Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
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inquiry1-Acenaphthenone Basic information Product Name: 1-Acenaphthenone Synonyms: ACENAPHTHENONE;AKOS 94209;1-ACENAPHTHENONE;AURORA KA-3379;1(2H)-Acenaphthylenone;2-Acenaphthenone;7-Acenaphthe
Cas:2235-15-6
Min.Order:1 Metric Ton
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Type:Lab/Research institutions
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:2235-15-6
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiry1-Acenaphthenone CAS:2235-15-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermed
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Min.Order:1 Gram
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:2235-15-6
Min.Order:1 Kilogram
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:2235-15-6
Min.Order:10 Gram
FOB Price: $100.0
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:2235-15-6
Min.Order:1 Kilogram
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inquiry1-AcenaphthenoneAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier
high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
We product this chemical more than 10 years . We are very experience to export it to many countries, Our superior & stable quality , competitive price gain warm reception from our customers. Application:Pharm intermediate
1-Acenaphthenone cas 2235-15-6Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
Best quality with low price Storage:ln stock Package:25kg/Barrel Application:Chemicals Transportation:Express/Sea/Air Port:Shanghai
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
good quality, competitive price, thoughtful after sale serviceAppearance:white powder Storage:Keep it in dry,shady and cool place Package:250mg Application:Pharma;Industry;Agricultural;chemical reaserch Transportation:by express or by sea Port:Any po
Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Best Seller, High Quality, Competitive Price, Fast Delivery, Quick ResponseAppearance:powder, or liquid Storage:Stored in room temperature, ventilated place Package:Bottle, barrel, cargo, container, etc. Application:Pharmaceuticals, intermediates, AP
Our mission is to provide high-quality and innovative products to our customers. By offering a broad range of products, custom synthesis and personalized services, Bide can help scientists speeding up their research in the chemical and pharmaceutical
1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G
Cas:2235-15-6
Min.Order:10 Milligram
Negotiable
Type:Lab/Research institutions
inquiryConditions | Yield |
---|---|
With oxygen; isobutyraldehyde In acetonitrile at 60℃; for 3h; | 98% |
With dinitrogen monoxide; dioxo(tetramesitylporphyrinato)ruthenium(VI) In fluorobenzene at 100℃; under 7500.6 Torr; | 87% |
With iodosylbenzene; iron(III) tetraphenylporphyrin In dichloromethane for 1h; | 58% |
With iodosylbenzene; μ-oxo dimer of iron(III)porphyrinate In methanol at 21.9℃; for 3h; Product distribution; Mechanism; catalysts also Fe(III)porphyrinate, Fe(III)tetraphenylporphyrinate; protic and aprotic solvents; inhibition effect by phenanthrene; by-products; | 28% |
With dinitrogen monoxide at 300℃; under 367754 Torr; |
Conditions | Yield |
---|---|
With potassium dichromate; sulfuric acid In diethyl ether; water at 0℃; for 0.666667h; | 97% |
With dinitrogen monoxide; dioxo(tetramesitylporphyrinato)ruthenium(VI) In 1,2-dichloro-ethane at 120℃; under 7600 Torr; for 7.5h; | 95% |
With dinitrogen monoxide; dioxo(tetramesitylporphyrinato)ruthenium(VI) In 1,2-dichloro-ethane at 120℃; under 7500.6 Torr; for 7.5h; | 95% |
Conditions | Yield |
---|---|
