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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

1-Acenaphthenol

Cas:6306-07-6

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

1-Acenaphthenol

Cas:6306-07-6

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Manufacturer supply CAS 6306-07-6 with best quality

Cas:6306-07-6

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

1-Acenaphthylenol,1,2-dihydro- 6306-07-6

Cas:6306-07-6

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

1-ACENAPHTHENOL CAS:6306-07-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermedia

1-ACENAPHTHENOL CAS:6306-07-6

Cas:6306-07-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

1-Acenaphthylenol,1,2-dihydro-

Cas:6306-07-6

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

1-Acenaphthylenol,1,2-dihydro-

Cas:6306-07-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

1-ACENAPHTHENOL

Cas:6306-07-6

Min.Order:4 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

1-Acenaphthylenol,1,2-dihydro-

Cas:6306-07-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

1-Acenaphthenol

Cas:6306-07-6

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

Hangzhou Huarong Pharm Co., Ltd.

Hangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu

1-Acenaphthenol (Acenaphthene-1-Hydroxy)

Cas:6306-07-6

Min.Order:0

Negotiable

Type:Trading Company

inquiry

TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

1-ACENAPHTHENOL

Cas:6306-07-6

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

inquiry

Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

1-Acenaphthenol

Cas:6306-07-6

Min.Order:0

Negotiable

Type:Other

inquiry

Hangzhou Dingyan Chem Co., Ltd

R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates

1-Acenaphthylenol,1,2-dihydro-

Cas:6306-07-6

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Henan Tianfu Chemical Co., Ltd.

1.Our services:A.Supply sampleB.The packing also can be according the customers` requirmentC.Any inquiries will be replied within 24 hoursD.we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate.

1-Acenaphthylenol,1,2-dihydro-

Cas:6306-07-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

1-Acenaphthylenol,1,2-dihydro-

Cas:6306-07-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Fandachem Co.,Ltd

1-Acenaphthenol cas 6306-07-6Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

1-Acenaphthenol cas 6306-07-6

Cas:6306-07-6

Min.Order:0

Negotiable

Type:Other

inquiry

Henan Kanbei Chemical Co.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

1-ACENAPHTHENOL

Cas:6306-07-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Chinqesen Biotechnology Co., Ltd.

Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen

6306-07-6

Cas:6306-07-6

Min.Order:0

Negotiable

Type:Trading Company

inquiry

ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

1-ACENAPHTHENOL

Cas:6306-07-6

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Amadis Chemical Co., Ltd.

1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G

(1R)-1,2-dihydroacenaphthylen-1-ol

Cas:6306-07-6

Min.Order:10 Milligram

Negotiable

Type:Lab/Research institutions

inquiry

Changzhou Extraordinary Pharmatech co.,LTD

Changzhou Extraordinary Pharmatech co., LTD. As a leading chemical manufacturer and supplier in China.DAS authentication is passed.We can provide the popular precursor chemicals, we have our own strong R & D team, have our own laboratories and fa

1-Acenaphthenol

Cas:6306-07-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Zhengzhou Kingorgchem Chemical Technology Co., Ltd.

1. Subsidiary of Institute of Chemistry, Henan Academy of Sciences, national research platform;2. About 30 years’ experience in this field since 1983;3. An experienced R&D team consisting of Doctors and Masters;4. Various types of analytical instrume

National Research Platform ISO 9001 6306-07-6

Cas:6306-07-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Jilin haofei import and export trade Co.,Ltd

Price, service, company and transport advantage: 1. Best service, place of origin China, high quality, and reasonable price. 2. It's customers' right to choose the package (EMS, DHL, FEDEX, UPS). 3. It's customers' right

1-Acenaphthenol CAS NO.6306-07-6

Cas:6306-07-6

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Yinghao Pharm Co.,Ltd.

Yinghao Pharm products include: leader molecule, heterocyclic compounds,chiral compounds, photoelectric materials, biochemical reagents etc. For example:benzene, pyrimidine, boricacid,pyridine, pyrazole, imidazole, pyrrole, fluorine and other derivat

1-ACENAPHTHENOL

Cas:6306-07-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai united Scientific Co.,Ltd.

United Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat

1-Acenaphthylenol,1,2-dihydro-

Cas:6306-07-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Chungking Joyinchem Co., Ltd.

