CAS No.654636-62-1,3,7-Dioxa-4-aza-6-phosphanonanoic acid, 4,5-bis(1,1-dimethylethyl)-6-ethoxy-2,2-dimethyl-, 6-oxide Suppliers

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N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide CAS:654636-62-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, producti

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3,7-Dioxa-4-aza-6-phosphanonanoic acid, 4,5-bis(1,1-dimethylethyl)-6-ethoxy-2,2-dimethyl-, 6-oxide

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3,7-Dioxa-4-aza-6-phosphanonanoic acid, 4,5-bis(1,1-dimethylethyl)-6-ethoxy-2,2-dimethyl-, 6-oxide

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Nanjing Raymon Biotech Co., Ltd.

3,7-Dioxa-4-aza-6-phosphanonanoic acid, 4,5-bis(1,1-dimethylethyl)-6-ethoxy-2,2-dimethyl-, 6-oxideAppearance:Off white to slight yellow solid Storage:Store in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical

3,7-Dioxa-4-aza-6-phosphanonanoic acid, 4,5-bis(1,1-dimethylethyl)-6-ethoxy-2,2-dimethyl-, 6-oxide

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Synthetic route

: 548761-51-9
N,N-diethyl-S-(α,α-dimethyl-α-acetic acid)dithiocarbamate

: 188526-94-5
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)aminoxyl

: 654636-62-1
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide

Conditions

Conditions	Yield
In ethanol at 10℃; for 4.5h; UV-irradiation;	95%

: 2,2'-azobis(isobutyric acid) disodium salt

: 188526-94-5
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)aminoxyl

: 654636-62-1
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide

Conditions

Conditions	Yield
In methanol; water at 10℃; for 4.5h; UV-irradiation;	93%

: 548761-51-9
N,N-diethyl-S-(α,α-dimethyl-α-acetic acid)dithiocarbamate

: 188526-94-5
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)aminoxyl

A: 97-77-8
disulfiram

B: 654636-62-1
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide

Conditions

Conditions	Yield
In ethanol at 20℃; for 4h; Product distribution / selectivity; Inert atmosphere; Photolysis;	A n/a B 90%

...Expand

: 2052-01-9
2-bromo-2-methylpropionic acid

: 188526-94-5
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)aminoxyl

: 654636-62-1
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide

Conditions

Conditions	Yield
Stage #1: 2-bromo-2-methylpropionic acid; N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)aminoxyl With N,N,N',N'',N'''-pentamethyldiethylenetriamine; copper; copper(I) bromide In methanol at 20℃; for 4h; Inert atmosphere; Stage #2: With hydrogenchloride In methanol; water at 12℃; pH=1.5; Product distribution / selectivity;	86%
With N,N,N',N'',N'''-pentamethyldiethylenetriamine; copper; copper(I) bromide In benzene at 20℃; for 3h;	75%
With N,N,N',N'',N'''-pentamethyldiethylenetriamine; copper; copper(I) bromide In toluene at 20℃; for 1.5h;	60%

: 2-methyl-2-[N-(diethoxyphosphoryl-2,2-dimethylpropyl)aminoxy]propionic acid, sodium salt

: 7732-18-5
water

: 654636-62-1
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide

Conditions

Conditions	Yield
With hydrogenchloride In methanol; water

: 654636-62-1
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide

: C24H43N2O6P

Conditions

Conditions	Yield
In tetrahydrofuran at 100℃; for 1h; Schlenk technique; Inert atmosphere;	85%

: 75-03-6
ethyl iodide

: 654636-62-1
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide

: 1034132-98-3
ethyl 2-((tert-butyl(1-(diethoxyphosphoryl)-2,2-dimethylpropyl)amino)oxy)-2-methylpropanoate

Conditions

Conditions	Yield
Stage #1: N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide With 1,8-diazabicyclo[5.4.0]undec-7-ene In benzene Inert atmosphere; Stage #2: ethyl iodide In benzene at 20℃; for 24h; Inert atmosphere;	78%

: 74-88-4
methyl iodide

: 654636-62-1
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide

: methyl 2-methyl-2-[N-tert-butyl-N-(1-diethoxyphosphoryl-2,2-dimethylpropyl)aminoxy]propionate

Conditions

Conditions	Yield
Stage #1: N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide With 1,8-diazabicyclo[5.4.0]undec-7-ene In benzene Inert atmosphere; Stage #2: methyl iodide In benzene at 20℃; for 24h; Inert atmosphere;	77%

: 1680-21-3
2-propenoic acid 1,2 ethanediylbis(oxy-2,1-ethanediyl) ester

: 654636-62-1
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide

: 871982-25-1
C46H90O18N2P2

Conditions

Conditions	Yield
In tert-butyl alcohol at 100℃; for 1h;	70%

: 141-32-2
acrylic acid n-butyl ester

: 654636-62-1
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide

: 2,2-dimethyl-4-[N-tert-butyl-N-(1-diethoxyphosphoryl-2,2-dimethylpropyl)aminoxy]-4-n-butoxycarbonylbutanoic acid

