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Cas:590-19-2
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inquiry1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ
1,2-BUTADIENE CAS:590-19-2 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates
Cas:590-19-2
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Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Cas:590-19-2
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Cas:590-19-2
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inquiryCAS Number: 590-19-2 Molecular formula: C4H6 Molecular Weight: 54.09 EINECS number: 209-674-2 Related Categories: Chemical Synthesis; Compressed and Liquefied Gases; Synthetic Reagents Mol file: 590-19-2.mol
Cas:590-19-2
Min.Order:1 Metric Ton
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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1,2-Butadiene cas 590-19-2Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
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1,2-Butadiene is a colorless, combustible gas with a characteristic odour. It is easily condensable under pressure. Butadiene-1,2 is soluble in hydrocarbons, alcohols and ethers, but virtually insoluble in water. Application:1,2-Butadiene is an al
Cas:590-19-2
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1,2-ButadieneAppearance:Pls see the Details Storage:Store in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/Pharmaceutical intermediates Transportation:By Sea,by Air,By courier like DHL or Fedx. Por
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3-methylpent-4-yn-2-ol
2,3-dimethylbutene
Conditions | Yield |
---|---|
at 660℃; under 0.001 Torr; | 98% |
Methylcyclopropen
A
dimethylacetylene
B
2,3-dimethylbutene
C
buta-1,3-diene
Conditions | Yield |
---|---|
With sulphur hexafluoride at 230.2℃; under 20.5 Torr; for 1.5h; Product distribution; Rate constant; Kinetics; var. time, var. pressure; | A 91.31% B 1.84% C 6.85% |
Product distribution; Quantum yield; Irradiation; | |
In gas under 0.1 - 6 Torr; Mechanism; Product distribution; Irradiation; |
3-chloro-but-1-yne
2,3-dimethylbutene
Conditions | Yield |
---|---|
61% |
Conditions | Yield |
---|---|
at 20℃; under 50 Torr; Kinetics; radical cross-combination reaction; Photolysis; | A 60% B 40% |
Conditions | Yield |
---|---|
With iron at 23 - 110℃; under 29420.3 Torr; Hydrogenation.in Gegenwart eines Polymerisationsinhibitors; |
Conditions | Yield |
---|---|
With cefaloridine at 280℃; | |
Cs-exchanged H(x)Cs30Na19(AlO2)54(SiO2)138 zeolite Ambient temperature; |
Conditions | Yield |
---|---|
at 275℃; Leiten ueber Floridin; |
Conditions | Yield |
---|---|
at 280℃; |
Conditions | Yield |
---|---|
With cefaloridine at 280℃; |
2-methyl-but-2-ene
A
propene
B
ethene
C
2,3-dimethylbutene
D
isoprene
Conditions | Yield |
---|---|
at 750℃; under 15 Torr; |
2-methyl-but-2-ene
A
naphthalene
B
ethene
C
2,3-dimethylbutene
D
benzene
Conditions | Yield |
---|---|
at 750℃; Produkt 5:Anthracen; |
Conditions | Yield |
---|---|
at 1300 - 1500℃; Pyrolysis; |
methylene
dibutyl ether
A
butyl methyl ether
B
2,3-dimethylbutene
C
n-butyl n-pentyl ether
2,3-dibromo-but-1-ene
2,3-dimethylbutene
Conditions | Yield |
---|---|
With ethanol; zinc |
Conditions | Yield |
---|---|
at 500℃; Pyrolysis; |
Conditions | Yield |
---|---|
Mechanism; |
Conditions | Yield |
---|---|
at 600℃; |
propane
A
propene
B
methane
C
ethene
D
2,3-dimethylbutene
Conditions | Yield |
---|---|
at 700 - 1000℃; bei der termischen Zersetzung; Produkt 5: Benzol; Produkt 6: Acetylen; Produkt 7: Kohlenstoff; Produkt 8: Wasserstoff; |
1,2,2,3-tetrachloro-butane
2,3-dimethylbutene
Conditions | Yield |
---|---|
With zinc copper; ethanol |
1,2-dibromo-2-butene
2,3-dimethylbutene
Conditions | Yield |
---|---|
With ethanol; zinc |
Conditions | Yield |
---|---|
With aluminum oxide at 360 - 460℃; |
Conditions | Yield |
---|---|
nach dem Houdry-Prozess; |
Conditions | Yield |
---|---|
at 600℃; |
Conditions | Yield |
---|---|
at 800℃; under 147.1 Torr; bei Verduennung mit Stickstoff und Kontaktzeit von 0.07 sec; |
Conditions | Yield |
---|---|
at 760 - 833℃; bei Verduennung mit Wasserdampf und einer Kontaktzeit von 0.005-0.1 sec; |
