84% |
4-ethoxy-1,1,1-trifluoro-3-butene-2-one
2-aminoacetophenone hydrochloride
(Z)-1,1,1-Trifluoro-4-(2-oxo-2-phenyl-ethylamino)-but-3-en-2-one
Conditions | Yield |
---|---|
With triethylamine In acetonitrile for 4h; Ambient temperature; | 100% |
2-aminoacetophenone hydrochloride
1,1,1-trifluoro-4-methoxypent-3-en-2-one
(Z)-1,1,1-Trifluoro-4-(2-oxo-2-phenyl-ethylamino)-pent-3-en-2-one
Conditions | Yield |
---|---|
With triethylamine In acetonitrile for 4h; Ambient temperature; | 100% |
2-aminoacetophenone hydrochloride
(S)-2-Amino-1-phenyl-1-ethanol
Conditions | Yield |
---|---|
With hydrogen; triethylamine; (2S,4S)-BCPM-rhodium In methanol at 50℃; under 15200 Torr; for 20h; | 100% |
Multi-step reaction with 4 steps 1: pyridine / 10 h / Ambient temperature 2: 88 percent / NaBH4 / ethanol / 6 h / 0 °C 3: 42 percent / 4 Angstroem sieves / hexane; tetrahydrofuran / 240 h / 25 °C / lipase from Pseudomonas cepacia 4: 10percent aq. HCl / methanol View Scheme | |
Multi-step reaction with 4 steps 1: pyridine / 10 h / Ambient temperature 2: 84 percent / NaBH4 / ethanol / 6 h / 0 °C 3: 43 percent / 4 Angstroem sieves / diisopropyl ether / 36 h / 25 °C / lipase from Pseudomonas cepacia 4: 10percent aq. HCl / methanol View Scheme | |
Multi-step reaction with 4 steps 1: pyridine / 10 h / Ambient temperature 2: 90 percent / NaBH4 / ethanol / 6 h / 0 °C 3: 4 Angstroem sieves / hexane; tetrahydrofuran / 120 h / 25 °C / lipase from Pseudomonas cepacia 4: 10percent aq. HCl / methanol View Scheme | |
Multi-step reaction with 4 steps 1: pyridine / 10 h / Ambient temperature 2: 93 percent / NaBH4 / ethanol / 6 h / 0 °C 3: 39 percent / 4 Angstroem sieves / hexane; tetrahydrofuran / 48 h / 25 °C / lipase from Pseudomonas cepacia 4: 10percent aq. HCl / methanol View Scheme |
2-aminoacetophenone hydrochloride
4-methyl-benzoyl chloride
4-Methyl-N-[1-(2-oxo-2-phenylethyl)]benzamide
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In ethyl acetate Ambient temperature; | 100% |
With sodium carbonate at 20℃; for 2h; Acylation; | 82% |
2-aminoacetophenone hydrochloride
4-chloro-benzoyl chloride
4-Chloro-N-[1-(2-oxo-2-phenylethyl)]benzamide
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In ethyl acetate Ambient temperature; | 100% |
With pyridine Acylation; Heating; | 78.5% |
With sodium acetate for 4h; | 42% |
2-aminoacetophenone hydrochloride
4-chlorobenzoyl chloride
4-Bromo-N-[1-(2-oxo-2-phenylethyl)]benzamide
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In ethyl acetate Ambient temperature; | 99% |
With pyridine Acylation; Heating; | 77.4% |
With sodium acetate for 4h; | 48% |
With pyridine for 0.5h; Heating; |
2-aminoacetophenone hydrochloride
methanesulfonyl chloride
N-(2-oxo-2-phenylethyl)methanesulfonamide
Conditions | Yield |
---|---|
With triethylamine In N,N-dimethyl-formamide at 0 - 20℃; for 12h; | 98% |
With triethylamine In N,N-dimethyl-formamide at 0 - 20℃; for 12h; | 98% |
With 4-methyl-morpholine In 1-methyl-pyrrolidin-2-one at 0℃; for 1h; | 85% |
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In dichloromethane; water at 20℃; Cooling with ice; | 96% |
With sodium carbonate In dichloromethane; water at 0 - 20℃; |
2-aminoacetophenone hydrochloride
4-methoxy-benzoyl chloride
4-methoxy-N-(2-oxo-2-phenylethyl)benzamide
