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Cas:83-32-9
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Cas:83-32-9
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inquiryProduct Name: Acenaphthene Synonyms: 1,2-dihydro-acenaphthylen;1,8-dihydroacenaphthalene;1,8-Ethylenenaphthalene1,2-Dihydroacenaphthylene;acenaphtene;Acenaphthcn;Acenaphthylene, 1,2-dihydro-;ethylenenaphtha
Cas:83-32-9
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inquiry1. Best prices with satisfied quality; 2. It's clients' right to choose the package's Courier (EMS, DHL, FedEx, UPS); 3.It's clients' right to choose the packing way for his produccts from many recent effective packing ways;
Product Description Product website: http://www.finerchem.com/pro01en/id/1757.html Product Name Acenaphthene CAS No. 83-32-9
Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
Cas:83-32-9
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Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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moderate price & quick delivery Appearance:white or pale yellow crystalline powder Storage:Keep away of light,cool place Package:100g/bottle,1kg/bottle,25kg/drum or as per your request Application:Polycyclic aromatic hydrocarbons as carcinogeni
Product name: Acenaphthene CAS No.: 83-32-9 Molecule Formula:C5H5ClN2O Molecule Weight:144.56 Purity: 98.0% Package: 25kg/bag Description:White or slight yellow crystalline powder Manufacture Standards:Enterprise Standard
Hangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
CHENGDU YANXI is a comprehensive manufacturer and an international distribution of products throughout the world. Specialized in Scrap metal, Chemical raw materials, Paper products and color industry. We aim to become leading position in global dis
Cas:83-32-9
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Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:83-32-9
Min.Order:1 Kilogram
FOB Price: $112.0
Type:Trading Company
inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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Xiamen Luyunjia Trading Co.,Ltd Package:1kg/bag; 1424kg/drum, or as customer's request. Application:Xiamen Luyunjia Trading Co.,Ltd Transportation:DHL, EMS, FedEx, TNT, AIR, SEA Port:Beijing,Shanghai,Guangzhou ,China main port
Hangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketing of chemicals. We have earned ourselves a good reputation at home an
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China
Conditions | Yield |
---|---|
With tetraethylammonium bromide In ethanol at 60℃; electrolysis, lead cathode; | 100% |
With benzenetellurol In ethanol; ethyl acetate for 4h; Product distribution; Heating; other reagent, reaction time; | 98% |
With iodine; hypophosphorous acid In acetic acid for 24h; Heating; | 98% |
Conditions | Yield |
---|---|
palladium on activated carbon at 250℃; for 2h; | A 93% B 90% |
Conditions | Yield |
---|---|
With hexamethyldistannane; palladium In toluene at 110℃; for 18h; | 90% |
With norborn-2-ene; benzophenone In acetonitrile Irradiation; | 8.1% |
With phenyllithium; benzene |
1,2,3,4-tetrahydro-9H-fluorene
acenaphthylene
A
9H-fluorene
B
acenaphthene
Conditions | Yield |
---|---|
A n/a B 90% |
5-bromoacenaphthene
A
1,1',2,2'-tetrahydro-5,5'-biacenaphthylene
B
acenaphthene
Conditions | Yield |
---|---|
With [2,2]bipyridinyl; nickel dichloride; zinc In N,N-dimethyl-formamide at 70℃; for 3h; Dimerization; dehalogenation; | A 85% B 5% |
