CHANGZHOU HANGYU PHARMACEUTICAL TECHNOLOGY CO., LTD. founded in 1984, engages in pharmaceutical research, development, production, process design and technical consultation of synthetic and fermentation pharmaceutical products. The organizational s
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inquiryProduct Description Product Name N-Ethylcarbazole CAS No. 86-28-2 Appearance White crystalline powder Assay ≥99% Capacity 200mt/year Min.packing 100gram
Cas:86-28-2
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inquiryUnique advantages for N-Ethylcarbazole Cas 86-28-2 Guaranteed the purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:Powder Storage:Store at room Package:25kg/drum Application:Intermediates Tra
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inquiryhigh quality Appearance:white to off white crystalline powder Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Intermediates Transportation:by air or by sea Port:Shanghai, Qingdao
N-Ethylcarbazole CAS No.:86-28-2 Name: N-Ethylcarbazole Synonyms: 9-Ethylcarbazole Molecular Structure Molecular Formula: C14H13N Molecular Weight: 195.26 CAS Registr
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CHENGDU YANXI is a comprehensive manufacturer and an international distribution of products throughout the world. Specialized in Scrap metal, Chemical raw materials, Paper products and color industry. We aim to become leading position in global dis
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inquiry★.Best quality according to requirement ★.Competitive price in China market ★.Mature Technical support ★.Professional logistic support ★.Shortest delivery time Appearance:refer to COA Storage:Store in dry, cool and ventilated place Package:Accor
Product Name: N-Ethylcarbazole CAS: 86-28-2 MF: C14H13N MW: 195.26 EINECS: 201-660-4 Mol File: 86-28-2.mol N-Ethylcarbazole Structure N-Ethylcarbazole Chemical Properties Melting point 68-70 °C (lit.) Boiling point 166
Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
N-Ethylcarbazole CAS:86-28-2 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediat
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inquiryPRODUCT DETAILS
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryConditions | Yield |
---|---|
100% | |
98.1% | |
93.1% | |
With sodium amide; toluene und Erwaermen des Reaktionsgemisches mit Aethylbromid; | |
Multi-step reaction with 2 steps 1: potassium hydroxide; decalin / 170 °C 2: nickel; methanol / 80 °C / 11032.6 Torr / Hydrogenation View Scheme |
Conditions | Yield |
---|---|
Stage #1: 9H-carbazole With potassium hydroxide In dimethyl sulfoxide at 20℃; for 0.333333h; Stage #2: ethyl bromide In dimethyl sulfoxide at 35℃; for 0.05h; Solvent; Sonication; | 99% |
With sodium hydroxide In N,N-dimethyl-formamide at 20℃; for 0.666667h; Cooling with ice; | 95% |
With potassium hydroxide; PEG-400-Et2 In water; benzene at 30℃; for 2h; | 92% |
Conditions | Yield |
---|---|
With ethanol; (BQ‑NCOP)IrHCl; sodium t-butanolate at 60℃; for 3h; Inert atmosphere; Schlenk technique; Sealed tube; | 98% |
With Rh4Co; cetyltrimethylammonim bromide; hydrazine hydrate In toluene at 60℃; for 3h; Schlenk technique; Inert atmosphere; | 95% |
With methanol; nickel at 80℃; under 11032.6 Torr; Hydrogenation; |
N-ethylphenothiazine sulfoxide
N-ethylcarbazole
Conditions | Yield |
---|---|
With sodium; lithium In tetrahydrofuran for 24h; Heating; | 98% |
Conditions | Yield |
