1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualified
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inquiry2-(3-bromophenyl)-4,6-diphenyl-1,3,5-triazine company introduction Hohance Chemical Co., Ltd. is a researchbased pharmaceutical & chemical corporation focusing on the custom synthesis service of novel products in the field of pharmaceuticals. W
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inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiryThe company has a professional R & D team, mature technology, very competitive prices and stable high quality products for customers to order high quality and low price product efforts! Appearance:White or off-white Solid Storage:Sealed, dry, m
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inquiryPuyang Huicheng Electronic Material Co., Ltd was founded in 2002, which is focus on high complex new type intermediates and fine chemical custom synthesis, LED&OLED materials and related intermediates, catalyst design and synthesi
Cas:864377-31-1
Min.Order:100 Gram
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
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inquiryProduct Description Product website: http://www.finerchem.com/pro01en/id/1472.html Product Name 2-(3-Bromophenyl)-4,6-diphenyl-1,3,5-triazine CAS No.
Cas:864377-31-1
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inquiry2-(3-Bromophenyl)-4,6-diphenyl-1,3,5-triazine Basic information Product Name: 2-(3-Bromophenyl)-4,6-diphenyl-1,3,5-triazine Synonyms: 2-(3-Bromophenyl)-4,6-diphenyl-1,3,5-triazine
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Min.Order:1 Kilogram
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryProduct Name 2-(3-bromophenyl)-4,6-diphenyl-1,3,5-triazine Structural formula CAS No. 864377-31-1 Appearance:White powder Storage:Store in cool and dry place, away from sun light. Package:25kg/drum Applicati
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inquiryBeluga chemical professional supply 2-(3-Bromophenyl)-4,6-diphenyl-1,3,5-triazine CAS 864377-31-1 1. Beluga Chemical has a professional RESEARCH and development team and strong technical force to ensure technical support and research capabilities.
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
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inquiry1.high quality: quality is life. quality is the most important element for all goods. we have a lab doing research in wuhan china. hplc and nmr is available if needed. 2.reasonable price: we provide high quality products wi
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inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists
Cas:864377-31-1
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
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Type:Trading Company
inquiryTriumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Service 1.Own made fine chemical products 2.Out sourcing and qua
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Min.Order:100 Gram
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inquirylarge capacity for chemical production, full facility for analysis, high purity oled intermediate superior quality, moderate price & quick delivery Welcome to contact us for more information about our quality products! Appearance:Off-white
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Min.Order:1 Kilogram
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Type:Trading Company
inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:864377-31-1
Min.Order:4 Kilogram
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inquiryWhy Choose Us: 1. Factory direct sales, so we can provide the competitive price and high quality product base on 8 years of production and R&D experience. 2. It is available in stock for quick shipment.Products could be packaged according to cu
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Min.Order:1 Gram
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inquiryChemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff
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Min.Order:100 Gram
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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Min.Order:10 Gram