Conditions

Conditions	Yield
In tert-butyl alcohol at 80℃; for 6h;	65%
In tert-butyl alcohol at 100℃; for 1.25h; Inert atmosphere;	45%

: 654636-62-1
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide

: 647018-77-7
2-{[(4-bromo-benzenesulfonyl)-phenyl-amino]-methyl}-acrylic acid ethyl ester

: 1-(4-bromo-benzenesulfonyl)-3-(2-carboxy-2-methyl-propyl)-2,3-dihydro-1H-indole-3-carboxylic acid ethyl ester

Conditions

Conditions	Yield
In tert-butyl alcohol at 70℃; for 12h;	62%

: 22421-62-1
N-(4-benzoylphenyl)acrylamide

: 654636-62-1
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide

: 1304668-93-6
C33H49N2O8P

Conditions

Conditions	Yield
In tetrahydrofuran at 100℃; for 1h; Inert atmosphere;	60%

: 654636-62-1
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide

: 2-{[tert-butoxycarbonyl-(4-nitro-phenyl)-amino]-methyl}-acrylic acid ethyl ester

: 3-(2-carboxy-2-methyl-propyl)-5-nitro-2,3-dihydro-indole-1,3-dicarboxylic acid 1-tert-butyl ester 3-ethyl ester

Conditions

Conditions	Yield
In tert-butyl alcohol at 70℃; for 12h;	58%

: 106-95-6
allyl bromide

: 654636-62-1
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide

: 1393670-68-2
allyl 2-((tert-butyl(1-(diethoxyphosphoryl)-2,2-dimethylpropyl)amino)oxy)-2-methylpropanoate

Conditions

Conditions	Yield
Stage #1: N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide With 1,8-diazabicyclo[5.4.0]undec-7-ene In benzene Inert atmosphere; Stage #2: allyl bromide In benzene at 20℃; for 24h; Inert atmosphere;	57%

: 4-acryloylbenzophenone

: 654636-62-1
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide

: 1304668-94-7
C33H48NO9P

Conditions

Conditions	Yield
In tetrahydrofuran at 100℃; for 1h; Inert atmosphere;	55%

: 654636-62-1
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide

: 647018-78-8
2-{[(4-bromo-benzenesulfonyl)-(4-methoxy-phenyl)-amino]-methyl}-acrylic acid ethyl ester

: 1-(4-bromo-benzenesulfonyl)-3-(2-carboxy-2-methyl-propyl)-5-methoxy-2,3-dihydro-1H-indole-3-carboxylic acid ethyl ester

Conditions

Conditions	Yield
In tert-butyl alcohol at 70℃; for 18h;	54%

: 647018-76-6
2-{[tert-butoxycarbonyl-(4-methoxy-phenyl)-amino]-methyl}-acrylic acid ethyl ester

: 654636-62-1
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide

: 3-(2-carboxy-2-methyl-propyl)-5-methoxy-2,3-dihydro-indole-1,3-dicarboxylic acid 1-tert-butyl ester 3-ethyl ester

Conditions

Conditions	Yield
In tert-butyl alcohol at 70℃; for 18h;	48%

: 647018-73-3
2-[(methyl-phenyl-amino)-methyl]-acrylic acid ethyl ester

: 654636-62-1
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide

: 3-(2-carboxy-2-methyl-propyl)-1-methyl-2,3-dihydro-1H-indole-3-carboxylic acid ethyl ester

Conditions

Conditions	Yield
In tert-butyl alcohol at 70℃; for 12h;	47%

: 647018-75-5
2-[(tert-butoxycarbonyl-phenyl-amino)-methyl]-acrylic acid ethyl ester

: 654636-62-1
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide

: 3-(2-carboxy-2-methyl-propyl)-2,3-dihydro-indole-1,3-dicarboxylic acid 1-tert-butyl ester 3-ethyl ester

Conditions

Conditions	Yield
In tert-butyl alcohol at 70℃; for 12h;	45%

: 1668-10-6
glycinamide hydrochloride

: 654636-62-1
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide

: 1228178-48-0
C19H40N3O6P

Conditions

Conditions	Yield
With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 1.5h; Inert atmosphere;	45%

: 647018-74-4
2-{[(4-methoxy-phenyl)-methyl-amino]-methyl}-acrylic acid ethyl ester

: 654636-62-1
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide

: 3-(2-carboxy-2-methyl-propyl)-5-methoxy-1-methyl-2,3-dihydro-1H-indole-3-carboxylic acid ethyl ester

Conditions

Conditions	Yield
In tert-butyl alcohol at 70℃; for 12h;	38%

: C52H83N12O13Pol

: 1563177-07-0
C9H14N4O4

: 654636-62-1
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide

: 1563177-09-2
C64H108N17O18P

Conditions

Conditions	Yield
Stage #1: C52H83N12O13Pol; N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In 1-methyl-pyrrolidin-2-one fluorenylmethoxycarbonyl (Fmoc) amide resin; Stage #2: C9H14N4O4 In N,N-dimethyl-formamide at 20 - 70℃; for 72.5h; fluorenylmethoxycarbonyl (Fmoc) amide resin; Inert atmosphere; Stage #3: With trifluoroacetic acid In water for 1.83333h; fluorenylmethoxycarbonyl (Fmoc) amide resin;	35%

