As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:6306-07-6
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiry1-ACENAPHTHENOL CAS:6306-07-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermedia
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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Min.Order:4 Kilogram
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:6306-07-6
Min.Order:10 Gram
FOB Price: $100.0
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inquiryHangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
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inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
Cas:6306-07-6
Min.Order:1 Kilogram
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates
1.Our services:A.Supply sampleB.The packing also can be according the customers` requirmentC.Any inquiries will be replied within 24 hoursD.we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate.
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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inquiry1-Acenaphthenol cas 6306-07-6Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
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Cas:6306-07-6
Min.Order:10 Milligram
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inquiryChangzhou Extraordinary Pharmatech co., LTD. As a leading chemical manufacturer and supplier in China.DAS authentication is passed.We can provide the popular precursor chemicals, we have our own strong R & D team, have our own laboratories and fa
1. Subsidiary of Institute of Chemistry, Henan Academy of Sciences, national research platform;2. About 30 years’ experience in this field since 1983;3. An experienced R&D team consisting of Doctors and Masters;4. Various types of analytical instrume
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inquiryPrice, service, company and transport advantage: 1. Best service, place of origin China, high quality, and reasonable price. 2. It's customers' right to choose the package (EMS, DHL, FEDEX, UPS). 3. It's customers' right
Yinghao Pharm products include: leader molecule, heterocyclic compounds,chiral compounds, photoelectric materials, biochemical reagents etc. For example:benzene, pyrimidine, boricacid,pyridine, pyrazole, imidazole, pyrrole, fluorine and other derivat
United Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat
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inquiryJoyinchem have been committed to chemical supply for several years and have built good cooperation records with multinational chemical corporations and importers from all over the world. Our services include:-Spot goods-Contract manufacturing-Custom
Cas:6306-07-6
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inquiry1-Acenaphthylenol,1,2-dihydro- Storage:keep in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/pharma intermediate Transportation:By Sea,by Air,By courier like DHL or Fedx. Port:Shanghai/Shenzhen
FINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the 1-ACENAPHTHENOL, CAS:6306-07-6 with the most competitive price and the best quality.
Conditions | Yield |
---|---|
With hydrogen In methanol at 100℃; under 30003 Torr; Temperature; Autoclave; | 94.2% |
With sodium tetrahydroborate In methanol at 20℃; for 2h; | 87% |
With hydrogen; nickel at 230℃; |
Conditions | Yield |
---|---|
With sodium tetrahydroborate; titanium tetrachloride In 1,2-dimethoxyethane Ambient temperature; | 88% |
With oxygen; tetraethylammonium borohydride; 5,10,15,20-tetraphenyl-21H,23H-porphine cobalt(II) In 1,2-dimethoxyethane; isopropyl alcohol for 192h; Ambient temperature; | 76% |
With sodium tetrahydroborate; oxygen; (pyridine)Co(dimethylglyoxime)2Cl In 1,2-dimethoxyethane for 20h; | 11% |
With sodium tetrahydroborate; tin(IV) chloride |
methanol
acenaphthene
A
1-methoxyacenaphthene
B
1-acenaphthenol
C
1(2H)-acenaphthylenone
Conditions | Yield |
---|---|
With ammonium cerium(IV) nitrate; oxygen In water at 20℃; for 0.0833333h; | A 14% B 12% C 59% |
Conditions | Yield |
---|---|