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inquiryour strengths: 1: Fast and guaranteed shipment (TNT;EMS;FEDEX;DHL;UPS;EUB, special line) 2: Various payment items accepted (Btc; MoneyGram; WU) 3: Valued package (Paraffin coating; Double aluminum foil bag; Vacuum packaging) 4: Efficient deliv
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Min.Order:1 Gram
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Type:Other
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:864377-31-1
Min.Order:1 Gram
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inquiryProduct name: 2-(3-Bromophenyl)-4,6-Diphenyl-1,3,5-Triazine CAS No.:864377-31-1 Molecule Formula:C21H14BrN3 Molecule Weight:388.26 Purity: 99% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard
Cas:864377-31-1
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryWe're in good position to supply OLED intermediates . In the past 25 years, we have won technical support from several well-known universities and institutes. We have developed many chemicals together. It makes us capable of developing Cust
Cas:864377-31-1
Min.Order:1 Kilogram
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Type:Trading Company
inquiryGMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
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Min.Order:1 Milligram
Negotiable
Type:Trading Company
inquiry2-chloro-4,6-diphenyl-1,3,5-triazine
(3-bromophenyl)boronic acid
2-(3-bromo-phenyl)-4,6-diphenyl-1,3,5-triazine
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water at 80℃; for 12h; Inert atmosphere; | 95% |
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water at 80℃; for 12h; Inert atmosphere; | 95% |
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water at 80℃; for 12h; Inert atmosphere; | 95% |
(3-Bromophenyl)methanol
benzamidin
2-(3-bromo-phenyl)-4,6-diphenyl-1,3,5-triazine
Conditions | Yield |
---|---|
With oxygen In toluene at 110℃; for 20h; Schlenk technique; | 90% |
benzamidine monohydrochloride
3-bromobenzyl chloride
2-(3-bromo-phenyl)-4,6-diphenyl-1,3,5-triazine
Conditions | Yield |
---|---|
With sodium carbonate; sulfur In dimethyl sulfoxide at 130℃; for 24h; | 90% |
With sulfur; potassium hydroxide In dimethyl sulfoxide at 130℃; for 24h; Sealed tube; | 88% |
2-bromo-4,6-diphenyl-1,3,5-triazabenzene
(3-bromophenyl)boronic acid
2-(3-bromo-phenyl)-4,6-diphenyl-1,3,5-triazine
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene at 90℃; for 5h; Inert atmosphere; | 87.46% |
Suzuki Coupling; | |
Suzuki Coupling; |
1-Bromo-3-iodobenzene
2-(3-bromo-phenyl)-4,6-diphenyl-1,3,5-triazine
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene at 90℃; for 5h; Inert atmosphere; | 83.1% |
1-Bromo-3-iodobenzene
2-(3-bromo-phenyl)-4,6-diphenyl-1,3,5-triazine
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water for 10h; Suzuki Coupling; Inert atmosphere; Reflux; | 83% |
m-bromobenzoic aldehyde
benzamidine monohydrochloride
2-(3-bromo-phenyl)-4,6-diphenyl-1,3,5-triazine
Conditions | Yield |
---|---|
With nickel diacetate; sodium carbonate In toluene at 110℃; for 30h; Reagent/catalyst; | 83% |
With copper(II) acetate monohydrate; sodium carbonate In toluene at 100℃; for 24h; | 68% |
With sodium carbonate; copper(l) chloride at 90 - 100℃; | 3.2 g |
N-(3-bromobenzylidene)-phenyl-amine
benzamidine monohydrochloride
2-(3-bromo-phenyl)-4,6-diphenyl-1,3,5-triazine
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol for 12h; Reflux; | 74% |
Stage #1: N-(3-bromobenzylidene)-phenyl-amine; benzamidine monohydrochloride With sodium hydroxide In ethanol at 80℃; for 16h; Inert atmosphere; Stage #2: With sodium t-butanolate In ethanol at 80℃; for 16h; Inert atmosphere; | 37% |
Stage #1: N-(3-bromobenzylidene)-phenyl-amine; benzamidine monohydrochloride With sodium hydroxide In ethanol at 80℃; for 16h; Inert atmosphere; Stage #2: With sodium t-butanolate In ethanol at 80℃; for 16h; | 37% |
Stage #1: N-(3-bromobenzylidene)-phenyl-amine; benzamidine monohydrochloride With sodium hydroxide In ethanol for 18h; Inert atmosphere; Reflux; Stage #2: With sodium t-butanolate In ethanol for 16h; Inert atmosphere; Reflux; | 26.7% |
3-bromobenzoyl chloride
benzamidine monohydrochloride
2-(3-bromo-phenyl)-4,6-diphenyl-1,3,5-triazine
Conditions | Yield |
---|---|
