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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

4-Hexanolide Manufacturer/High quality/Best price/In stock

Cas:695-06-7

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 4-Hexanolide supplier in China

Cas:695-06-7

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

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Hefei TNJ chemical industry co.,ltd

Colourless liquid, with boiling point 220 ℃, soluble in ethanol and oil. Has a moderate and strong flavours of herbs. Not dissolve in water but in alcohol organic solvent. Appearance:Colorless liquid Storage:Stored in shade,cool dry ventilated and

4-Hexanolide

Cas:695-06-7

Min.Order:1 Metric Ton

Negotiable

Type:Trading Company

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Hexan-4-olide

Cas:695-06-7

Min.Order:1

Negotiable

Type:Other

inquiry

Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

Factory Price 99% Food Grade 4-Hexanolide 695-06-7 Kosher Manufacturer

Cas:695-06-7

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

inquiry

Shanghai Seasonsgreen Chemical Co.,Ltd

Shanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu

lower price High quality 4-Hexanolide

Cas:695-06-7

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Manufacturers

inquiry

COLORCOM LTD.

Colorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on

Gamma Hexalactone

Cas:695-06-7

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

τ-Hexalactone

Cas:695-06-7

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

Gamma Hexalactone CAS 695-06-7

Cas:695-06-7

Min.Order:1 Gram

FOB Price: $6.0 / 9.0

Type:Trading Company

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Manufacturer supply CAS 695-06-7 with best quality

Cas:695-06-7

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

inquiry

Henan Tianfu Chemical Co., Ltd.

fast delivery,best price Appearance:c'less oily liquid Storage:Stored in shade,cool dry ventilated and a away from flame sources,sunshine and rain Package:200kgs or 30kgs metal drum lined PVF Application:Not dissolve in water but in alcohol organi

695-06-7

Cas:695-06-7

Min.Order:1 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Henan Sinotech Import&Export Corporation

Product property Product name:4-Hexanolide CAS:695-06-7 MF:C6H10O2 MW:114.14 Density:1.023 g/ml Melting point:-18°C Package:1 L/bottle, 25 L/drum, 200 L/drum Appearance:Colorless clear liquid Storage:Preserve in well-closed, light-resis

4-Hexanolide

Cas:695-06-7

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

inquiry

Henan Wentao Chemical Product Co., Ltd.

We are leading fine chemicals supplier in China and Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED intermediat

695-06-7CAS NO.: 695-06-7

Cas:695-06-7

Min.Order:1 Kilogram

FOB Price: $4.0 / 5.0

Type:Lab/Research institutions

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

2(3H)-Furanone,5-ethyldihydro- 695-06-7

Cas:695-06-7

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Leader Biochemical Group

About Our Group Since 1996 when our factory was put into production to year of 2020, our group has successively invested in more than 52 factories with shares and subordinates.We focus on manufacture Pharm & c

China Biggest Factory Manufacturer Supply Gamma-Hexalactone CAS 695-06-7

Cas:695-06-7

Min.Order:500 Kilogram

FOB Price: $1.0 / 2.0

Type:Lab/Research institutions

inquiry

Changchun Artel lmport and Export trade company

Product Detail Minimum Order Qty. 10 Gram

Factory Supply 99% 4-Hexanolide ,Gamma-Hexalactone in stock CAS NO.695-06-7

Cas:695-06-7

Min.Order:10 Gram

Negotiable

Type:Trading Company

inquiry

Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s

4-Hexanolide

Cas:695-06-7

Min.Order:1 Kilogram

FOB Price: $40.0 / 50.0

Type:Lab/Research institutions

inquiry

JINING XINHE CHEMICAL CO., LTD

Advantage 1: The product passed the professional production process and quality inspection, the purity is 99% +. 2: Highly qualified engineers to provide technical documents and service. 3: We could provide sample for your test. 4: High qualit

Propyl caprolactone695-06-7

Cas:695-06-7

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

γ-Hexalactone,Tonkalide

Cas:695-06-7

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Γ-Hexalactone

Cas:695-06-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Miheng Trading Co., Ltd.