Joyinchem have been committed to chemical supply for several years and have built good cooperation records with multinational chemical corporations and importers from all over the world. Our services include:-Spot goods-Contract manufacturing-Custom

1-Acenaphthylenol,1,2-dihydro-

Cas:6306-07-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Nanjing Raymon Biotech Co., Ltd.

1-Acenaphthylenol,1,2-dihydro- Storage:keep in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/pharma intermediate Transportation:By Sea,by Air,By courier like DHL or Fedx. Port:Shanghai/Shenzhen

1-Acenaphthylenol,1,2-dihydro-

Cas:6306-07-6

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Finetech Industry Limited

FINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the 1-ACENAPHTHENOL, CAS:6306-07-6 with the most competitive price and the best quality.

1-ACENAPHTHENOL

Cas:6306-07-6

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Jinan Great Chemical Co.,Ltd.

Application:Pharmaceutical intermediates

1-ACENAPHTHENOL

Cas:6306-07-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

1(2H)-acenaphthylenone
2235-15-6

1(2H)-acenaphthylenone

1-acenaphthenol
6306-07-6

1-acenaphthenol

Conditions
ConditionsYield
With hydrogen In methanol at 100℃; under 30003 Torr; Temperature; Autoclave;94.2%
With sodium tetrahydroborate In methanol at 20℃; for 2h;87%
With hydrogen; nickel at 230℃;
acenaphthylene
208-96-8

acenaphthylene

1-acenaphthenol
6306-07-6

1-acenaphthenol

Conditions
ConditionsYield
With sodium tetrahydroborate; titanium tetrachloride In 1,2-dimethoxyethane Ambient temperature;88%
With oxygen; tetraethylammonium borohydride; 5,10,15,20-tetraphenyl-21H,23H-porphine cobalt(II) In 1,2-dimethoxyethane; isopropyl alcohol for 192h; Ambient temperature;76%
With sodium tetrahydroborate; oxygen; (pyridine)Co(dimethylglyoxime)2Cl In 1,2-dimethoxyethane for 20h;11%
With sodium tetrahydroborate; tin(IV) chloride
methanol
67-56-1

methanol

acenaphthene
83-32-9

acenaphthene

A

1-methoxyacenaphthene
21857-35-2

1-methoxyacenaphthene

B

1-acenaphthenol
6306-07-6

1-acenaphthenol

C

1(2H)-acenaphthylenone
2235-15-6

1(2H)-acenaphthylenone

Conditions
ConditionsYield
With ammonium cerium(IV) nitrate; oxygen In water at 20℃; for 0.0833333h;A 14%
B 12%
C 59%
acenaphthene
83-32-9

acenaphthene

A

1-acenaphthenol
6306-07-6

1-acenaphthenol

B

1(2H)-acenaphthylenone
2235-15-6

1(2H)-acenaphthylenone

Conditions
ConditionsYield
With N-hydroxyphthalimide; 1,4-diamino-2,3-dichloroanthraquinone; oxygen In acetonitrile at 80℃; under 1875.15 - 2250.18 Torr; for 10h;A 25 % Chromat.
B 54%
With N-hydroxyphthalimide; bromine; oxygen; acridine yellow In acetonitrile at 100℃; under 2250.18 Torr; for 24h;
With Cr2O4(2-)*Cu(2+); dihydrogen peroxide In acetonitrile at 50℃; for 10h;
acenaphthene quinone
82-86-0

acenaphthene quinone

A

1-acenaphthenol
6306-07-6

1-acenaphthenol

B

acenaphthene
83-32-9

acenaphthene

C

acenaphthylene
208-96-8

acenaphthylene

Conditions
ConditionsYield
With samarium diiodide; water In tetrahydrofuran at 20℃; for 0.00277778h;A 41%
B 26%
C 23%
acenaphthene quinone
82-86-0

acenaphthene quinone

A

decacyclene
191-48-0

decacyclene

B

1-acenaphthenol
6306-07-6

1-acenaphthenol

C

acenaphthene
83-32-9

acenaphthene

D

acenaphthylene
208-96-8

acenaphthylene

Conditions
ConditionsYield
bis(η6-biphenyl)titanium(0) In toluene at 110℃; for 2h; Further byproducts given;A 21%
B 10%
C 11%
D 31%
1-acetoxyacenaphthene
14966-36-0