With 9,10-phenanthroline; nickel dichloride; zinc In N,N-dimethyl-formamide at 70℃; for 3h; Dehalogenation; dimerization; | A 71% B 15% |
Stage #1: 5-bromoacenaphthene With [2,2]bipyridinyl; nickel dichloride; zinc In N,N-dimethyl-formamide at 70℃; for 6h; Stage #2: With hydrogenchloride In N,N-dimethyl-formamide at 30 - 40℃; for 0.5h; Title compound not separated from byproducts; | A 95 % Chromat. B 5 % Chromat. |
Conditions | Yield |
---|---|
With 4-methyl-morpholine; tetrahydroxydiboron; 5%-palladium/activated carbon In 1,2-dichloro-ethane at 50℃; for 2h; | 81% |
acetic anhydride
acenaphthylene
A
5-ethylacenaphthene
B
1-acenaphthen-3-yl-ethanone
C
5-acetylacenaphthene
D
acenaphthene
Conditions | Yield |
---|---|
With iodine; hypophosphorous acid In acetic acid for 24h; Heating; | A 5% B 40% C 3% D 52% |
5-bromoacenaphthene
carbon monoxide
A
acenaphthene-5-carboxylic acid
B
acenaphthene
Conditions | Yield |
---|---|
With dicobalt octacarbonyl; potassium carbonate; methyloxirane In methanol at 60℃; under 760 Torr; for 6h; | A 50% B n/a |
4-chloro-n-butyric anhydride
acenaphthylene
A
acenaphthene
B
1-Acenaphthen-1-yl-4-chloro-butan-1-one
D
1(2H)-acenaphthylenone
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide electrolysis at -1.7 V (0.1 M TBAI); Further byproducts given; | A 6% B 46% C n/a D 8.5% |
In N,N-dimethyl-formamide electrolysis at -1.7 V (0.1 M TBAI); Further byproducts given; | A 6% B 46% C 8.5% D 8.5% |
4-chloro-n-butyric anhydride
acenaphthylene
A
acenaphthene
B
1-Acenaphthen-1-yl-4-chloro-butan-1-one
D
1(2H)-acenaphthylenone
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide electrolysis at -1.7 V (0.1 M TBAI); Further byproducts given; | A 6% B 46% C 3.5% D 8.5% |
acetic anhydride
acenaphthylene
A
acenaphthene
D
1(2H)-acenaphthylenone
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide electrolysis at -1.7 V (0.1 M TBAI); Further byproducts given; | A 9% B 43% C 18% D n/a |
Conditions | Yield |
---|---|
at 780℃; under 1 Torr; for 0.0833333h; | A 43% B 19% C 37% |
acenaphthene quinone
A
1-acenaphthenol
B
acenaphthene
C
acenaphthylene
Conditions | Yield |
---|---|
With samarium diiodide; water In tetrahydrofuran at 20℃; for 0.00277778h; | A 41% B 26% C 23% |
A
acenaphthene
B
9-Hydroxymethyl-1H-naphtho[1,2-c]furan-3-one
C
acenaphthylene
Conditions | Yield |
---|---|
at 730℃; under 0.03 Torr; for 0.05h; | A 9% B 38% C 12% |
acenaphthene quinone
A
decacyclene
B
1-acenaphthenol
C
acenaphthene
D
acenaphthylene
Conditions | Yield |
---|---|
bis(η6-biphenyl)titanium(0) In toluene at 110℃; for 2h; Further byproducts given; | A 21% B 10% C 11% D 31% |
carbon dioxide
acenaphthylene
methyl iodide
A
acenaphthene
trans-1,2-dicarbomethoxy-1,2-dihydroacenaphthylene
D
1(2H)-acenaphthylenone
Conditions | Yield |
---|---|
1.) electrolysis at -1.7 V (0.1 M TBAI), DMF, -35 deg C; 2) overnight; Yield given. Multistep reaction. Further byproducts given; | A 9% B n/a C 18% D n/a |
acenaphthene
Conditions | Yield |
---|---|
With benzophenone In acetonitrile Irradiation; | 12.3% |
In cyclohexane Irradiation; with a KrF (248 nm) excimer laser; | |
In cyclohexane Irradiation; |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide electrolysis at -1.7 V (0.1 M TBAI); Further byproducts given; | A 9% B 3% C 4% D 11% |
1,8-bis(phenylthiomethyl)-naphthalene
acenaphthene
Conditions | Yield |
---|---|
With benzophenone In acetonitrile Irradiation; | 5.5% |
In cyclohexane Irradiation; with a KrF (248 nm) excimer laser; | 72 % Spectr. |
In cyclohexane Irradiation; |
n-butyl magnesium bromide