4-Hexanolide CAS 695-06-7 Our advantage 1.Top quality: Using high quality material and establishing a strict quality control system,assigning specific persons in charge of each part of production,from raw material purchase to assembly. 2 Pr

4-Hexanolide CAS 695-06-7

Cas:695-06-7

Min.Order:1 Kilogram

FOB Price: $10.0 / 50.0

Type:Trading Company

inquiry

BOC Sciences

BOC Sciences provides a wide range of research chemicals and biochemicals including inhibitors, building blocks, GMP Products, impurities and metabolites, APIs for Veterinary, Natural Compounds, ADCs, Stem Cell Molecule and chiral compounds. https:

gamma-HEXALACTONE FCC cas 695-06-7

Cas:695-06-7

Min.Order:1 Gram

Negotiable

Type:Trading Company

inquiry

Hefei Zhaobo Technology Co., Ltd.

4-Hexanolide CAS 695-06-7 Purity: 99% Min Application: Intermediates Appearance: Powder Package: Bag Delivery: 3-5days Our Advantage & Service 1.Top quality: Using high quality material and establishing a strict quality control syste

4-Hexanolide CAS 695-06-7

Cas:695-06-7

Min.Order:1 Kilogram

FOB Price: $10.0 / 50.0

Type:Trading Company

inquiry

Siwei Development Group Ltd.

Product name: Gamma Hexalactone CAS No.:695-06-7 Molecule Formula:C6H10O2 Molecule Weight:114.14 Purity: 99.0% Package: 200kg/drum Description:Colorless to pale yellow liquid Manufacture Standards:Enterprise Standard TESTING ITEM

Best Quality Gamma Hexalactone with good supplier

Cas:695-06-7

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

γ-Hexalactone,Tonkalide

Cas:695-06-7

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Hangzhou Huarong Pharm Co., Ltd.

Hangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu

Gamma-Hexanolactone

Cas:695-06-7

Min.Order:0

Negotiable

Type:Trading Company

inquiry

TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

4-Hexanolide

Cas:695-06-7

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

γ-Hexalactone,Tonkalide

Cas:695-06-7

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

γ-Hexalactone,Tonkalide

Cas:695-06-7

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

Hangzhou ZeErRui Chemical Co., Ltd.

Hangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketing of chemicals. We have earned ourselves a good reputation at home

gamma-hexalactone china manufacture

Cas:695-06-7

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

5-ethyl-5H-furan-2-one
2407-43-4

5-ethyl-5H-furan-2-one

hexan-4-olide
695-06-7

hexan-4-olide

Conditions
ConditionsYield
With dodecacarbonyltetrarhodium(0); triphenylphosphine; isopropyl alcohol at 220℃; for 1h;91%
(4R,5S)-5-Ethyl-4-iodo-dihydro-furan-2-one

(4R,5S)-5-Ethyl-4-iodo-dihydro-furan-2-one

hexan-4-olide
695-06-7

hexan-4-olide

Conditions
ConditionsYield
With nickel; isopropyl alcohol for 0.25h; Heating;90%
hex-3-enoic acid
4219-24-3

hex-3-enoic acid

hexan-4-olide
695-06-7

hexan-4-olide

Conditions
ConditionsYield
With calcium(II) bis(trifluoromethanesulfonyl)imide; tert-butylammonium hexafluorophosphate(V) at 80℃; for 2h; Sealed tube;88%
With chloro-trimethyl-silane; water; sodium iodide In hexane for 44h; Ambient temperature;66%
5-hexanolide
823-22-3, 26991-67-3

5-hexanolide

hexan-4-olide
695-06-7

hexan-4-olide

Conditions
ConditionsYield
With W(OTf)6 at 180℃; for 10h; Schlenk technique; Ionic liquid; Inert atmosphere; Green chemistry;86%
With hydrogen iodide at 125℃; for 4h;
4-Methoxymethoxy-hexanoic acid trimethylhydrazide
128756-18-3