1-acetoxyacenaphthene

1-acenaphthenol
6306-07-6

1-acenaphthenol

Conditions
ConditionsYield
With sodium hydroxide
acenaphthene
83-32-9

acenaphthene

1-acenaphthenol
6306-07-6

1-acenaphthenol

Conditions
ConditionsYield
With lead dioxide; acetic acid
With lead(II,IV) oxide; acetic acid at 60 - 70℃; Verseifen des Acetats mit waessrig-methylalkoholischer Natronlauge;
Multi-step reaction with 2 steps
1: Pb3O4 / 60 - 70 °C
2: aqueous methanol. NaOH
View Scheme
Multi-step reaction with 2 steps
1: glacial acetic acid; lead (IV)-acetate
2: aqueous methanol. NaOH
View Scheme
Stage #1: acenaphthene With water In acetone for 2h; Darkness;
Stage #2: In acetone for 8h; Irradiation;
isobutylmagnesium bromide
926-62-5

isobutylmagnesium bromide

1(2H)-acenaphthylenone
2235-15-6

1(2H)-acenaphthylenone

A

1-acenaphthenol
6306-07-6

1-acenaphthenol

B

1-isobutyl-acenaphthen-1-ol

1-isobutyl-acenaphthen-1-ol

Conditions
ConditionsYield
With diethyl ether
1-bromoacenaphthene
24171-73-1

1-bromoacenaphthene

1-acenaphthenol
6306-07-6

1-acenaphthenol

Conditions
ConditionsYield
(i) MeCN, NaCN, (ii) aq. NaCl; Multistep reaction;
acenaphthene
83-32-9

acenaphthene

A

1-acenaphthenol
6306-07-6

1-acenaphthenol

B

1-hydroperoxy-1,2-dihydroacenaphthylene
119951-85-8

1-hydroperoxy-1,2-dihydroacenaphthylene

C

acenaphthene quinone
82-86-0

acenaphthene quinone

D

1(2H)-acenaphthylenone
2235-15-6

1(2H)-acenaphthylenone

Conditions
ConditionsYield
tetraethylammonium chloride; oxygen In benzonitrile; chlorobenzene at 84.9℃; for 1.25h; Product distribution; var. oxidants;
With oxygen; tetrabutylammonium perchlorate In benzonitrile; chlorobenzene at 84.85℃; for 2h; Kinetics; Further Variations:; Catalysts; Oxidation;
With tetrabutylammonium perchlorate; oxygen In benzonitrile; chlorobenzene at 84.85℃; for 1.5h; Product distribution; Kinetics; Further Variations:; Reaction partners; var. time; Oxidation;
With N-hydroxyphthalimide; [bis(acetoxy)iodo]benzene; oxygen In chlorobenzene at 75℃; under 760.051 Torr; Kinetics; Activation energy; Reagent/catalyst; Solvent;
acenaphthene
83-32-9

acenaphthene

acetic acid
64-19-7

acetic acid

lead dioxide

lead dioxide

A

1-acenaphthenol
6306-07-6

1-acenaphthenol

B

acenaphthenol acetate

acenaphthenol acetate

diethyl ether
60-29-7

diethyl ether

isobutylmagnesium bromide
926-62-5

isobutylmagnesium bromide

1(2H)-acenaphthylenone
2235-15-6

1(2H)-acenaphthylenone

A

1-acenaphthenol
6306-07-6

1-acenaphthenol

B

1-isobutyl-acenaphthenol-(1)

1-isobutyl-acenaphthenol-(1)

decalin
91-17-8

decalin

1(2H)-acenaphthylenone
2235-15-6

1(2H)-acenaphthylenone

nickel

nickel

A

1,2,2a,3,4,5-hexahydro-acenaphthylene
480-72-8

1,2,2a,3,4,5-hexahydro-acenaphthylene

B

1-acenaphthenol
6306-07-6

1-acenaphthenol

C

acenaphthene
83-32-9

acenaphthene

D

acenaphthylene
208-96-8

acenaphthylene

Conditions
ConditionsYield
at 230℃; unter Druck.Hydrogenation;
acenaphthene quinone
82-86-0

acenaphthene quinone

1-acenaphthenol
6306-07-6

1-acenaphthenol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: nickel; decalin / 120 - 180 °C / Hydrogenation.unter Druck
2: hydrogen; nickel / 230 °C
View Scheme
naphth-1-yl acetic acid
86-87-3