phosgene
diethyl ether
3-bromoacenaphthene
acenaphthene
Conditions | Yield |
---|---|
bei Rotglut; |
naphthalene
ethene
A
2,2'-binaphthalene
B
phenanthrene
C
acenaphthene
Conditions | Yield |
---|---|
beim Leiten durch ein gluehendes Rohr; |
Conditions | Yield |
---|---|
With sulfur at 180℃; |
cis-acenaphthene-1,2-diol
(+/-)-(2aξH)-2a.3.4.5-tetrahydro-acenaphthenediol-(1r.2c)
B
acenaphthene
Conditions | Yield |
---|---|
With hydrogenchloride; ethanol; iron(III) chloride at 50℃; Hydrogenation.weiteres Reagens: Platin; |
Conditions | Yield |
---|---|
With acetic acid; zinc |
Conditions | Yield |
---|---|
With palladium on activated charcoal |
Conditions | Yield |
---|---|
With palladium on activated charcoal |
(8-carboxy-[1]naphthyl)-glyoxylic acid
acenaphthene
Conditions | Yield |
---|---|
With phosphorus; hydrogen iodide |
acenaphthene-1,5-dicarboxylic acid
A
acenaphthene-5-carboxylic acid
B
acenaphthene
Conditions | Yield |
---|---|
at 280℃; |
Conditions | Yield |
---|---|
at 200℃; im Rohr; |
Conditions | Yield |
---|---|
100% | |
aluminum nickel | 100% |
Rh/C | 100% |
acenaphthene
9,9,10,10-tetradeuteroacenaphthene tetradeuteroacenaphthene
Conditions | Yield |
---|---|
With dimethylsulfoxide-d6; sodium hydride at 78℃; for 22h; | 100% |
With sodium dimsylate-d5; dimethylsulfoxide-d6 at 75℃; for 20h; | |
With water-d2; sodium hydride In dimethylsulfoxide-d6 | 99.8 %Spectr. |
With dimethylsulfoxide-d6; sodium hydride |
Conditions | Yield |
---|---|
With oxygen at 300 - 330℃; | 100% |
With oxygen at 300 - 330℃; | 100% |
With oxygen at 300 - 330℃; | 100% |
acenaphthene
Conditions | Yield |
---|---|
With hydrogen; palladium 10% on activated carbon at 130℃; under 3000.3 - 7500.75 Torr; for 4 - 10h; Product distribution / selectivity; | 99.5% |
Conditions | Yield |
---|---|
With cerium(III) chloride heptahydrate; dihydrogen peroxide; acetic acid; sodium bromide In water at 20℃; for 3h; Reagent/catalyst; Temperature; | 97.5% |
With N-Bromosuccinimide In N,N-dimethyl-formamide at 20℃; for 3h; | 97% |
With N-Bromosuccinimide In N,N-dimethyl-formamide at 20℃; | 96% |
chloro-trimethyl-silane
acenaphthene
4,5,7,8-tetrakis(trimethylsilyl)-4,5,7,8-tetrahydroacenaphthene
Conditions | Yield |
---|---|
With lithium In tetrahydrofuran at 0 - 5℃; | 97% |
Conditions | Yield |
---|---|
With Iron(III) nitrate nonahydrate; acetic acid at 35℃; for 5h; Reagent/catalyst; Temperature; | 96% |
With bismuth(III) nitrate; acetic anhydride; acetic acid at 20℃; for 6h; Reagent/catalyst; Temperature; | 96.5% |
With nitric acid In dichloromethane at 10℃; for 1.33333h; | 90% |
Conditions | Yield |
---|---|
With hydrogen In n-heptane at 150 - 200℃; under 15001.5 Torr; for 1h; Autoclave; | 96.2% |
With Raney Ni-Al In potassium hydroxide; water at 90℃; for 6.5h; Reduction; | 93% |
With cobalt(II) chloride hexahydrate; lithium In tetrahydrofuran at 25℃; for 2h; Birch reaction; Inert atmosphere; regioselective reaction; | 88% |
acenaphthene
7,7',8,8'-tetracyanoquinodimethane
A
9-Acenaphthyl<4-(dicyanomethyl)phenyl>dicyanomethane
B
acenaphthylene
Conditions | Yield |
---|---|
for 0.0833333h; Heating; | A 95.5% B n/a |
chloral hydrate
acenaphthene
1,1,1-trichloro-2,2-di(acenaphth-4-yl)ethane
Conditions | Yield |
---|---|
With sulfuric acid In chloroform 1.) 20 deg C, 1 h, 2.) 25 deg C, 3 h; | 94% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20℃; for 3h; | 93.6% |
Conditions | Yield |
---|---|
With sodium dichromate | 92% |
With copper(II) acetate dihydrate; manganese(II) acetate dihydrate; oxygen; acetic acid; potassium bromide at 105℃; | 90% |