Conditions | Yield |
---|---|
at 650℃; bei Verduennung mit Wasserdampf und Kontaktzeit von 0.4-1 sec; |
2,3-dimethylbutene
Conditions | Yield |
---|---|
at 750℃; under 0.001 Torr; |
Conditions | Yield |
---|---|
tetrahydrofuran; samarium at 79.9℃; |
but-1-yne
A
dimethylacetylene
B
2,3-dimethylbutene
C
buta-1,3-diene
Conditions | Yield |
---|---|
calcium oxide at 30℃; Product distribution; |
dimethylacetylene
A
1-butylene
B
(Z)-2-Butene
C
2,3-dimethylbutene
Conditions | Yield |
---|---|
With hydrogen; tetrahydrofuran; samarium variation of rare earth catalyst, selectivity; | |
With hydrogen; tetrahydrofuran; samarium at 79.9℃; |
2,3-dimethylbutene
2-(methyldiphenylsilyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
Conditions | Yield |
---|---|
With catalyst:Pd(dba)2/R-1,1'-bina-2yl-P(3,5C6H3-Me2)2 In toluene 0°C, 22-90 h, bis(dibenzylideneacetone) palladium / (R)-(1,1')binaphthalenyl-2-yl-bis-(3,5-dimethyl-phenyl)-phosphane as catalyst; | 96% |
2,3-dimethylbutene
Conditions | Yield |
---|---|
In dichloromethane (Ar, Schlenk) methylallene was passed through a stirred soln. of complexin CH2Cl2 for 1 min at a rate 0.1 mL/s, stirred under methylallene atm. at ambient temp. for 24 h; reduced in vol., diethyl ether was added, ppt. was washed with diethyl ether (twice) and dried in vac.; elem. anal.; | 94% |
2,3-dimethylbutene
(1R,2R,6S,8R)-4-(Dimethyl-phenyl-silanyl)-2,9,9-trimethyl-3,5-dioxa-4-bora-tricyclo[6.1.1.02,6]decane
Conditions | Yield |
---|---|
With (C5H5)(allyl)Pd; (R)-Ph2PC10H6C10H7 In toluene allene (1.2 equiv.) added to mixt. of P ligand and Pd compd. in toluene at room temp.; (R)-silylborane added; mixt. stirred at room temp. for 8-24 h; bulb-to-bulb distd. under vac.; ratio of (R,S) to (R,R) = 93:7; | 92% |
2,3-dimethylbutene
Conditions | Yield |
---|---|
With HBF4*Et2O In chlorobenzene under inert gas; addn. of HBF4*OEt2 to a soln of (C5H5)Re(NO)(PPh3)(CH3) at -45°C with stirring, after 30 min addn. of 1,2-butadiene, stirring at room temp. for 5 d;; evapn., pptn., filtration, dissolving (CH2Cl2), addn. to hexane, pptn., crystn. (CH2Cl2/ether); elem. anal.; | 90% |
Conditions | Yield |
---|---|
With [2,2]bipyridinyl; carbon dioxide In tetrahydrofuran MeCH=C=CH2 was added at -78°C to a suspn. of (COD)2Ni and bipy in THF, reaction vessel was evacuated, CO2 admitted at -78°C, mixt. was warmed at 20°C and stirred for 48 h; soln. was concd. in vacuo, pentane added, ppt. was filtered off, washedwith pentane and dried in vacuo; elem. anal.; | 88.5% |
2,3-dimethylbutene
1,2-dimethoxy-1,1,2,2-tetramethyldisilane
Conditions | Yield |
---|---|
With butene-2; tetrakis(triphenylphosphine) palladium(0) at 120℃; for 15h; | 88% |
With tetrakis(triphenylphosphine) palladium(0) In benzene at 120℃; for 15h; | 88% |
2,3-dimethylbutene
dimethylphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silane
Conditions | Yield |
---|---|
With ethriol phosphite; tris(dibenzylideneacetone)dipalladium (0) In tetrahydrofuran at 80℃; for 9h; Addition; | 88% |
With catalyst: Pd2(dba)3 + etpo In tetrahydrofuran heating catalyst at 80°C for 5 min, addn. of diene and B-compound, heating at 80°C for 9 h; TLC; | 88% |
Conditions | Yield |
---|---|
Stage #1: 2,3-dimethylbutene; acetophenone With (R)-Cl-MeO-BiPhep; bis(pinacol)diborane; copper(l) chloride; sodium t-butanolate In tetrahydrofuran at 22℃; for 18h; Inert atmosphere; Stage #2: With sodium perborate In tetrahydrofuran; water at 22℃; for 1h; Inert atmosphere; enantioselective reaction; | A n/a B 88% |
2,3-dimethylbutene
methoxypentamethyldisilane
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0) In benzene at 120℃; for 15h; | 87% |
Conditions | Yield |
---|---|
Stage #1: 2,3-dimethylbutene; acetophenone With 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; bis(pinacol)diborane; copper(l) chloride; sodium t-butanolate In tetrahydrofuran at 22℃; for 18h; Inert atmosphere; Stage #2: With sodium perborate In tetrahydrofuran; water at 22℃; for 1h; Inert atmosphere; diastereoselective reaction; | 87% |
2,3-dimethylbutene
1,1,2,2-tetramethoxy-1,2-dimethyl-disilane