With N-hydroxyphthalimide; 1,4-diamino-2,3-dichloroanthraquinone; oxygen In acetonitrile at 80℃; under 1875.15 - 2250.18 Torr; for 10h; | A 25 % Chromat. B 54% |
With N-hydroxyphthalimide; bromine; oxygen; acridine yellow In acetonitrile at 100℃; under 2250.18 Torr; for 24h; | |
With Cr2O4(2-)*Cu(2+); dihydrogen peroxide In acetonitrile at 50℃; for 10h; |
acenaphthene quinone
A
1-acenaphthenol
B
acenaphthene
C
acenaphthylene
Conditions | Yield |
---|---|
With samarium diiodide; water In tetrahydrofuran at 20℃; for 0.00277778h; | A 41% B 26% C 23% |
acenaphthene quinone
A
decacyclene
B
1-acenaphthenol
C
acenaphthene
D
acenaphthylene
Conditions | Yield |
---|---|
bis(η6-biphenyl)titanium(0) In toluene at 110℃; for 2h; Further byproducts given; | A 21% B 10% C 11% D 31% |
1-acetoxyacenaphthene
1-acenaphthenol
Conditions | Yield |
---|---|
With sodium hydroxide |
Conditions | Yield |
---|---|
With lead dioxide; acetic acid | |
With lead(II,IV) oxide; acetic acid at 60 - 70℃; Verseifen des Acetats mit waessrig-methylalkoholischer Natronlauge; | |
Multi-step reaction with 2 steps 1: Pb3O4 / 60 - 70 °C 2: aqueous methanol. NaOH View Scheme | |
Multi-step reaction with 2 steps 1: glacial acetic acid; lead (IV)-acetate 2: aqueous methanol. NaOH View Scheme | |
Stage #1: acenaphthene With water In acetone for 2h; Darkness; Stage #2: In acetone for 8h; Irradiation; |
Conditions | Yield |
---|---|
With diethyl ether |
1-bromoacenaphthene
1-acenaphthenol
Conditions | Yield |
---|---|
(i) MeCN, NaCN, (ii) aq. NaCl; Multistep reaction; |
acenaphthene
A
1-acenaphthenol
B
1-hydroperoxy-1,2-dihydroacenaphthylene
C
acenaphthene quinone
D
1(2H)-acenaphthylenone
Conditions | Yield |
---|---|
tetraethylammonium chloride; oxygen In benzonitrile; chlorobenzene at 84.9℃; for 1.25h; Product distribution; var. oxidants; | |
With oxygen; tetrabutylammonium perchlorate In benzonitrile; chlorobenzene at 84.85℃; for 2h; Kinetics; Further Variations:; Catalysts; Oxidation; | |
With tetrabutylammonium perchlorate; oxygen In benzonitrile; chlorobenzene at 84.85℃; for 1.5h; Product distribution; Kinetics; Further Variations:; Reaction partners; var. time; Oxidation; | |
With N-hydroxyphthalimide; [bis(acetoxy)iodo]benzene; oxygen In chlorobenzene at 75℃; under 760.051 Torr; Kinetics; Activation energy; Reagent/catalyst; Solvent; |
diethyl ether
isobutylmagnesium bromide
1(2H)-acenaphthylenone
A
1-acenaphthenol
decalin
1(2H)-acenaphthylenone
A
1,2,2a,3,4,5-hexahydro-acenaphthylene
B
1-acenaphthenol
C
acenaphthene
D
acenaphthylene
Conditions | Yield |
---|---|
at 230℃; unter Druck.Hydrogenation; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: nickel; decalin / 120 - 180 °C / Hydrogenation.unter Druck 2: hydrogen; nickel / 230 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: thionyl chloride / dichloromethane / 2.5 h / 0 - 20 °C 2: aluminum (III) chloride / dichloromethane / 2 h / 0 - 20 °C 3: sodium tetrahydroborate / methanol / 2 h / 20 °C View Scheme | |
Multi-step reaction with 3 steps 1: thionyl chloride / dichloromethane / 1 h / 0 °C / Heating / reflux 2: aluminum (III) chloride / 1,2-dichloro-ethane / 1 h / 0 - 20 °C 3: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aluminum (III) chloride / dichloromethane / 2 h / 0 - 20 °C 2: sodium tetrahydroborate / methanol / 2 h / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: aluminum (III) chloride / 1,2-dichloro-ethane / 1 h / 0 - 20 °C 2: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C View Scheme |
1-acenaphthenol
1-bromoacenaphthene
Conditions | Yield |
---|---|
With phosphorus tribromide In diethyl ether; dichloromethane at 25℃; for 0.5h; | 99% |
With bromine; 1,2-bis-(diphenylphosphino)ethane In dichloromethane at -20 - 15℃; Inert atmosphere; | 78% |
With pyridine; phosphorus tribromide In dichloromethane at -10℃; for 0.5h; | 68% |
Conditions | Yield |
---|---|
With potassium dichromate; sulfuric acid In diethyl ether; water at 0℃; for 0.666667h; | 97% |
With dinitrogen monoxide; dioxo(tetramesitylporphyrinato)ruthenium(VI) In 1,2-dichloro-ethane at 120℃; under 7600 Torr; for 7.5h; | 95% |