4-Methoxymethoxy-hexanoic acid trimethylhydrazide

hexan-4-olide
695-06-7

hexan-4-olide

Conditions
ConditionsYield
With perchloric acid In dichloromethane for 8h; Ambient temperature;85%
hexahydro-2H-oxepin-2-one
502-44-3

hexahydro-2H-oxepin-2-one

hexan-4-olide
695-06-7

hexan-4-olide

Conditions
ConditionsYield
With W(OTf)6 at 180℃; for 10h; Catalytic behavior; Reagent/catalyst; Temperature; Time; Schlenk technique; Ionic liquid; Inert atmosphere; Green chemistry;85%
With silica-alumina In water at 374.84℃; under 750.075 Torr; Kinetics; Flow conditions;
With W(OTf)6 at 150℃; for 10h; Reagent/catalyst; Temperature; Green chemistry;99 %Chromat.
γ-Hydroxycapronitril
51827-43-1

γ-Hydroxycapronitril

hexan-4-olide
695-06-7

hexan-4-olide

Conditions
ConditionsYield
With Rhodococcus rhodochrous IFO 15564 at 30℃; phosphate buffer, pH 6;79%
(E)-3-hexenoic acid
1577-18-0

(E)-3-hexenoic acid

hexan-4-olide
695-06-7

hexan-4-olide

Conditions
ConditionsYield
With trifluorormethanesulfonic acid In nitromethane for 3h; Heating;77%
With sulfuric acid
ethyloxirane
106-88-7

ethyloxirane

C20H15NP(1-)*Na(1+)

C20H15NP(1-)*Na(1+)

hexan-4-olide
695-06-7

hexan-4-olide

Conditions
ConditionsYield
In benzene alkalical hydrolysis;71%
hept-6-en-3-ol
19781-77-2

hept-6-en-3-ol

hexan-4-olide
695-06-7

hexan-4-olide

Conditions
ConditionsYield
With cethyltrimethylammonium permanganate In chloroform at 25℃; for 4h;69%
With (bipyH2)-CrOCl5 In dichloromethane Heating;40%
D-allono-1,4-lactone
29474-78-0

D-allono-1,4-lactone

A

hexan-4-olide
695-06-7

hexan-4-olide

B

4-Iodohexanoic acid
62885-37-4

4-Iodohexanoic acid

C

5-Iodohexanoic acid

5-Iodohexanoic acid

Conditions
ConditionsYield
With hydrogen iodide at 125℃; for 4h;A 67%
B 7%
C 14%
D-Glucono-1,5-lactone
90-80-2

D-Glucono-1,5-lactone

hexan-4-olide
695-06-7

hexan-4-olide

Conditions
ConditionsYield
With hydrogen iodide at 125℃; for 4h;67%
5-Acetyloxyhexanenitrile
89701-67-7

5-Acetyloxyhexanenitrile

A

hexan-4-olide
695-06-7

hexan-4-olide

B

5-hexanolide
823-22-3, 26991-67-3

5-hexanolide

Conditions
ConditionsYield
With sulfuric acid at 130℃; Yields of byproduct given;A 62%
B n/a
hexanoic acid
142-62-1

hexanoic acid

A

hexan-4-olide
695-06-7

hexan-4-olide

B

5-hexanolide
823-22-3, 26991-67-3

5-hexanolide

Conditions
ConditionsYield
With sodium persulfate In water at 85 - 90℃; for 5h;A 60%
B 22%
6-Hydroxyhexanoic acid
1191-25-9

6-Hydroxyhexanoic acid

hexan-4-olide
695-06-7

hexan-4-olide

Conditions
ConditionsYield
With W(OTf)6 at 180℃; for 10h; Schlenk technique; Ionic liquid; Inert atmosphere; Green chemistry;57%
With aluminium(III) triflate at 200℃; for 10h; Reagent/catalyst; Temperature; Green chemistry;96 %Chromat.
hexa-2,4-dienoic acid
110-44-1

hexa-2,4-dienoic acid

hexan-4-olide
695-06-7

hexan-4-olide

Conditions
ConditionsYield
With chloro-trimethyl-silane; water; sodium iodide In hexane for 18h; Heating;54%
hept-6-en-3-ol
19781-77-2

hept-6-en-3-ol

A

hexan-4-olide
695-06-7

hexan-4-olide

B

hept-6-en-3-one
2565-39-1

hept-6-en-3-one

Conditions
ConditionsYield
With chromium(V)A 40%
B 50%
With potassium permanganate; water; copper(II) sulfate In dichloromethane 1.) reflux, 5 min, 2.) RT, 4 h; Yield given. Yields of byproduct given;
heptanamide
628-62-6