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In ethyl acetate Ambient temperature; | 95% |
With sodium carbonate |
2-aminoacetophenone hydrochloride
1,3,4,6-Tetra-O-acetyl-2-deoxy-2-isothiocyanato-α-D-glucopyranose
1,3,4,6-tetra-O-acetyl-2-deoxy-2-(3-phenacylthioureido)-α-D-glucopyranose
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water; acetone for 2h; Ambient temperature; | 95% |
2-aminoacetophenone hydrochloride
1,1-Diphenyl-2-iodoethyl isocyanate
N-(2-Iodo-1,1-diphenylethyl)-N'-phenacylurea
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water; acetone for 0.5h; Ambient temperature; | 95% |
potassium (4-fluorobenzoyl)trifluoroborate
2-aminoacetophenone hydrochloride
4-Fluoro-N-[1-(2-oxo-2-phenylethyl)]benzamide
Conditions | Yield |
---|---|
With 1,3-dichloro-5,5-dimethylhydantoin In tetrahydrofuran at 20℃; for 1.5h; pH=3; chemoselective reaction; | 95% |
Conditions | Yield |
---|---|
Stage #1: 4-(trifluoromethyl)phenyl isothiocyanate; 2-aminoacetophenone hydrochloride With potassium carbonate In acetonitrile at 0 - 25℃; for 2h; Stage #2: With iodine; potassium carbonate In acetonitrile at 60℃; for 1h; | 95% |
With tetra-(n-butyl)ammonium iodide; triethylamine In methanol; acetonitrile at 0℃; for 5h; Electrolysis; | 78% |
Conditions | Yield |
---|---|
Stage #1: 2-aminoacetophenone hydrochloride; p-nitrophenyl isothiocyanate With potassium carbonate In acetonitrile at 0 - 25℃; for 1h; Stage #2: With iodine; potassium carbonate In acetonitrile at 60℃; for 0.5h; | 95% |
With tetra-(n-butyl)ammonium iodide; triethylamine In methanol; acetonitrile at 0℃; for 5h; Electrolysis; | 82% |
3,5-bistrifluoromethylphenylisothiocyanate
2-aminoacetophenone hydrochloride
Conditions | Yield |
---|---|
With tetra-(n-butyl)ammonium iodide; triethylamine In methanol; acetonitrile at 0℃; for 5h; Electrolysis; | 95% |
methyl 4-(chlorocarbonyl)butyrate
2-aminoacetophenone hydrochloride
N-(4-Carbomethoxybutanoyl)-2-aminoacetophenone
Conditions | Yield |
---|---|
In pyridine | 94% |
trans-1-iodo-2-isocyanatocyclohexane
2-aminoacetophenone hydrochloride
N-(trans-2-Iodocyclohexyl)-N'-phenacylurea
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water; acetone for 0.5h; Ambient temperature; | 94% |
Conditions | Yield |
---|---|
In toluene Heating; | 94% |
2-aminoacetophenone hydrochloride
p-chlorphenylisocyanate
N-(4-Chlorophenyl)carbamoyl-α-aminoacetophenone
Conditions | Yield |
---|---|
With sodium carbonate In water at 20℃; for 24h; | 94% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; | 94% |
1-isothiocyanato-4-(trifluoromethoxy)benzene
2-aminoacetophenone hydrochloride
Conditions | Yield |
---|---|
With tetra-(n-butyl)ammonium iodide; triethylamine In methanol; acetonitrile at 0℃; for 5h; Electrolysis; | 93% |
ethyl 3-(chloroformyl)propionate
2-aminoacetophenone hydrochloride
N-(3-Carbethoxypropanoyl)-ω-aminoacetophenone
Conditions | Yield |
---|---|
In pyridine at 25℃; for 96h; | 92% |
di-tert-butyl dicarbonate
2-aminoacetophenone hydrochloride
(2-Oxo-2-phenylethyl)carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In ethanol at 20℃; for 48h; | 92% |
With sodium hydrogencarbonate In methanol for 20h; | 91% |
With sodium hydrogencarbonate In methanol; water for 20h; | 91% |
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