DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:617-92-5
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inquiryTIANFUCHEM-- 617-92-5--High purity N-ETHYLPYRROLEin stock Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable business r
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inquirysuperior quality moderate price & quick delivery Appearance:powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Used to make other ch
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
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Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
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inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
EthylpyrroleAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air
Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
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We are committed to providing our customers with the best products and services at the most competitive prices.Appearance:white to light yellow crystal powder Storage:Room temperature with sealed well Package:according to the clients requirement Appl
1H-Pyrrole, 1-ethyl- cas 617-92-5Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiryCompound sourcing ServicesAgency of testing serviceFactory audit serviceFounded in Dec. 1999, Nanjing Chemlin Chemical Industrial Co.,Ltd(CHEMLIN) has been covering the business scope from trading of chemicals to custom-synthesis & Manufacturing. Co
Yinghao Pharm products include: leader molecule, heterocyclic compounds,chiral compounds, photoelectric materials, biochemical reagents etc. For example:benzene, pyrimidine, boricacid,pyridine, pyrazole, imidazole, pyrrole, fluorine and other derivat
Conditions | Yield |
---|---|
With potassium hydroxide; PEG-400-Et2 In water; benzene at 30℃; for 2h; | 88% |
With potassium hydroxide; PEG-400-Et2 In water; benzene at 45℃; for 2h; Product distribution; other heterocycles; var. solvents, var. phase transfer catalysts; | 84% |
Conditions | Yield |
---|---|
With potassium hydroxide; tetrabutylammomium bromide at 25℃; for 24h; | 85% |
With potassium tert-butylate; 18-crown-6 ether In diethyl ether for 1h; Ambient temperature; | 83% |
With potassium hydroxide; tetrabutylammomium bromide Product distribution; multistep reaction: 1.) room temperature, 1 h, 2.) 24 h; alkylation with phase transfer catalysis without solvent; |
Conditions | Yield |
---|---|
With potassium hydroxide In dimethyl sulfoxide for 0.833333h; | 65% |
1,1-diethyl-5-phenyl-1,5-diazapentadiene
A
1-ethyl-1H-pyrrole
B
1-ethyl-2-methylpyrrole
C
aniline
D
N-methylaniline
Conditions | Yield |
---|---|
at 800℃; under 0.007 Torr; for 1h; Further byproducts given. Title compound not separated from byproducts; | A 24% B 13% C 41% D 13% |
1-ethyl-1-methyl-5-phenyl-1,5-diazapentadiene
A
N-Methylpyrrole
B
1-ethyl-1H-pyrrole
C
1,2-dimethylpyrrole
D
aniline
Conditions | Yield |
---|---|
at 800℃; under 0.004 Torr; for 3h; Further byproducts given. Title compound not separated from byproducts; | A 21% B 13% C 14% D 37% |
((E)-Buta-1,3-dienyl)-diethyl-amine
A
3-methylpyrrole
B
2-ethyl-1H-pyrrole
C
3-ethyl-1H-pyrrole
D
1-ethyl-1H-pyrrole
Conditions | Yield |
---|---|
at 800℃; under 0.01 Torr; for 0.166667h; | A 17% B 7.5% C 2% D 14% |
1-ethyl-1-methyl-5-phenyl-1,5-diazapentadiene
1-ethyl-1H-pyrrole
Conditions | Yield |
---|---|
at 500℃; | 15% |
((E)-Buta-1,3-dienyl)-diethyl-amine
A
2-ethyl-1H-pyrrole
B
3-ethyl-1H-pyrrole
C
1-ethyl-1H-pyrrole
D
pyrrole
Conditions | Yield |
---|---|