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0) In benzene at 120℃; for 15h; | 86% |
2,3-dimethylbutene
Conditions | Yield |
---|---|
With trimethylamine oxide In dichloromethane byproducts: CO; (Ar); passing methylallene through a soln. of cluster in CH2Cl2, addn. of amine oxide, stirring for 30 min; filtration, addn. of pentane, washing ppt. with ether, drying in argon; elem. anal.; | 86% |
2,3-dimethylbutene
[IrOs(CO)3(μ-η3:κ1-CH2CCHCH3)(μ-Ph2PCH2PPh2)2][BF4]
Conditions | Yield |
---|---|
In dichloromethane byproducts: CO; (Ar); CH3CHCCH2 passed through a soln. of Ir complex for 1 min, stirred under CH3CHCCH2 for 4 h at ambient temp.; concd., pptd. (Et2O), washed (Et2O), dried (vac.); elem. anal.; | 85% |
With (CH3)3NO In not given (Ar); |
2,3-dimethylbutene
1,1,2-trichloro-1,2,2-trimethyldisilane
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0) In 1,3,5-trimethyl-benzene at 100℃; for 5h; | 84% |
Conditions | Yield |
---|---|
With butene-2; tetrakis(triphenylphosphine) palladium(0) at 100℃; for 5h; | 84% |
2,3-dimethylbutene
A
3-methyl-undeca-1,2-diene
B
2,3-dodecadiene
C
3-methylundec-1-yne
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran; hexane -78 deg C, 30 min -> room temperature; | A 15% B 84% C 1% |
Conditions | Yield |
---|---|
With isopropyl alcohol; caesium carbonate In ethyl acetate; 1,2-dichloro-ethane at 75℃; for 14h; | 83% |
2,3-dimethylbutene
Conditions | Yield |
---|---|
In not given in react. of (HB(pz)3)(1-) with the solvated cation (Pt(CH3)(COD))(1+) an insol. and probably polymeric product is formed; this reacts readily with substituted allene;; | 83% |
In not given in react. of (HB(pz)3)(1-) with the solvated cation (Pt(CH3)(COD))(1+) an insol. and probably polymeric product is formed; this reacts readily with substituted allene;; | 83% |
Conditions | Yield |
---|---|
caesium carbonate In ethyl acetate; 1,2-dichloro-ethane at 75℃; for 14h; | 82% |
Conditions | Yield |
---|---|
Stage #1: 2,3-dimethylbutene; cyclohexane carbonitrile; bis(pinacol)diborane With (2R)-1-[(1R)-1-[bis(1,1-dimethylethyl)phosphino]ethyl]-2-(diphenylphosphino)ferrocene; mesitylcopper(I) In methanol; diethyl ether at -40℃; for 10h; Stage #2: With aluminium(III) triflate In methanol for 2h; Stage #3: With methanol; lithium borohydride at -78℃; for 4h; stereoselective reaction; | 81% |
[Ni(1,5,9-cyclododecatriene)]
2,3-dimethylbutene
1,2-bis-(dicyclohexylphosphino)ethane
Conditions | Yield |
---|---|
With carbon dioxide In tetrahydrofuran MeCH=C=CH2 was added at -78°C to a suspn. of (CDT)Ni and diphosphine in THF, reaction vessel was evacuated, CO2 admitted at -78°C, mixt. was warmed at 20°C and stirred for 48 h; soln. was concd. in vacuo, pentane added, ppt. was filtered off, washedwith pentane and dried in vacuo; elem. anal.; | 80.2% |
Conditions | Yield |
---|---|
With <2,6-(ipr)2-C6H3-N=CH-CH=N-2,6-(ipr)2C6H3>Pd-(COOMe)4-cyclopentadiene In toluene at 40℃; for 48h; | 80% |
2,3-dimethylbutene
[IrRu(CO)4(bis(diphenylphosphino)methane)2][BF4]
Conditions | Yield |
---|---|
In dichloromethane (N2); Schlenk technique; stirred soln. of Ir-Ru complex in CH2Cl2 was satd. with methylallene; stirred at ambient temp. for 24 h; pentane added; filtered; rinsed (pentane); dried (vac.); | 80% |
Conditions | Yield |
---|---|
With isopropyl alcohol; caesium carbonate In ethyl acetate; 1,2-dichloro-ethane at 75℃; for 14h; | 79% |
2,3-dimethylbutene
methyl 3,3,3-trifluoropyruvate
Conditions | Yield |
---|---|
at 100℃; for 24h; | 78% |
2,3-dimethylbutene
1-phenylethan-1-iminium chloride
bis(pinacol)diborane
Conditions | Yield |
---|---|
With C57H66N2O3S; copper(l) chloride; sodium t-butanolate In tetrahydrofuran at 22℃; for 24h; stereoselective reaction; | 78% |
Conditions | Yield |
---|---|
With isopropyl alcohol; caesium carbonate In ethyl acetate; 1,2-dichloro-ethane at 75℃; for 14h; | 77% |
2,3-dimethylbutene
bis(pinacol)diborane
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0) In toluene room temp., 14 h; chromy. on silica; | 77% |
With tris-(dibenzylideneacetone)dipalladium(0) In toluene room temp., 14 h; chromy. on silica; | 68% |
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