With sodium dichromate In acetic acid at 75℃; for 8h; | 80% |
2,2-bis(4-chlorocarbonylphenyl)-hexafluoropropane
acenaphthene
(4-{1-[4-(Acenaphthene-5-carbonyl)-phenyl]-2,2,2-trifluoro-1-trifluoromethyl-ethyl}-phenyl)-acenaphthen-5-yl-methanone
Conditions | Yield |
---|---|
With aluminium trichloride In 1,2-dichloro-ethane 1.) 0 -> 60 deg C, 2 h, 2.) 60 deg C, 1 h; | 92% |
1,2,4,5-tetracyanobenzene
acenaphthene
A
5-(acenapthen-1-yl)benzene-1,2,4-tricarbonitrile
B
4,6-di(acenaphthen-1-yl)benzene-1,3-dicarbonitrile
C
acenaphthene quinone
Conditions | Yield |
---|---|
In acetonitrile for 12h; Product distribution; Mechanism; Irradiation; other solvents, irradiation at different wave-length; | A 90% B 1.5% C n/a |
In acetonitrile for 12h; Irradiation; | A 90% B 1.5% C 2 mg |
acenaphthene
trifluoromethanesulphonyloxy-methylene-N,N-dimethyliminium trifluoromethanesulphonate
acenaphthene-5-carbaldehyde
Conditions | Yield |
---|---|
In chloroform at 130℃; for 72h; | 90% |
1,8-bis(2,6-dichlorophenylethynyl)naphthalene
acenaphthene
7,14-bis(2,6-dichlorophenyl)acenaphtho[1,2-k]fluoranthene
Conditions | Yield |
---|---|
Stage #1: 1,8-bis(2,6-dichlorophenylethynyl)naphthalene; acenaphthene With tris(triphenylphosphine)rhodium(l) chloride In 5,5-dimethyl-1,3-cyclohexadiene at 110℃; for 60h; Inert atmosphere; Sealed tube; Stage #2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone In 5,5-dimethyl-1,3-cyclohexadiene at 20 - 110℃; Inert atmosphere; Sealed tube; | 90% |
acenaphthene
N,N-dimethyl-formamide
1,2-dihydroacenaphthylene-3-carbaldehyde
Conditions | Yield |
---|---|
With silica gel; trichlorophosphate for 0.025h; Formylation; Microwave irradiation (300 W); | 89% |
Conditions | Yield |
---|---|
With aluminum (III) chloride In 1,1,2,2-tetrachloroethane at 20℃; | 87% |
With carbon disulfide; aluminium trichloride |
acenaphthene
N,N-dimethyl-formamide
acenaphthene-5-carbaldehyde
Conditions | Yield |
---|---|
With trichlorophosphate at 90 - 95℃; for 3h; Vilsmeier Reaction; | 85% |
With trichlorophosphate at 70℃; for 3h; | 57% |
With trichlorophosphate at 90 - 95℃; for 3.33h; | 46.74% |
acenaphthene
1,2-dibromoacenaphthylene
Conditions | Yield |
---|---|
With N-Bromosuccinimide; dibenzoyl peroxide In tetrachloromethane for 4h; Inert atmosphere; Reflux; | 84% |
With N-Bromosuccinimide; benzoic acid anhydride | |
With N-Bromosuccinimide; dibenzoyl peroxide In tetrachloromethane for 2h; Reflux; | |
With N-Bromosuccinimide |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; V2O5/TiO2 In water at 80℃; for 8h; Sealed tube; Green chemistry; | 82% |
With potassium permanganate; sulfuric acid; triethylamine In chloroform Ambient temperature; | 76% |
With tetrakis(pyridine)silver(II) peroxodisulfate In acetonitrile for 1h; Heating; | 60% |
Conditions | Yield |
---|---|
With benzeneseleninic anhydride In chlorobenzene at 120℃; for 24h; | 81% |
With sodium dichromate; acetic acid ; cerium (IV)-acetate; acetic acid at 40℃; Reagens 4: CeCl3; | |
With ammonium dichromate; acetic acid at 100℃; |
Conditions | Yield |
---|---|
With tin(IV) chloride at 140℃; | 80% |
With tin(IV) chloride |
Conditions | Yield |
---|---|
With 2,3-dicyano-5,6-dichloro-p-benzoquinone In toluene for 24h; Reflux; | 80% |
With oxygen; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium nitrite In toluene at 120℃; under 9750.98 Torr; for 8h; | 77% |
With manganese(IV) oxide In benzene for 30h; Heating; | 41% |
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