at 800℃; under 0.001 - 0.01 Torr; for 0.166667h; | A 7.5% B 2% C 14% D 6% |
Conditions | Yield |
---|---|
Ueberleiten auf Palladium/Asbest bei 290grad; |
Conditions | Yield |
---|---|
at 400℃; |
Conditions | Yield |
---|---|
With ethylamine Ueberleiten auf Aluminiumoxid bei 480grad; |
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride; aluminium trichloride; diethyl ether |
1,2-diazine
ethylmagnesium bromide
A
1-ethyl-1H-pyrrole
D
4-Ethyl-1,4-dihydro-pyridazine
Conditions | Yield |
---|---|
In diethyl ether for 0.05h; Product distribution; Mechanism; var. Grignard reagents; |
Conditions | Yield |
---|---|
In acetic acid Heating; | |
With acetic acid | |
With acetic acid Heating; |
pyrrole
ethyl cation
A
2-ethyl-1H-pyrrole
B
3-ethyl-1H-pyrrole
C
1-ethyl-1H-pyrrole
Conditions | Yield |
---|---|
With oxygen; trimethylamine at 37.5℃; under 760 Torr; Product distribution; Mechanism; Irradiation; other heteroarenes; var. reaction cond.; |
Conditions | Yield |
---|---|
Yield given. Multistep reaction; |
1-vinyl-1H-pyrrole
carbon monoxide
A
1-ethyl-1H-pyrrole
B
2-pyrrol-1-yl-propionaldehyde
Conditions | Yield |
---|---|
With dodecacarbonyltetrarhodium(0); hydrogen In benzene at 40℃; under 91200 Torr; for 22h; Product distribution; influence of the reaction temperature on regioselectivity of hydroformylation; |
1-ethyl-1H-pyrrole
Conditions | Yield |
---|---|
With diluted acid |
N-acetylpyrrole
aluminium trichloride
diethyl ether
1-ethyl-1H-pyrrole
1-ethyl-1H-pyrrole
Conditions | Yield |
---|---|
bei der trocknen Destillation; |
1-ethyl-1H-pyrrole
Conditions | Yield |
---|---|
bei der trocknen Destillation; |
Conditions | Yield |
---|---|
at 350℃; |
Conditions | Yield |
---|---|
at 300℃; |
butanedinitrile
ethylamine
A
1-ethylpyrrolidine
B
1-ethyl-1H-pyrrole
Conditions | Yield |
---|---|
With hydrogen; palladium |
1-ethyl-1H-pyrrole
formaldehyd
N,N-dimethylammonium chloride
2-(N,N-dimethylaminomethyl)-1-ethylpyrrole
Conditions | Yield |
---|---|
In water at 0 - 20℃; for 7.5h; | 97% |
1-ethyl-1H-pyrrole
(E)-3-(4,4,4-trifluorobut-2-enoyl)oxazolidin-2-one
C13H15F3N2O3
Conditions | Yield |
---|---|
With bis((1,1,1-trifluoro-N-(trifluoromethyl)sulfonyl)methylsulfonamido)zinc; (R,R)-4,6-dibenzofurandiyl-2,2'-bis(4-phenyloxazoline) In dichloromethane at -60℃; for 24h; Friedel Crafts alkylation; Inert atmosphere; Molecular sieve; optical yield given as %ee; enantioselective reaction; | 97% |
1-ethyl-1H-pyrrole
ferrocenecarboxaldehyde
(C5H5)Fe(C5H4CH(C4H3NC2H5))(1+)*ClO4(1-) = [(C5H5)Fe(C5H4CH(C4H3NC2H5))](ClO4)
Conditions | Yield |
---|---|
In perchloric acid; diethyl ether aq. HClO4 addn. to ferrocene derivative, indole and POCl3 (room temp., over 0.25 h), addn. of ether, standing (15 h), pptn.; collection (filtration), washing (ether); elem. anal.; | 96% |
1-ethyl-1H-pyrrole
(E)-3-(4,4,4-trifluorobut-2-enoyl)oxazolidin-2-one
Conditions | Yield |
---|---|
With bis((1,1,1-trifluoro-N-(trifluoromethyl)sulfonyl)methylsulfonamido)zinc; Ph-dbfox In dichloromethane at -75℃; for 24h; Friedel Crafts alkylation; Inert atmosphere; Molecular sieve; optical yield given as %ee; enantioselective reaction; | 96% |
1-ethyl-1H-pyrrole
Conditions | Yield |
---|---|
With trifluoroacetic acid In chlorobenzene at 20℃; for 6h; | 96% |
1-ethyl-1H-pyrrole
2-(2-methyl-acryloyl)-isoxazolidin-3-one
2-[3-(1-ethyl-1H-pyrrol-2-yl)-2-methyl-propionyl]-isoxazolidin-3-one
Conditions | Yield |
---|---|
With bis((1,1,1-trifluoro-N-(trifluoromethyl)sulfonyl)methylsulfonamido)zinc; 4,6-dibenzofurandiyl-2,2'-bis(4-phenyloxazolidine) In dichloromethane at -30℃; for 1h; Friedel Crafts alkylation; Molecular sieve; optical yield given as %ee; enantioselective reaction; | 92% |