naphth-1-yl acetic acid

1-acenaphthenol
6306-07-6

1-acenaphthenol

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: thionyl chloride / dichloromethane / 2.5 h / 0 - 20 °C
2: aluminum (III) chloride / dichloromethane / 2 h / 0 - 20 °C
3: sodium tetrahydroborate / methanol / 2 h / 20 °C
View Scheme
Multi-step reaction with 3 steps
1: thionyl chloride / dichloromethane / 1 h / 0 °C / Heating / reflux
2: aluminum (III) chloride / 1,2-dichloro-ethane / 1 h / 0 - 20 °C
3: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C
View Scheme
naphthalen-1-yl-acetyl chloride
5121-00-6

naphthalen-1-yl-acetyl chloride

1-acenaphthenol
6306-07-6

1-acenaphthenol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: aluminum (III) chloride / dichloromethane / 2 h / 0 - 20 °C
2: sodium tetrahydroborate / methanol / 2 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: aluminum (III) chloride / 1,2-dichloro-ethane / 1 h / 0 - 20 °C
2: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C
View Scheme
1-acenaphthenol
6306-07-6

1-acenaphthenol

1-bromoacenaphthene
24171-73-1

1-bromoacenaphthene

Conditions
ConditionsYield
With phosphorus tribromide In diethyl ether; dichloromethane at 25℃; for 0.5h;99%
With bromine; 1,2-bis-(diphenylphosphino)ethane In dichloromethane at -20 - 15℃; Inert atmosphere;78%
With pyridine; phosphorus tribromide In dichloromethane at -10℃; for 0.5h;68%
1-acenaphthenol
6306-07-6

1-acenaphthenol

1(2H)-acenaphthylenone
2235-15-6

1(2H)-acenaphthylenone

Conditions
ConditionsYield
With potassium dichromate; sulfuric acid In diethyl ether; water at 0℃; for 0.666667h;97%
With dinitrogen monoxide; dioxo(tetramesitylporphyrinato)ruthenium(VI) In 1,2-dichloro-ethane at 120℃; under 7600 Torr; for 7.5h;95%
With dinitrogen monoxide; dioxo(tetramesitylporphyrinato)ruthenium(VI) In 1,2-dichloro-ethane at 120℃; under 7500.6 Torr; for 7.5h;95%
1-acenaphthenol
6306-07-6

1-acenaphthenol

acetic anhydride
108-24-7

acetic anhydride

1-acetoxyacenaphthene
14966-36-0

1-acetoxyacenaphthene

Conditions
ConditionsYield
With dmap In triethylamine 0 degC -> r.t., overnight;95%
With dmap; triethylamine Acetylation;
With dmap; triethylamine In diethyl ether
With dmap; triethylamine In diethyl ether
1-acenaphthenol
6306-07-6

1-acenaphthenol

acenaphthylene
208-96-8

acenaphthylene

Conditions
ConditionsYield
methyltrioxorhenium(VII) In benzene for 72h;89%
zirconium(IV) chloride In acetonitrile at 20℃; for 0.666667h;89%
With pyridine; thionyl chloride
1-acenaphthenol
6306-07-6

1-acenaphthenol

A

benzoic acid
65-85-0

benzoic acid

B

1(2H)-acenaphthylenone
2235-15-6

1(2H)-acenaphthylenone

Conditions
ConditionsYield
With dibenzoyl peroxide In dichloromethane for 3h; Ambient temperature; Irradiation;A n/a
B 84%
1-acenaphthenol
6306-07-6

1-acenaphthenol

allyl-trimethyl-silane
762-72-1

allyl-trimethyl-silane

1-(2-propenyl)-acenaphthalene

1-(2-propenyl)-acenaphthalene

Conditions
ConditionsYield
bismuth(III) chloride In dichloromethane at 80℃; for 3h;82%
With indium(III) bromide In dichloromethane at 40℃; for 7h;80%
N-hydroxyphthalimide
524-38-9

N-hydroxyphthalimide

1-acenaphthenol
6306-07-6

1-acenaphthenol

2-(1,2-dihydro-1-acenaphthylenyloxy)-1H-isoindole-1,3(2H)-dione

2-(1,2-dihydro-1-acenaphthylenyloxy)-1H-isoindole-1,3(2H)-dione

Conditions
ConditionsYield
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 20℃; for 25h; Mitsunobu reaction;81%
1-acenaphthenol
6306-07-6