With dibenzoyl peroxide In dichloromethane for 3h; Ambient temperature; Irradiation; | A n/a B 84% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; V2O5/TiO2 In water at 80℃; for 8h; Sealed tube; Green chemistry; | 82% |
With potassium permanganate; sulfuric acid; triethylamine In chloroform Ambient temperature; | 76% |
With tetrakis(pyridine)silver(II) peroxodisulfate In acetonitrile for 1h; Heating; | 60% |
acenaphthene quinone
A
decacyclene
B
2-hydroxyacenaphthylen-1-one
C
1(2H)-acenaphthylenone
Conditions | Yield |
---|---|
With TiCl3-1,2-dimethoxyethane; copper; zinc In 1,2-dimethoxyethane for 1h; Heating; | A n/a B 80% C 5% |
1-formyl-2-(1-pyrrolidinyl)acenaphthylene
1(2H)-acenaphthylenone
Conditions | Yield |
---|---|
With hydrogenchloride In 1,4-dioxane for 0.5h; Heating; | 62% |
methanol
acenaphthene
A
1-methoxyacenaphthene
B
1-acenaphthenol
C
1(2H)-acenaphthylenone
Conditions | Yield |
---|---|
With ammonium cerium(IV) nitrate; oxygen In water at 20℃; for 0.0833333h; | A 14% B 12% C 59% |
Conditions | Yield |
---|---|
With aluminum (III) chloride In dichloromethane at 20℃; for 3h; | 58% |
With aluminium trichloride In carbon disulfide | |
With aluminum (III) chloride In carbon disulfide for 2h; Inert atmosphere; Reflux; |
Conditions | Yield |
---|---|
With N-hydroxyphthalimide; 1,4-diamino-2,3-dichloroanthraquinone; oxygen In acetonitrile at 80℃; under 1875.15 - 2250.18 Torr; for 10h; | A 25 % Chromat. B 54% |
With N-hydroxyphthalimide; bromine; oxygen; acridine yellow In acetonitrile at 100℃; under 2250.18 Torr; for 24h; | |
With Cr2O4(2-)*Cu(2+); dihydrogen peroxide In acetonitrile at 50℃; for 10h; |
1-hydroperoxy-1,2-dihydroacenaphthylene
1(2H)-acenaphthylenone
Conditions | Yield |
---|---|
With perchloric acid In methanol at 60℃; for 2h; | 50% |
With sodium hydroxide In methanol; water at 30℃; Rate constant; |
2-diazoacenaphthen-1-one
A
1,1'-Bi(acenaphthen-1-ylidene)-2,2'-dione
B
1,2-acenaphthenothiophene
D
1(2H)-acenaphthylenone
Conditions | Yield |
---|---|
With Lawessons reagent; N,N,N,N,N,N-hexamethylphosphoric triamide In benzene Heating; | A 17% B 12% C 48% D 13% |
4-chloro-n-butyric anhydride
acenaphthylene
A
acenaphthene
B
1-Acenaphthen-1-yl-4-chloro-butan-1-one
D
1(2H)-acenaphthylenone
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide electrolysis at -1.7 V (0.1 M TBAI); Further byproducts given; | A 6% B 46% C n/a D 8.5% |
In N,N-dimethyl-formamide electrolysis at -1.7 V (0.1 M TBAI); Further byproducts given; | A 6% B 46% C 8.5% D 8.5% |
4-chloro-n-butyric anhydride
acenaphthylene
A
acenaphthene
B
1-Acenaphthen-1-yl-4-chloro-butan-1-one
D
1(2H)-acenaphthylenone
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide electrolysis at -1.7 V (0.1 M TBAI); Further byproducts given; | A 6% B 46% C 3.5% D 8.5% |
acetic anhydride
acenaphthylene
A
acenaphthene
D
1(2H)-acenaphthylenone
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide electrolysis at -1.7 V (0.1 M TBAI); Further byproducts given; | A 9% B 43% C 18% D n/a |
acenaphthene
A
(R)-1,2-dihydroacenaphthylen-1-ol
B
(S)-(+)-1,2-dihydroacenaphthylen-1-ol
C
1(2H)-acenaphthylenone
Conditions | Yield |
---|---|
With 5-chloro-4,9-(chlorobenzene-2,3-diyl)-2,4-dihydroxy-3a,4,9,9a-tetrahydro-1H-benzo[f]isoindole-1,3(2H)-dione; oxygen; cobalt(II) acetate In acetonitrile at 60℃; under 760.051 Torr; for 10h; | A n/a B n/a C 35% |
2-diazoacenaphthen-1-one
A
1,8-Naphthalic anhydride
B
1,1'-Bi(acenaphthen-1-ylidene)-2,2'-dione
C
1(2H)-acenaphthylenone
Conditions | Yield |
---|---|
With oxygen; isopropyl alcohol for 2h; Ambient temperature; Irradiation; | A 25% B 2% C 24% |
carbon dioxide
acenaphthylene
methyl iodide
A
acenaphthene
trans-1,2-dicarbomethoxy-1,2-dihydroacenaphthylene
D
1(2H)-acenaphthylenone