With dinitrogen monoxide; dioxo(tetramesitylporphyrinato)ruthenium(VI) In 1,2-dichloro-ethane at 120℃; under 7500.6 Torr; for 7.5h; | 95% |
Conditions | Yield |
---|---|
With dmap In triethylamine 0 degC -> r.t., overnight; | 95% |
With dmap; triethylamine Acetylation; | |
With dmap; triethylamine In diethyl ether | |
With dmap; triethylamine In diethyl ether |
Conditions | Yield |
---|---|
methyltrioxorhenium(VII) In benzene for 72h; | 89% |
zirconium(IV) chloride In acetonitrile at 20℃; for 0.666667h; | 89% |
With pyridine; thionyl chloride |
Conditions | Yield |
---|---|
With dibenzoyl peroxide In dichloromethane for 3h; Ambient temperature; Irradiation; | A n/a B 84% |
Conditions | Yield |
---|---|
bismuth(III) chloride In dichloromethane at 80℃; for 3h; | 82% |
With indium(III) bromide In dichloromethane at 40℃; for 7h; | 80% |
Conditions | Yield |
---|---|
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 20℃; for 25h; Mitsunobu reaction; | 81% |
1-acenaphthenol
Conditions | Yield |
---|---|
Stage #1: 1-acenaphthenol With sodium hydride In N,N-dimethyl-formamide; mineral oil at 20℃; for 0.5h; Schlenk technique; Inert atmosphere; Stage #2: dimethyl 2-((fluoromethyl)(phenyl)-l4-sulfaneylidene)malonate In N,N-dimethyl-formamide; mineral oil at 20℃; for 12h; Schlenk technique; Inert atmosphere; | 79% |
1-acenaphthenol
3,4-dichlorobenzoyl chloride
(+/-)-1,2-dihydroacenaphthylen-1-yl 3,4-dichlorobenzoate
Conditions | Yield |
---|---|
With pyridine; N,N,N,N,-tetramethylethylenediamine at 20℃; for 18h; | 76% |
Conditions | Yield |
---|---|
With Lawessons reagent In toluene for 0.5h; Heating; | A 72% B 13% |
With Lawessons reagent In toluene for 0.5h; Heating; | A 72% B 13% |
1-acenaphthenol
p-toluenesulfonylhydrazone glyoxylic acid chloride
1,2-dihydroacenaphthylen-1-yl diazoacetate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane for 1h; | 71% |
Conditions | Yield |
---|---|
Stage #1: 1-acenaphthenol With potassium tert-butylate In dimethyl sulfoxide at 20℃; for 0.5h; Inert atmosphere; Stage #2: ethyl acetate In dimethyl sulfoxide at 20℃; for 0.5h; Inert atmosphere; | 70% |
4-Nitrophthalonitrile
1-acenaphthenol
4-(1,2-dihydroacenaphthylen-1-yloxy)phthalonitrile
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 50℃; for 72h; Inert atmosphere; | 69% |
1-acenaphthenol
4-bromo-3-methylbenzoyl chloride
(+/-)-1,2-dihydroacenaphthylen-1-yl 4-bromo-3-methylbenzoate
Conditions | Yield |
---|---|
With pyridine; N,N,N,N,-tetramethylethylenediamine at 20℃; for 18h; | 65% |
1-acenaphthenol
Conditions | Yield |
---|---|
With 1,1'-carbonyldiimidazole In dichloromethane for 2h; | 61% |
1-acenaphthenol
4-chloro-3-nitro-benzoyl chloride
(+/-)-1,2-dihydroacenaphthylen-1-yl 4-chloro-3-nitrobenzoate
Conditions | Yield |
---|---|
With pyridine; N,N,N,N,-tetramethylethylenediamine at 20℃; for 18h; | 53% |
vinyl acetate
1-acenaphthenol
(R)-(+)-1,2-dihydroacenaphthylen-1-yl acetate
Conditions | Yield |
---|---|
With Pseudomonas fluorescens lipase [E.(1)C313] In diethyl ether at 20℃; Enzymatic reaction; | 26% |
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane for 1.5h; Ambient temperature; | 23% |
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In ethyl acetate at -10℃; for 20h; | 21% |
Isopropenyl acetate
1-acenaphthenol
A
(R)-(+)-1,2-dihydroacenaphthylen-1-yl acetate
B
(S)-(+)-1,2-dihydroacenaphthylen-1-ol
Conditions | Yield |
---|---|
With Pseudomonas fluorescens lipase [E.(1)C313] In diethyl ether at 20℃; Enzymatic reaction; | A n/a B 21% C n/a |
N-Isopropyl-N-[3-(piperidinomethyl)phenyl]-3-(2-dicyanomethylidene imidazolidin-1-yl)propionamide
1-acenaphthenol
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); triphenylphosphine In tetrahydrofuran | 20% |
1-acenaphthenol
1,5-dibromo-acenaphthene
Conditions | Yield |
---|---|
With bromine; acetic acid |
1-acenaphthenol
1-chloro-1,2-dihydroacenaphthylene
Conditions | Yield |
---|---|
With hydrogenchloride; diethyl ether; calcium chloride | |
With thionyl chloride; N,N-dimethyl-formamide In dichloromethane at -20℃; for 2h; |
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