heptanamide

A

hexan-4-olide
695-06-7

hexan-4-olide

B

hexanoic acid
142-62-1

hexanoic acid

C

5-hexanolide
823-22-3, 26991-67-3

5-hexanolide

Conditions
ConditionsYield
With sodium persulfate; copper dichloride at 85 - 90℃; for 5h;A 38%
B 42%
C 18%
methyl 3-(oxiran-2-yl)propanoate
76543-09-4

methyl 3-(oxiran-2-yl)propanoate

methylmagnesium bromide
75-16-1

methylmagnesium bromide

hexan-4-olide
695-06-7

hexan-4-olide

Conditions
ConditionsYield
Stage #1: methylmagnesium bromide With copper(l) iodide In tetrahydrofuran; diethyl ether at 0℃; for 0.5h; Inert atmosphere;
Stage #2: methyl 3-(oxiran-2-yl)propanoate In tetrahydrofuran; diethyl ether at -30℃; for 2h; Inert atmosphere;
Stage #3: With ammonium chloride In tetrahydrofuran; diethyl ether; water
42%
Caproamide
628-02-4

Caproamide

A

hexan-4-olide
695-06-7

hexan-4-olide

B

hexanoic acid
142-62-1

hexanoic acid

C

5-hexanolide
823-22-3, 26991-67-3

5-hexanolide

Conditions
ConditionsYield
With sodium persulfate; sodium chloride In water at 85 - 90℃; for 10h;A 40%
B 41%
C 19%
With sodium persulfate; sodium chloride In water at 85 - 90℃; for 10h;A 40 % Chromat.
B 41 % Chromat.
C 19%
With sodium persulfate; sodium chloride In water at 85 - 90℃; for 10h;A 40 % Chromat.
B 41 % Chromat.
C 19 % Chromat.
methyl 3-(oxiran-2-yl)propanoate
76543-09-4

methyl 3-(oxiran-2-yl)propanoate

methyllithium
917-54-4

methyllithium

hexan-4-olide
695-06-7

hexan-4-olide

Conditions
ConditionsYield
Stage #1: methyllithium With copper(I) cyanide In tetrahydrofuran; diethyl ether at 0℃; for 0.5h; Inert atmosphere;
Stage #2: methyl 3-(oxiran-2-yl)propanoate In tetrahydrofuran; diethyl ether at -30℃; for 2h; Inert atmosphere;
Stage #3: With ammonium chloride In tetrahydrofuran; diethyl ether; water
40%
(E)-hex-4-enoic acid
1577-20-4

(E)-hex-4-enoic acid

hexan-4-olide
695-06-7

hexan-4-olide

Conditions
ConditionsYield
With 1-Cyanonaphthalene; biphenyl In water; acetonitrile for 13.3333h;36%
5-bromomethyl-γ-butyrolactone
32730-32-8

5-bromomethyl-γ-butyrolactone

methyllithium
917-54-4

methyllithium

hexan-4-olide
695-06-7

hexan-4-olide

Conditions
ConditionsYield
Stage #1: methyllithium With copper(l) iodide In diethyl ether at 0℃; for 0.25h; Inert atmosphere;
Stage #2: 5-bromomethyl-γ-butyrolactone In diethyl ether at -70 - 0℃; for 5.5h; Inert atmosphere;
Stage #3: With ammonium chloride In diethyl ether; water
34%
sorbic Acid
110-44-1

sorbic Acid

hexan-4-olide
695-06-7

hexan-4-olide

Conditions
ConditionsYield
With hydrogenchloride; acetic acid; zinc at 85℃;
With hydrogenchloride; tin(ll) chloride at 85℃; Reagens 4: Eisessig;
With hydrogenchloride; tin at 85℃; Reagens 4: Eisessig;
2-ethyl-5-oxo-tetrahydro-furan-3-carboxylic acid
28274-28-4