Conditions | Yield |
---|---|
1.) electrolysis at -1.7 V (0.1 M TBAI), DMF, -35 deg C; 2) overnight; Yield given. Multistep reaction. Further byproducts given; | A 9% B n/a C 18% D n/a |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide electrolysis at -1.7 V (0.1 M TBAI); Further byproducts given; | A 3% B 4% C 11% D 8% |
1(2H)-acenaphthylenone
Conditions | Yield |
---|---|
In acetonitrile for 5h; Irradiation; | 11% |
C
1(2H)-acenaphthylenone
Conditions | Yield |
---|---|
With acenaphthylene anion radical In N,N-dimethyl-formamide Yield given. Yields of byproduct given; | A n/a B n/a C 7% |
Conditions | Yield |
---|---|
With PPA | |
Multi-step reaction with 2 steps 1: SOCl2 2: AlCl3 / CS2 View Scheme | |
Stage #1: naphth-1-yl acetic acid With thionyl chloride; pyridine In dichloromethane at 20℃; for 3h; Friedal Craft reaction; Stage #2: With carbon disulfide; aluminum (III) chloride |
2-acetylacenaphthenone
diethyl ether
A
acetophenone
B
1(2H)-acenaphthylenone
acenaphthenequinone monoxime
1(2H)-acenaphthylenone
Conditions | Yield |
---|---|
With hydrogenchloride; iron; acetic acid |
1,2-dibromoacenaphthene
A
1,1'-biacenaphthylenyliden-2-one
B
1(2H)-acenaphthylenone
Conditions | Yield |
---|---|
With hydrogenchloride; ethanol |
2,2-Dichlor-1(2H)-acenaphthenon
1(2H)-acenaphthylenone
Conditions | Yield |
---|---|
With acetic acid; zinc |
1,2-dihydroacenaphthylene-1,2-diol
1(2H)-acenaphthylenone
Conditions | Yield |
---|---|
With sodium ethanolate; methyl iodide | |
With hydrogenchloride |
2-phenylimino-acenaphthen-1-one
1(2H)-acenaphthylenone
Conditions | Yield |
---|---|
With hydrogenchloride; iron; acetic acid |
Conditions | Yield |
---|---|
Einwirkung von Sonnenlicht; |
Conditions | Yield |
---|---|
With aluminium trichloride |
Conditions | Yield |
---|---|
With trifluoroacetic acid In dichloromethane at 20℃; | 99% |
1(2H)-acenaphthylenone
(S)-(+)-1,2-dihydroacenaphthylen-1-ol
Conditions | Yield |
---|---|
With formic acid; C29H38N3O2RuS; triethylamine In ethyl acetate at 40℃; for 24h; Reagent/catalyst; Inert atmosphere; enantioselective reaction; | 96% |
With (+)-β-chlorodiisopinocampheylborane In tetrahydrofuran at -25℃; for 11h; under argon atmosphere; | |
With borane-THF; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole In tetrahydrofuran; dichloromethane; toluene at -30℃; |
Conditions | Yield |
---|---|
With hydrogenchloride In acetic acid for 3h; | 95% |
Conditions | Yield |
---|---|
With N-Bromosuccinimide; dimethyl sulfoxide Ambient temperature; | 95% |
With N-Bromosuccinimide In dimethyl sulfoxide for 24h; Product distribution; Ambient temperature; further halogenating agents; variation of concentration, temperature and time; | 95% |
Multi-step reaction with 2 steps 1: ethanol; aqueous NaOH-solution 2: diluted aqueous sulfuric acid View Scheme |
1(2H)-acenaphthylenone
(R)-1,2-dihydroacenaphthylen-1-ol
Conditions | Yield |
---|---|
With formic acid; C38H40ClN2O3RhS; triethylamine In neat (no solvent) at 24 - 30℃; for 5.5h; Reagent/catalyst; Inert atmosphere; enantioselective reaction; | 95% |
With (-)-diisopinocamphenylborane chloride In tetrahydrofuran at -25℃; for 11h; under argon atmosphere; |
Conditions | Yield |
---|---|
With hydrogen In methanol at 100℃; under 30003 Torr; Temperature; Autoclave; | 94.2% |
With sodium tetrahydroborate In methanol at 20℃; for 2h; | 87% |
With hydrogen; nickel at 230℃; |
N,N-dimethyl-formamide
1(2H)-acenaphthylenone
2-bromoacenaphthylene-1-carbaldehyde
Conditions | Yield |
---|---|
Stage #1: N,N-dimethyl-formamide With phosphorus tribromide In chloroform at 0 - 20℃; for 0.583333h; Stage #2: 1(2H)-acenaphthylenone In chloroform at 20℃; for 12h; | 94% |
With phosphorus tribromide | |