---|---|
With sodium In acetonitrile at 90℃; under 37503.8 Torr; for 6h; Pressure; Temperature; Autoclave; | 97.53% |
Conditions | Yield |
---|---|
With potassium tert-butylate In N,N-dimethyl-formamide Heating; | 97% |
Conditions | Yield |
---|---|
Stage #1: 9H-carbazole With potassium hydroxide In N,N-dimethyl-formamide at 20℃; for 0.5h; Stage #2: ethyl iodide In N,N-dimethyl-formamide at 20℃; for 12h; | 96% |
Stage #1: 9H-carbazole With potassium hydroxide In N,N-dimethyl-formamide for 0.0833333h; Stage #2: ethyl iodide In N,N-dimethyl-formamide at 20℃; for 24h; | 90% |
With potassium tert-butylate In N,N-dimethyl-formamide at 75℃; for 24h; Reflux; |
9-(1-Benzotriazol-1-yl-ethyl)-9H-carbazole
N-ethylcarbazole
Conditions | Yield |
---|---|
With sodium tetrahydroborate at 150℃; for 7h; | 95% |
N(10)-ethylphenothiazine-S,S-dioxide
N-ethylcarbazole
Conditions | Yield |
---|---|
With sodium; lithium In tetrahydrofuran for 24h; Heating; | 94% |
Conditions | Yield |
---|---|
Stage #1: 9H-carbazole With sodium hydroxide In water; dimethyl sulfoxide at 20℃; for 0.0833333h; Stage #2: ethyl halide In water; dimethyl sulfoxide at 20℃; | 94% |
9-<1-(Phenylthio)ethyl>carbazole
N-ethylcarbazole
Conditions | Yield |
---|---|
W-2 Raney nickel In ethanol for 4h; Heating; | 93% |
Conditions | Yield |
---|---|
With potassium hydroxide In acetone for 4h; Reflux; | 90% |
In acetone at 40℃; for 0.333333h; | 76.3% |
With sodium hydroxide In acetone | 75% |
9-ethyl-1,2,3,4-tetrahydrocarbazole
N-ethylcarbazole
Conditions | Yield |
---|---|
With iodine In dimethyl sulfoxide at 100℃; for 8h; | 87% |
With palladium on activated charcoal; xylene | |
5% Pd(II)/C(eggshell) In o-xylene at 200℃; for 10h; Product distribution / selectivity; Inert atmosphere; |
Conditions | Yield |
---|---|
With sodium; lithium In tetrahydrofuran for 24h; Heating; | 86% |
Conditions | Yield |
---|---|
With trimethylsilyl trifluoromethanesulfonate In dichloromethane at -78℃; | 82% |
N-ethylcarbazole
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene at 80℃; for 3h; Inert atmosphere; | 82% |
Conditions | Yield |
---|---|
With 1-methyl-4-nitrobenzene at 160℃; for 5h; Inert atmosphere; | 81% |
N-ethyl-[1,1'-biphenyl]-2-amine
N-ethylcarbazole
Conditions | Yield |
---|---|
Stage #1: N-ethyl-[1,1'-biphenyl]-2-amine With palladium diacetate In toluene at 20℃; for 1h; Stage #2: With [bis(acetoxy)iodo]benzene In toluene at 20℃; for 3h; | 81% |
Conditions | Yield |
---|---|
With tris(1,10-phenanthroline)iron(II) bis(bis(trifluoromethane)sulfonimide); oxygen In tetrahydrofuran at 20℃; under 2068.65 Torr; for 4h; Irradiation; Inert atmosphere; | 80% |
With tetrakis(acetonitrile)copper(I)tetrafluoroborate; 2.9-dimethyl-1,10-phenanthroline; iodine; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; methyloxirane In tetrahydrofuran at 20℃; for 20h; Catalytic behavior; Flow reactor; Inert atmosphere; Irradiation; | 79% |
Conditions | Yield |
---|---|
With potassium tert-butylate In N,N-dimethyl-formamide at 20℃; for 0.116667h; Microwave irradiation; | 76% |
Conditions | Yield |
---|---|
Stage #1: 9H-carbazole With potassium hydroxide In acetone at 20℃; for 0.5h; Stage #2: ethylene dibromide In acetone at 20℃; for 10h; | 74.3% |
dodecahydro-N-ethyl-1H-carbazole
N-ethylcarbazole
Conditions | Yield |
---|---|
With boron nitride at 120℃; for 12h; Reagent/catalyst; | 74% |