2-ethyl-5-oxo-tetrahydro-furan-3-carboxylic acid

A

hexan-4-olide
695-06-7

hexan-4-olide

B

hex-3-enoic acid
4219-24-3

hex-3-enoic acid

Conditions
ConditionsYield
bei der Destillation;
trans-3-hexenenitrile
127727-92-8

trans-3-hexenenitrile

hexan-4-olide
695-06-7

hexan-4-olide

Conditions
ConditionsYield
With sulfuric acid
(E)-2-Hexenoic acid
13419-69-7

(E)-2-Hexenoic acid

hexan-4-olide
695-06-7

hexan-4-olide

Conditions
ConditionsYield
With sulfuric acid
5-hexenoic acid
1577-22-6

5-hexenoic acid

hexan-4-olide
695-06-7

hexan-4-olide

Conditions
ConditionsYield
With PPA at 70℃;
5-hexen-3-ol
688-99-3

5-hexen-3-ol

A

hexan-4-olide
695-06-7

hexan-4-olide

B

4-oxohexanoic acid
1117-74-4

4-oxohexanoic acid

Conditions
ConditionsYield
With sodium dichromate; dimethylsulfide borane complex; sulfuric acid 1.) Et2O, a) -78 to 25 deg C, b) 25 deg C, 12 h, 2.) reflux, 1 h; Yield given. Multistep reaction;
γ-Hydroxycaproic acid
13532-38-2, 87241-93-8, 97189-67-8

γ-Hydroxycaproic acid

hexan-4-olide
695-06-7

hexan-4-olide

Conditions
ConditionsYield
With hydrogenchloride In methanol; water at 0℃; for 1h; Yield given;
hexan-4-olide
695-06-7

hexan-4-olide

4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane
25015-63-8

4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

4,4,5,5-tetramethyl-2-((4-((3,3,4,4-tetramethylborolan-1-yl)oxy)hexyl)oxy)-1,3,2-dioxaborolane

4,4,5,5-tetramethyl-2-((4-((3,3,4,4-tetramethylborolan-1-yl)oxy)hexyl)oxy)-1,3,2-dioxaborolane

Conditions
ConditionsYield
With C12H36MgN2Si4 In neat (no solvent) at 20℃; for 0.25h; Catalytic behavior; Reagent/catalyst; Solvent; Inert atmosphere; Schlenk technique;99%
hexan-4-olide
695-06-7

hexan-4-olide

hexanoic acid
142-62-1

hexanoic acid

Conditions
ConditionsYield
With palladium 10% on activated carbon; W(OTf)6; hydrogen at 135℃; under 760.051 Torr; for 12h;97%
With palladium on activated carbon; W(OTf)6; hydrogen In neat (no solvent) at 135℃; under 760.051 Torr; for 12h;94%
hexan-4-olide
695-06-7

hexan-4-olide

carbon monoxide
201230-82-2

carbon monoxide

2-methylhexane-1,6-dioic acid
626-70-0

2-methylhexane-1,6-dioic acid

Conditions
ConditionsYield
With hexafluoroantimonic acid at 0℃; for 1h;96%
hexan-4-olide
695-06-7

hexan-4-olide

hexan-1-amine
111-26-2

hexan-1-amine

N-hexyl-4-hydroxyhexanamide
1378491-89-4

N-hexyl-4-hydroxyhexanamide

Conditions
ConditionsYield
With sodium methylate In toluene at 50℃; for 70h; Inert atmosphere;94%
hexan-4-olide
695-06-7

hexan-4-olide

hexane-1,4-diol
16432-53-4

hexane-1,4-diol

Conditions
ConditionsYield
With lithium aluminium tetrahydride In diethyl ether at 0 - 20℃; for 16h; Inert atmosphere;92%
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 20℃;77%
With lithium aluminium tetrahydride In tetrahydrofuran for 2h; Ambient temperature; Yield given;
hexan-4-olide
695-06-7

hexan-4-olide

5-ethyl-dihydro-furan-2-thione

5-ethyl-dihydro-furan-2-thione

Conditions
ConditionsYield
With Lawessons reagent; Hexamethyldisiloxane at 120℃; for 0.025h; microwave irradiation;92%
hexan-4-olide
695-06-7