1-acenaphthenol

dimethyl 2-((fluoromethyl)(phenyl)-l4-sulfaneylidene)malonate

dimethyl 2-((fluoromethyl)(phenyl)-l4-sulfaneylidene)malonate

1-(fluoromethoxy)-1,2-dihydroacenaphthylene

1-(fluoromethoxy)-1,2-dihydroacenaphthylene

Conditions
ConditionsYield
Stage #1: 1-acenaphthenol With sodium hydride In N,N-dimethyl-formamide; mineral oil at 20℃; for 0.5h; Schlenk technique; Inert atmosphere;
Stage #2: dimethyl 2-((fluoromethyl)(phenyl)-l4-sulfaneylidene)malonate In N,N-dimethyl-formamide; mineral oil at 20℃; for 12h; Schlenk technique; Inert atmosphere;
79%
1-acenaphthenol
6306-07-6

1-acenaphthenol

3,4-dichlorobenzoyl chloride
3024-72-4

3,4-dichlorobenzoyl chloride

(+/-)-1,2-dihydroacenaphthylen-1-yl 3,4-dichlorobenzoate
1161742-29-5

(+/-)-1,2-dihydroacenaphthylen-1-yl 3,4-dichlorobenzoate

Conditions
ConditionsYield
With pyridine; N,N,N,N,-tetramethylethylenediamine at 20℃; for 18h;76%
1-acenaphthenol
6306-07-6

1-acenaphthenol

A

acenaphthene-1-thiol

acenaphthene-1-thiol

B

acenaphthylene
208-96-8

acenaphthylene

Conditions
ConditionsYield
With Lawessons reagent In toluene for 0.5h; Heating;A 72%
B 13%
With Lawessons reagent In toluene for 0.5h; Heating;A 72%
B 13%
1-acenaphthenol
6306-07-6

1-acenaphthenol

p-toluenesulfonylhydrazone glyoxylic acid chloride
14661-69-9

p-toluenesulfonylhydrazone glyoxylic acid chloride

1,2-dihydroacenaphthylen-1-yl diazoacetate
182313-50-4

1,2-dihydroacenaphthylen-1-yl diazoacetate

Conditions
ConditionsYield
With triethylamine In dichloromethane for 1h;71%
1-acenaphthenol
6306-07-6

1-acenaphthenol

ethyl acetate
141-78-6

ethyl acetate

1-acetoxyacenaphthene
14966-36-0

1-acetoxyacenaphthene

Conditions
ConditionsYield
Stage #1: 1-acenaphthenol With potassium tert-butylate In dimethyl sulfoxide at 20℃; for 0.5h; Inert atmosphere;
Stage #2: ethyl acetate In dimethyl sulfoxide at 20℃; for 0.5h; Inert atmosphere;
70%
4-Nitrophthalonitrile
31643-49-9

4-Nitrophthalonitrile

1-acenaphthenol
6306-07-6

1-acenaphthenol

4-(1,2-dihydroacenaphthylen-1-yloxy)phthalonitrile
1288981-15-6

4-(1,2-dihydroacenaphthylen-1-yloxy)phthalonitrile

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 50℃; for 72h; Inert atmosphere;69%
1-acenaphthenol
6306-07-6

1-acenaphthenol

4-bromo-3-methylbenzoyl chloride
21900-25-4

4-bromo-3-methylbenzoyl chloride

(+/-)-1,2-dihydroacenaphthylen-1-yl 4-bromo-3-methylbenzoate
1161742-31-9

(+/-)-1,2-dihydroacenaphthylen-1-yl 4-bromo-3-methylbenzoate

Conditions
ConditionsYield
With pyridine; N,N,N,N,-tetramethylethylenediamine at 20℃; for 18h;65%
p-toluenesulfonic acid

p-toluenesulfonic acid

1-acenaphthenol
6306-07-6

1-acenaphthenol

4-Methyl-benzenesulfinic acid acenaphthen-1-yl ester

4-Methyl-benzenesulfinic acid acenaphthen-1-yl ester

Conditions
ConditionsYield
With 1,1'-carbonyldiimidazole In dichloromethane for 2h;61%
1-acenaphthenol
6306-07-6