Stage #1: N,N-dimethyl-formamide With phosphorus tribromide In chloroform at 20℃; Cooling with ice; Stage #2: 1(2H)-acenaphthylenone In chloroform at 20℃; for 8.16667h; | |
With phosphorus tribromide In chloroform at 20℃; for 12h; | |
Stage #1: N,N-dimethyl-formamide With phosphorus(V) oxybromide In chloroform at 0 - 20℃; for 1.5h; Inert atmosphere; Stage #2: 1(2H)-acenaphthylenone In chloroform at 20℃; for 16h; | 6.0 g |
1(2H)-acenaphthylenone
2-bromoacenaphthylen-1(2H)-one
Conditions | Yield |
---|---|
With copper(ll) bromide In ethyl acetate Reflux; | 91% |
With N-Bromosuccinimide; dichloromethane | 59% |
With carbon disulfide; bromine |
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol for 1h; Ambient temperature; | 91% |
Conditions | Yield |
---|---|
With hydrogenchloride In acetic acid for 3h; | 91% |
Conditions | Yield |
---|---|
Stage #1: ethyl trifluoroacetate, With sodium hydride In tetrahydrofuran at 20℃; for 0.5h; Stage #2: 1(2H)-acenaphthylenone In tetrahydrofuran for 2h; Reflux; | 89% |
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran at 65℃; for 3h; Inert atmosphere; | 89% |
2-chloro-benzaldehyde
1(2H)-acenaphthylenone
O-chlorobenzylidineacenaphthenone
Conditions | Yield |
---|---|
With alkaline hydroxide In ethanol at 0℃; | 87.7% |
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol for 1h; Ambient temperature; | 87% |
6-(naphthalen-1-yl)-2-oxo-4-(piperidin-1-yl)-2H-pyran-3-carbonitrile
1(2H)-acenaphthylenone
10-(naphthalen-1-yl)-8-(piperidin-1-yl)fluoranthene-7-carbonitrile
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran; mineral oil at 20℃; for 0.216667h; | 85% |
1(2H)-acenaphthylenone
6-(4-methoxyphenyl)-2-oxo-4-(piperidin-1-yl)-2H-pyran-3-carbonitrile
10-(4-methoxyphenyl)-8-(piperidin-1-yl)fluoranthene-7-carbonitrile
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran; mineral oil at 20℃; for 0.2h; | 84% |
1(2H)-acenaphthylenone
6-(4-methoxyphenyl)-2-oxo-4-(piperidin-1-yl)-2H-pyran-3-carbonitrile
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran; mineral oil at 25℃; for 0.25h; | 84% |
trifluorormethanesulfonic acid
4,4-dimethyl-1-phenyl-1-penten-3-one
1(2H)-acenaphthylenone
4-phenyl-2-t-butyl-1-oxoniafluoranthene trifluoromethanesulphonate
Conditions | Yield |
---|---|
at 100℃; for 5h; | 83% |
Conditions | Yield |
---|---|
With triethylsilane; 2C2H3F3O*BF3 In dichloromethane at 20℃; for 4h; | 82% |
With nickel; decalin at 230℃; Hydrogenation; |
Conditions | Yield |
---|---|
With aluminium trichloride In dichloromethane | 82% |
With toluene-4-sulfonic acid In benzene for 12h; Heating; |
2-oxo-4-(piperidin-1-yl)-6-(pyren-1-yl)-2H-pyran-3-carbonitrile
1(2H)-acenaphthylenone
8-(piperidin-1-yl)-10-(pyren-1-yl)fluoranthene-7-carbonitrile
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran; mineral oil at 20℃; for 0.25h; | 82% |
6-(1-naphthyl)-2-oxo-4-pyrrolidin-1-yl-2H-pyran-3-carbonitrile
1(2H)-acenaphthylenone
10-(naphthalen-1-yl)-8-(pyrrolidin-1-yl)fluoranthene-7-carbonitrile
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran; mineral oil at 20℃; for 0.2h; | 82% |
1(2H)-acenaphthylenone
2-oxo-4-(piperidin-1-yl)-6-(thiophen-2-yl)-2H-pyran-3-carbonitrile
10-phenyl-8-(pyrrolidin-1-yl)fluoranthene-7-carbonitrile
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran; mineral oil at 20℃; for 0.2h; | 82% |
2-oxo-6-phenyl-4-(pyrrolidin-1-yl)-2H-pyran-3-carbonitrile
1(2H)-acenaphthylenone
10-phenyl-8-(pyrrolidin-1-yl)fluoranthene-7-carbonitrile
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran; mineral oil at 27℃; for 0.2h; | 82% |
1(2H)-acenaphthylenone
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran; mineral oil at 25℃; for 0.25h; | 81% |
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