hexan-4-olide

Benzyl propargyl ether
4039-82-1

Benzyl propargyl ether

1-benzyloxy-7-hydroxynon-2-yn-4-one

1-benzyloxy-7-hydroxynon-2-yn-4-one

Conditions
ConditionsYield
Stage #1: Benzyl propargyl ether With n-butyllithium In tetrahydrofuran at -78 - -30℃;
Stage #2: hexan-4-olide With boron trifluoride diethyl etherate In tetrahydrofuran at -78 - 20℃; for 1h;
92%
hexan-4-olide
695-06-7

hexan-4-olide

5-ethyltetrahydrofuran-2-ol
30414-44-9

5-ethyltetrahydrofuran-2-ol

Conditions
ConditionsYield
With diisobutylaluminium hydride In hexane; dichloromethane at -78℃; for 1h;91%
With diisobutylaluminium hydride In tetrahydrofuran at -78℃;85%
Stage #1: hexan-4-olide With diisobutylaluminium hydride In toluene at -63 - -61℃; for 1.5h; Inert atmosphere;
Stage #2: With methanol In diethyl ether; toluene at 20℃;
52%
Stage #1: hexan-4-olide With diisobutylaluminium hydride In toluene at -63 - -61℃; for 1.5h; Inert atmosphere;
Stage #2: With methanol In diethyl ether; toluene at 20℃;
Stage #1: hexan-4-olide With diisobutylaluminium hydride In hexane; dichloromethane at -75 - -70℃; for 4.5h;
Stage #2: With water; ammonium chloride In hexane; dichloromethane Cooling with ice;
hexan-4-olide
695-06-7

hexan-4-olide

chloro-trimethyl-silane
75-77-4

chloro-trimethyl-silane

dimethyl lithiomethylphosphonate
34939-91-8, 58648-56-9

dimethyl lithiomethylphosphonate

(2-oxo-5-trimethylsilanyloxy-heptyl)-phosphonic acid dimethyl ester

(2-oxo-5-trimethylsilanyloxy-heptyl)-phosphonic acid dimethyl ester

Conditions
ConditionsYield
Stage #1: hexan-4-olide; dimethyl lithiomethylphosphonate
Stage #2: With lithium diisopropyl amide
Stage #3: chloro-trimethyl-silane
90%
hexan-4-olide
695-06-7

hexan-4-olide

4-amino-2,2,6,6-tetramethyl-1-piperidine-1-oxyl
14691-88-4

4-amino-2,2,6,6-tetramethyl-1-piperidine-1-oxyl

C15H29N2O3

C15H29N2O3

Conditions
ConditionsYield
at 130℃; for 2h;89%
hexan-4-olide
695-06-7

hexan-4-olide

4-hydroxyhexanamide
40726-47-4

4-hydroxyhexanamide

Conditions
ConditionsYield
With ammonia at 20℃; for 240h;87%
With ethanol; ammonia at 100℃;
With ammonia; water durch Schuetteln;
hexan-4-olide
695-06-7

hexan-4-olide

diphenyl diselenide
1666-13-3

diphenyl diselenide

5-ethyl-3-(phenylselanyl)dihydrofuran-2(3H)-one

5-ethyl-3-(phenylselanyl)dihydrofuran-2(3H)-one

Conditions
ConditionsYield
Stage #1: hexan-4-olide With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 1.25h;
Stage #2: diphenyl diselenide With N,N,N,N,N,N-hexamethylphosphoric triamide In tetrahydrofuran at -78 - -40℃;
87%
hexan-4-olide
695-06-7

hexan-4-olide

tert-butyl propionate
20487-40-5

tert-butyl propionate

tert-butyldimethylsilyl chloride
18162-48-6

tert-butyldimethylsilyl chloride

3,6-bis-(tert-butyl-dimethyl-silanyloxy)-2-methyl-oct-2-enoic acid tert-butyl ester

3,6-bis-(tert-butyl-dimethyl-silanyloxy)-2-methyl-oct-2-enoic acid tert-butyl ester