1-acenaphthenol

4-chloro-3-nitro-benzoyl chloride
38818-50-7

4-chloro-3-nitro-benzoyl chloride

(+/-)-1,2-dihydroacenaphthylen-1-yl 4-chloro-3-nitrobenzoate
1161742-30-8

(+/-)-1,2-dihydroacenaphthylen-1-yl 4-chloro-3-nitrobenzoate

Conditions
ConditionsYield
With pyridine; N,N,N,N,-tetramethylethylenediamine at 20℃; for 18h;53%
vinyl acetate
108-05-4

vinyl acetate

1-acenaphthenol
6306-07-6

1-acenaphthenol

(R)-(+)-1,2-dihydroacenaphthylen-1-yl acetate
14966-36-0

(R)-(+)-1,2-dihydroacenaphthylen-1-yl acetate

Conditions
ConditionsYield
With Pseudomonas fluorescens lipase [E.(1)C313] In diethyl ether at 20℃; Enzymatic reaction;26%
Iodoacetic acid
64-69-7

Iodoacetic acid

1-acenaphthenol
6306-07-6

1-acenaphthenol

1,2-dihydroacenaphthylen-1-yl iodoacetate

1,2-dihydroacenaphthylen-1-yl iodoacetate

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In dichloromethane for 1.5h; Ambient temperature;23%
1-acenaphthenol
6306-07-6

1-acenaphthenol

Propiolic acid
471-25-0

Propiolic acid

Propynoic acid acenaphthen-1-yl ester
182313-38-8

Propynoic acid acenaphthen-1-yl ester

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In ethyl acetate at -10℃; for 20h;21%
Isopropenyl acetate
108-22-5

Isopropenyl acetate

1-acenaphthenol
6306-07-6

1-acenaphthenol

A

(R)-(+)-1,2-dihydroacenaphthylen-1-yl acetate
14966-36-0

(R)-(+)-1,2-dihydroacenaphthylen-1-yl acetate

B

(S)-(+)-1,2-dihydroacenaphthylen-1-ol
121961-98-6

(S)-(+)-1,2-dihydroacenaphthylen-1-ol

C

(S)-(-)-1,2-dihydroacenaphthylen-1-yl acetate

(S)-(-)-1,2-dihydroacenaphthylen-1-yl acetate

Conditions
ConditionsYield
With Pseudomonas fluorescens lipase [E.(1)C313] In diethyl ether at 20℃; Enzymatic reaction;A n/a
B 21%
C n/a
N-Isopropyl-N-[3-(piperidinomethyl)phenyl]-3-(2-dicyanomethylidene imidazolidin-1-yl)propionamide
617709-38-3

N-Isopropyl-N-[3-(piperidinomethyl)phenyl]-3-(2-dicyanomethylidene imidazolidin-1-yl)propionamide

1-acenaphthenol
6306-07-6

1-acenaphthenol

N-isopropyl-N-[3-(piperidinomethyl)phenyl]-3-[3-(1-acenaphthenyl)-2-dicyanomethylidene imidazolidin-1-yl]propionamide

N-isopropyl-N-[3-(piperidinomethyl)phenyl]-3-[3-(1-acenaphthenyl)-2-dicyanomethylidene imidazolidin-1-yl]propionamide

Conditions
ConditionsYield
With 2,2'-azobis(isobutyronitrile); triphenylphosphine In tetrahydrofuran20%
1-acenaphthenol
6306-07-6

1-acenaphthenol

chromium(lll) acetate
1066-30-4

chromium(lll) acetate

1(2H)-acenaphthylenone
2235-15-6

1(2H)-acenaphthylenone

1-acenaphthenol
6306-07-6

1-acenaphthenol

1,5-dibromo-acenaphthene
25132-44-9

1,5-dibromo-acenaphthene

Conditions
ConditionsYield
With bromine; acetic acid
1-acenaphthenol
6306-07-6

1-acenaphthenol

1-chloro-1,2-dihydroacenaphthylene
40745-49-1

1-chloro-1,2-dihydroacenaphthylene

Conditions
ConditionsYield
With hydrogenchloride; diethyl ether; calcium chloride
With thionyl chloride; N,N-dimethyl-formamide In dichloromethane at -20℃; for 2h;

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