Yield

Stage #1: C52H83N12O13Pol; N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In 1-methyl-pyrrolidin-2-one fluorenylmethoxycarbonyl (Fmoc) amide resin;
Stage #2: C9H14N4O4 In N,N-dimethyl-formamide at 20 - 70℃; for 72.5h; fluorenylmethoxycarbonyl (Fmoc) amide resin; Inert atmosphere;
Stage #3: With trifluoroacetic acid In water for 1.83333h; fluorenylmethoxycarbonyl (Fmoc) amide resin;

35%

...Expand

: C52H83N12O13Pol

: 1563177-08-1
C21H37N9O7

: 654636-62-1
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide

: 1563177-10-5
C76H131N22O21P

Conditions

Conditions	Yield
Stage #1: C52H83N12O13Pol; N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In 1-methyl-pyrrolidin-2-one fluorenylmethoxycarbonyl (Fmoc) amide resin; Stage #2: C21H37N9O7 In N,N-dimethyl-formamide at 20 - 70℃; fluorenylmethoxycarbonyl (Fmoc) amide resin; Inert atmosphere; Stage #3: With trifluoroacetic acid In water for 1.83333h; fluorenylmethoxycarbonyl (Fmoc) amide resin; chemoselective reaction;	30%

Yield

Stage #1: C52H83N12O13Pol; N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In 1-methyl-pyrrolidin-2-one fluorenylmethoxycarbonyl (Fmoc) amide resin;
Stage #2: C21H37N9O7 In N,N-dimethyl-formamide at 20 - 70℃; fluorenylmethoxycarbonyl (Fmoc) amide resin; Inert atmosphere;
Stage #3: With trifluoroacetic acid In water for 1.83333h; fluorenylmethoxycarbonyl (Fmoc) amide resin; chemoselective reaction;

30%

...Expand

: C52H83N12O13Pol

: C15H26N6O5

: 654636-62-1
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide

: 1563177-12-7
C70H120N19O19P

Conditions

Conditions	Yield
Stage #1: C52H83N12O13Pol; N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In 1-methyl-pyrrolidin-2-one fluorenylmethoxycarbonyl (Fmoc) amide resin; Stage #2: C15H26N6O5 In N,N-dimethyl-formamide at 20 - 70℃; fluorenylmethoxycarbonyl (Fmoc) amide resin; Inert atmosphere; Stage #3: With trifluoroacetic acid In water for 1.83333h; fluorenylmethoxycarbonyl (Fmoc) amide resin; Temperature; Time;	15%

Yield

Stage #1: C52H83N12O13Pol; N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In 1-methyl-pyrrolidin-2-one fluorenylmethoxycarbonyl (Fmoc) amide resin;
Stage #2: C15H26N6O5 In N,N-dimethyl-formamide at 20 - 70℃; fluorenylmethoxycarbonyl (Fmoc) amide resin; Inert atmosphere;
Stage #3: With trifluoroacetic acid In water for 1.83333h; fluorenylmethoxycarbonyl (Fmoc) amide resin; Temperature; Time;

15%

...Expand

: 112-43-6
10-Undecen-1-ol

: 654636-62-1
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide

: 1393670-66-0
undec-10-en-1-yl 2-((tert-butyl(1-(diethoxyphosphoryl)-2,2-dimethylpropyl)amino)oxy)-2-methylpropanoate

Conditions

Conditions	Yield
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0℃; Mitsunobu reaction;	11%

: 654636-62-1
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide

: 188526-94-5
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)aminoxyl

Conditions

Conditions	Yield
With oxygen at 120℃; Kinetics;

: 654636-62-1
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide

: C17H35ClNO5P

Conditions

Conditions	Yield
With thionyl chloride In dichloromethane at 20℃; for 2h;

: 2695-37-6
sodium 4-styrenesulfonate

: 654636-62-1
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide

: 947705-50-2
C25H43NO9PS(1-)*Na(1+)

Conditions

Conditions	Yield
In ethanol; water at 70℃; for 6h; Inert atmosphere;

: 6066-82-6
1-hydroxy-pyrrolidine-2,5-dione

: 654636-62-1
N-(2-methyl-2-propyl)-N-(1-diethylphosphono-2,2-dimethylpropyl)-O-(2-carboxyprop-2-yl)hydroxylamide

: 1068449-32-0
2-methyl-2-[N-tert-butyl-N-(1-diethoxyphosphoryl-2,2-dimethylpropyl)aminoxy]-N-propionyloxysuccinimide

Conditions

Conditions	Yield
With dicyclohexyl-carbodiimide In tetrahydrofuran at 0℃; for 1.5h;
With dicyclohexyl-carbodiimide In tetrahydrofuran at 5℃;

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