1-ethyl-1H-pyrrole
N-methyl bis[(trifluoromethyl)sulfonyl]imide
Conditions | Yield |
---|---|
In chloroform at 70℃; for 10h; Inert atmosphere; | 92% |
Conditions | Yield |
---|---|
With C28H49OSiY In toluene at 100℃; for 24h; Schlenk technique; Sealed tube; | 89% |
Conditions | Yield |
---|---|
In 1,2-dichloro-ethane for 7h; Reflux; | 88% |
Conditions | Yield |
---|---|
With silver (II) carbonate; palladium diacetate; Trimethylacetic acid In water at 40℃; for 24h; regioselective reaction; | 87% |
Conditions | Yield |
---|---|
In ethyl acetate at 70℃; for 2.5h; | 85.8% |
Conditions | Yield |
---|---|
In dichloromethane at 0℃; for 2h; | 83% |
Conditions | Yield |
---|---|
In acetone at 55℃; for 8h; | 82.9% |
1-ethyl-1H-pyrrole
acetylferrocene
(C5H5)Fe(C5H4C(CH3)(C4H3NC2H5))(1+)*ClO4(1-) = [(C5H5)Fe(C5H4C(CH3)(C4H3NC2H5))](ClO4)
Conditions | Yield |
---|---|
In perchloric acid; diethyl ether aq. HClO4 addn. to ferrocene derivative, ethylpyrrole and POCl3 (room temp., over 3 h), addn. of ether, standing (15 h), pptn.; collection (filtration), washing (ether); elem. anal.; | 74% |
1-ethyl-1H-pyrrole
trimethylsilyl trifluoromethanesulfonate
A
1-Ethyl-3-trimethylsilanyl-1H-pyrrole
B
1-Ethyl-2,4-bis-trimethylsilanyl-1H-pyrrole
Conditions | Yield |
---|---|
With triethylamine for 72h; Ambient temperature; | A 71% B 18% |
1-ethyl-1H-pyrrole
sodium difluoromethanesulfinate
Conditions | Yield |
---|---|
With chloro-trimethyl-silane; phosphonic acid diethyl ester In toluene at 85℃; for 3h; Sealed tube; | 71% |
1-ethyl-1H-pyrrole
3-Dimethylamino-2-(dimethylaminomethylenamino)acrylsaeure-ethylester
ethyl 1-ethyl-1H-pyrrolo[3,2-c]pyridine-6-carboxylate
Conditions | Yield |
---|---|
Stage #1: 1-ethyl-1H-pyrrole; 3-Dimethylamino-2-(dimethylaminomethylenamino)acrylsaeure-ethylester With trifluoroacetic acid In acetic acid at 20℃; for 16h; Stage #2: at 180℃; for 0.0333333h; microwave irradiation; | 70% |
1-ethyl-1H-pyrrole
N-fluorobis(benzenesulfon)imide
Conditions | Yield |
---|---|
With sodium fluoride In chloroform for 12h; | 65% |
1-ethyl-1H-pyrrole
di(1-adamantyl) ketone
Conditions | Yield |
---|---|
Stage #1: 1-ethyl-1H-pyrrole With tert.-butyl lithium In diethyl ether; pentane at 0 - 20℃; Metallation; Stage #2: di(1-adamantyl) ketone In diethyl ether; pentane at 20℃; Addition; | 55% |
1-ethyl-1H-pyrrole
carbon monoxide
(4-methoxyphenyl)(1-methyl-1H-pyrrol-2-yl)-methanone
Conditions | Yield |
---|---|
With bis(tri-t-butylphosphine)palladium(0); N-ethyl-N,N-diisopropylamine In acetonitrile at 115℃; under 3040.2 Torr; for 24h; Inert atmosphere; Autoclave; | 54% |
Conditions | Yield |
---|---|
Stage #1: 1-ethyl-1H-pyrrole; isocyanate de chlorosulfonyle In acetonitrile at -10 - 0℃; for 0.5h; Inert atmosphere; Stage #2: With triethylamine; N,N-dimethyl-formamide In acetonitrile at 0 - 25℃; for 16h; Inert atmosphere; | 53.6% |
Conditions | Yield |
---|---|
With di(rhodium)tetracarbonyl dichloride; tris(1,1,1,3,3,3-hexafluoroisopropyl)phosphite; silver carbonate In 1,2-dimethoxyethane; m-xylene at 150℃; for 24h; Inert atmosphere; Sealed tube; regioselective reaction; | 53% |
1-ethyl-1H-pyrrole
Conditions | Yield |
---|---|
With N-Bromosuccinimide In tetrahydrofuran at -78 - 20℃; Inert atmosphere; | 40% |
Conditions | Yield |
---|---|
With palladium(II) trimethylacetate; silver carbonate In dimethyl sulfoxide; N,N-dimethyl-formamide at 80℃; for 19h; chemoselective reaction; | 39% |
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