With 5%-palladium/activated carbon In decalin at 169.84℃; under 757.576 Torr; for 1.56667h; Kinetics; Temperature; Time; | |
With platinum at 106.84℃; Mechanism; Temperature; |
2-(ethyl(phenyl)amino)benzoic acid
N-ethylcarbazole
Conditions | Yield |
---|---|
With pyridine In dimethylsulfoxide-d6 for 48h; Irradiation; | 72% |
With copper diacetate; palladium diacetate In N,N-dimethyl acetamide at 130℃; for 72h; Inert atmosphere; chemoselective reaction; | 37% |
Conditions | Yield |
---|---|
Stage #1: 9-acetylcarbazole With sodium triethylborohydride; benzo[1,3,2]dioxaborole In tetrahydrofuran at 80℃; for 12h; Inert atmosphere; Sealed tube; Stage #2: With hydrogenchloride In tetrahydrofuran; water at 20℃; for 2h; | 72% |
Conditions | Yield |
---|---|
With 10 wt% Pd(OH)2 on carbon; sodium formate; trifluoroacetic acid In m-xylene at 140℃; for 24h; Inert atmosphere; | 72% |
1-(1-ethyl-1H-indol-2-yl)buta-2,3-dien-1-ol
N-ethylcarbazole
Conditions | Yield |
---|---|
With platinum(II) chloride In toluene at 20℃; for 4h; Inert atmosphere; | 70% |
With platinum(II) chloride In toluene at 20℃; for 4h; Inert atmosphere; | 70% |
9H-carbazole
diethoxy(methyl)carbenium tetrafluoroborate
N-ethylcarbazole
Conditions | Yield |
---|---|
In dichloromethane for 96h; Ambient temperature; | 67% |
Conditions | Yield |
---|---|
In n-heptane Inert atmosphere; UV-irradiation; | 52% |
dodecahydro-N-ethyl-1H-carbazole
A
9-ethyl-2,3,4,5,6,7,8,9-octahydrocarbazole
B
N-ethylcarbazole
Conditions | Yield |
---|---|
With RhCl(CO)(PMe3)2 for 3h; Irradiation; Inert atmosphere; Overall yield = 80 %; | A 48% B 22% |
N-ethylcarbazole
dodecahydro-N-ethyl-1H-carbazole
Conditions | Yield |
---|---|
With hydrogen at 150℃; under 22502.3 Torr; for 5.6h; Kinetics; Reagent/catalyst; Temperature; Autoclave; Glovebox; | 100% |
With 1,4-dioxane; nickel at 200℃; under 183877 - 220652 Torr; Hydrogenation; | |
With 5 wt% Ru/C; hydrogen at 160℃; under 37503.8 Torr; for 48h; Inert atmosphere; | > 99 %Chromat. |
N-ethylcarbazole
9-ethyl-1,3,6-trisbromocarbazole
Conditions | Yield |
---|---|
With N-Bromosuccinimide; silica gel In dichloromethane at 18℃; for 72h; | 100% |
N-ethylcarbazole
9,9'-diethyl-9H,9'H-3,3'-bicarbazole
Conditions | Yield |
---|---|
Stage #1: N-ethylcarbazole With methanesulfonic acid In dichloromethane at 0℃; Inert atmosphere; Stage #2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone In dichloromethane at 20℃; for 0.0166667h; Reagent/catalyst; Inert atmosphere; regioselective reaction; | 99% |
With iron(III) chloride In chloroform at 20℃; for 24h; | 92.7% |
With iron(III) chloride In chloroform at 20℃; | 90% |
N-ethylcarbazole
3,6-dibromo-9-ethyl-9H-carbazole
Conditions | Yield |
---|---|
With N-Bromosuccinimide In dichloromethane at 25℃; | 98% |
With N-Bromosuccinimide In chloroform at 20℃; for 5h; | 91% |
With N-Bromosuccinimide In N,N-dimethyl-formamide at 20℃; | 68% |
Conditions | Yield |
---|---|
In 1,2-dichloro-ethane at 100℃; Friedel-Crafts Acylation; Schlenk technique; | 98% |
N-ethylcarbazole
pentafluoropropionic acid
2,2,3,3,3-pentafluoropropanoic anhydride
Conditions | Yield |
---|---|
In 1,2-dichloro-ethane at 100℃; Friedel-Crafts Acylation; Schlenk technique; | 96% |
Conditions | Yield |
---|---|
With aluminum (III) chloride In dichloromethane at 20℃; for 0.166667h; Cooling with ice; | 95% |
N-ethylcarbazole
3-bromo-9-ethyl-9H-carbazole
Conditions | Yield |
---|---|
With N-Bromosuccinimide In acetonitrile for 0.5h; Cooling with ice; | 94% |