Conditions
ConditionsYield
Stage #1: tert-butyl propionate With lithium diisopropyl amide In tetrahydrofuran; hexane at -78℃;
Stage #2: hexan-4-olide In tetrahydrofuran; hexane at -78℃; for 2h;
Stage #3: tert-butyldimethylsilyl chloride With tert-butoxide In tetrahydrofuran at 20℃;
86%
hexan-4-olide
695-06-7

hexan-4-olide

acetic acid tert-butyl ester
540-88-5

acetic acid tert-butyl ester

tert-butyldimethylsilyl chloride
18162-48-6

tert-butyldimethylsilyl chloride

3,6-bis-(tert-butyl-dimethyl-silanyloxy)-oct-2-enoic acid tert-butyl ester

3,6-bis-(tert-butyl-dimethyl-silanyloxy)-oct-2-enoic acid tert-butyl ester

Conditions
ConditionsYield
Stage #1: acetic acid tert-butyl ester With lithium diisopropyl amide In tetrahydrofuran; hexane at -78℃;
Stage #2: hexan-4-olide In tetrahydrofuran; hexane at -78℃;
Stage #3: tert-butyldimethylsilyl chloride With tert-butoxide In tetrahydrofuran at 20℃;
85%
hexan-4-olide
695-06-7

hexan-4-olide

N,O-dimethylhydroxylamine*hydrochloride
6638-79-5

N,O-dimethylhydroxylamine*hydrochloride

4-hydroxy-N-methoxy-N-methylhexanamide
1360562-58-8

4-hydroxy-N-methoxy-N-methylhexanamide

Conditions
ConditionsYield
With isopropylmagnesium chloride In tetrahydrofuran at -20 - -15℃; for 0.333333h; Inert atmosphere;85%
hexan-4-olide
695-06-7

hexan-4-olide

triethylsilane
617-86-7

triethylsilane

triethylsilyl 4-iodohexanoate

triethylsilyl 4-iodohexanoate

Conditions
ConditionsYield
With 1,2-bis-(diphenylphosphino)ethane; methyl iodide; palladium(II) acetylacetonate at 80 - 90℃; for 12h;82%
hexan-4-olide
695-06-7

hexan-4-olide

4-oxohexanoic acid
1117-74-4

4-oxohexanoic acid

Conditions
ConditionsYield
Stage #1: hexan-4-olide With sodium hydroxide In ethanol
Stage #2: With sodium hypochlorite In aq. phosphate buffer at 20℃; for 20h;
81%
With tetraethylammonium bromide In N,N-dimethyl-formamide at 20℃;72%
With sodium hydroxide; bromine; magnesium sulfate
Multi-step reaction with 2 steps
1: NaOH / ethanol
2: NaOCl / aq. phosphate buffer / 20 h / 20 °C / pH 6.6
View Scheme
hexan-4-olide
695-06-7

hexan-4-olide

O-benzylhydoxylamine hydrochloride
2687-43-6

O-benzylhydoxylamine hydrochloride

N-(benzyloxy)-4-hydroxyhexanamide

N-(benzyloxy)-4-hydroxyhexanamide

Conditions
ConditionsYield
Stage #1: O-benzylhydoxylamine hydrochloride With trimethylaluminum In tetrahydrofuran; toluene at 0 - 20℃; for 0.833333h;
Stage #2: hexan-4-olide In tetrahydrofuran; toluene at 0℃; for 1.5h;
80%
hexan-4-olide
695-06-7

hexan-4-olide

4-methoxy-benzylamine
2393-23-9

4-methoxy-benzylamine

4-Hydroxyhexanoic acid 4-methoxybenzylamide

4-Hydroxyhexanoic acid 4-methoxybenzylamide

Conditions
ConditionsYield
In neat (no solvent) at 80 - 85℃; for 16h; Heating; Large scale;72.8%
In ethyl acetate
hexan-4-olide
695-06-7

hexan-4-olide

ethyl iodide
75-03-6

ethyl iodide

3,5-diethyl-dihydro-furan-2-one
14668-68-9

3,5-diethyl-dihydro-furan-2-one

Conditions
ConditionsYield
With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; lithium diisopropyl amide In tetrahydrofuran at -78℃;68%
Stage #1: hexan-4-olide With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; diisopropylamine In tetrahydrofuran at -78℃; for 2h; Inert atmosphere;
Stage #2: ethyl iodide In tetrahydrofuran at -78℃; for 1h; Inert atmosphere;

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