With N-Bromosuccinimide In N,N-dimethyl-formamide at 20℃; Inert atmosphere; Darkness; | 88% |
With silica-supported quinolinium tribromide In acetonitrile at 20℃; for 5h; regioselective reaction; | 87% |
N-ethylcarbazole
N,N-dimethyl-formamide
N-ethyl-3-carbazolealdehyde
Conditions | Yield |
---|---|
With trichlorophosphate at 100℃; for 1.16667h; Inert atmosphere; | 93% |
Stage #1: N,N-dimethyl-formamide With trichlorophosphate at 20℃; for 1.16667h; Cooling with ice; Inert atmosphere; Stage #2: N-ethylcarbazole at 100℃; for 1.16667h; Microwave irradiation; Inert atmosphere; | 93% |
With trichlorophosphate for 0.025h; Vilsmeier reaction; microwave irradiation; | 89% |
Conditions | Yield |
---|---|
With aluminum (III) chloride In dichloromethane at 20℃; for 8h; | 92% |
N-ethylcarbazole
N,N-dimethyl-formamide
3,6-diformyl-9-ethylcarbazole
Conditions | Yield |
---|---|
With trichlorophosphate for 24h; Reflux; | 90% |
With trichlorophosphate In 1,2-dichloro-benzene at 85℃; Vilsmeier reaction; | 78% |
Stage #1: N-ethylcarbazole; N,N-dimethyl-formamide With zinc(II) chloride at 100℃; for 0.25h; Stage #2: With trichlorophosphate at 100℃; for 24.25h; Cooling with ice; | 75% |
N-ethylcarbazole
3,6-diiodo-9-ethylcarbazole
Conditions | Yield |
---|---|
With Iodine monochloride In ethanol for 2h; Heating; | 90% |
With potassium iodate; potassium iodide In acetic acid | |
With potassium iodate; acetic acid; potassium iodide |
N-ethylcarbazole
acetyl chloride
1,1′-(9-ethyl-9H-carbazole-3,6-diyl)diethanone
Conditions | Yield |
---|---|
With aluminum (III) chloride In dichloromethane at 20℃; for 50h; Friedel-Crafts Acylation; Cooling with ice; | 90% |
Stage #1: N-ethylcarbazole; acetyl chloride; aluminum (III) chloride In dichloromethane at 0 - 20℃; for 7h; Stage #2: With water In dichloromethane at 0℃; | 85% |
Stage #1: N-ethylcarbazole; acetyl chloride With aluminum (III) chloride In dichloromethane at 0 - 20℃; Stage #2: With water In dichloromethane Cooling with ice; | 85% |
Conditions | Yield |
---|---|
Stage #1: N-ethylcarbazole With aluminum (III) chloride In dichloromethane at 20℃; for 0.0833333h; Stage #2: 2-Bromoacetyl bromide In dichloromethane at 0 - 20℃; for 17h; | 90% |
With aluminum (III) chloride In dichloromethane at 0 - 5℃; Friedel-Crafts Acylation; | 60% |
With aluminum (III) chloride In dichloromethane Friedel-Crafts Alkylation; |
N-ethylcarbazole
cinnamoyl chloride
1‐(9‐ethyl‐9H‐carbazol‐3‐yl)‐3‐phenylprop‐2‐en‐1‐one
Conditions | Yield |
---|---|
With aluminum (III) chloride In 1,2-dichloro-ethane at 0℃; Reflux; | 89.3% |
Conditions | Yield |
---|---|
With nitric acid In acetic acid at 23℃; for 6h; | 89% |
With uronium nitrate In acetic acid for 20h; | 81% |
With nitric acid In water; 1,2-dichloro-ethane at 10℃; for 1h; | 81% |
N-ethylcarbazole
9-ethyl-carbazole-3-sulfonic acid
Conditions | Yield |
---|---|
With chlorosulfonic acid In dichloromethane at -5℃; for 2h; | 89% |
N-ethylcarbazole
Acetyl bromide
1,1′-(9-ethyl-9H-carbazole-3,6-diyl)diethanone
Conditions | Yield |
---|---|
With aluminum (III) chloride In 1,2-dichloro-ethane at 20℃; for 5h; | 89% |
Stage #1: N-ethylcarbazole With tin(IV) chloride In dichloromethane at 20℃; for 0.166667h; Stage #2: Acetyl bromide In dichloromethane at 20℃; for 24h; | 62% |
With carbon disulfide; aluminum (III) chloride for 3h; Friedel-Crafts Acylation; Cooling with ice; Reflux; | 7.2 g |
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