Stage #1: 3-bromobenzoyl chloride; benzamidine monohydrochloride With triethylamine In 5,5-dimethyl-1,3-cyclohexadiene at 0 - 60℃; for 3.5h; Inert atmosphere; Stage #2: With 1,1,3,3-tetramethyldisilazane In 5,5-dimethyl-1,3-cyclohexadiene at 150℃; for 5h; Inert atmosphere; | 72% |
2-chloro-4,6-diphenyl-1,3,5-triazine
(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)bromobenzene)
2-(3-bromo-phenyl)-4,6-diphenyl-1,3,5-triazine
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In 1,4-dioxane for 5h; Inert atmosphere; Reflux; | 72% |
3-bromobenzoyl chloride
benzonitrile
2-(3-bromo-phenyl)-4,6-diphenyl-1,3,5-triazine
Conditions | Yield |
---|---|
Stage #1: 3-bromobenzoyl chloride; benzonitrile In dichloromethane at 0 - 5℃; for 0.5h; Inert atmosphere; Cooling with ice; Stage #2: With antimonypentachloride In dichloromethane at 20℃; for 1h; Inert atmosphere; Stage #3: With ammonia In water at 0 - 20℃; for 3.5h; Cooling with ice; | 66.7% |
Stage #1: 3-bromobenzoyl chloride; benzonitrile With aluminum (III) chloride; thionyl chloride In 1,2-dichloro-benzene at 100℃; for 20h; Stage #2: With ammonium chloride In 1,2-dichloro-benzene at 100℃; for 3h; | 40% |
m-bromobenzoic aldehyde
2-(3-bromo-phenyl)-4,6-diphenyl-1,3,5-triazine
Conditions | Yield |
---|---|
With sodium carbonate; copper dichloride In toluene at 130℃; | 52% |
1,3-dibromobenzene
2-chloro-4,6-diphenyl-1,3,5-triazine
2-(3-bromo-phenyl)-4,6-diphenyl-1,3,5-triazine
Conditions | Yield |
---|---|
Stage #1: 1,3-dibromobenzene With n-butyllithium In tetrahydrofuran-d8 at -78℃; for 1h; Stage #2: 2-chloro-4,6-diphenyl-1,3,5-triazine In tetrahydrofuran at 20℃; for 5h; | 40.4% |
With n-butyllithium In tetrahydrofuran at -78 - 20℃; for 12h; | 28% |
Stage #1: 1,3-dibromobenzene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 1h; Stage #2: 2-chloro-4,6-diphenyl-1,3,5-triazine In tetrahydrofuran; hexane at 20℃; for 3h; |
1-Bromo-3-iodobenzene
2-chloro-4,6-diphenyl-1,3,5-triazine
2-(3-bromo-phenyl)-4,6-diphenyl-1,3,5-triazine
Conditions | Yield |
---|---|
Stage #1: 1-Bromo-3-iodobenzene With n-butyllithium In tetrahydrofuran at -78℃; for 1.5h; Inert atmosphere; Stage #2: 2-chloro-4,6-diphenyl-1,3,5-triazine In tetrahydrofuran at 20℃; for 1.5h; Inert atmosphere; | 30% |
With n-butyllithium In tetrahydrofuran at -78℃; for 2h; Inert atmosphere; | 30% |
Stage #1: 1-Bromo-3-iodobenzene With n-butyllithium In tetrahydrofuran at -78℃; for 1.5h; Inert atmosphere; Stage #2: 2-chloro-4,6-diphenyl-1,3,5-triazine In tetrahydrofuran at -78 - 20℃; for 1.5h; Inert atmosphere; | 30% |
m-bromobenzoic aldehyde
2-(3-bromo-phenyl)-4,6-diphenyl-1,3,5-triazine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: toluene / 8 h / Reflux 2.1: sodium hydroxide / ethanol / 16 h / 80 °C / Inert atmosphere 2.2: 16 h / 80 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1: ethanol / 3 h / 20 °C 2: sodium hydroxide / ethanol / 12 h / Reflux View Scheme | |
Multi-step reaction with 2 steps 1.1: toluene / 8 h / Reflux 2.1: sodium hydroxide / ethanol / 16 h / 80 °C / Inert atmosphere 2.2: 16 h / 80 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: toluene / 8 h / Inert atmosphere; Reflux; Dean-Stark 2.1: sodium hydroxide / ethanol / 18 h / Inert atmosphere; Reflux 2.2: 16 h / Inert atmosphere; Reflux View Scheme |
2-chloro-4,6-diphenyl-1,3,5-triazine
2-(3-bromo-phenyl)-4,6-diphenyl-1,3,5-triazine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; tricyclohexylphosphine / N,N-dimethyl-formamide / 12 h / Inert atmosphere; Reflux 2: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / tetrahydrofuran; water / 10 h / Inert atmosphere; Reflux View Scheme |
phenylboronic acid
2-(3-bromo-phenyl)-4,6-diphenyl-1,3,5-triazine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane; toluene; water / 6 h / 100 °C 2: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane; toluene / 12 h / 100 °C View Scheme |
2-(3-bromo-phenyl)-4,6-diphenyl-1,3,5-triazine
bis(pinacol)diborane
Conditions | Yield |
---|---|
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate In 1,4-dioxane for 17h; Reflux; | 96% |
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate In 1,4-dioxane at 90℃; for 12h; Reflux; | 96.8% |
With bis-triphenylphosphine-palladium(II) chloride; potassium acetate In tetrahydrofuran at 80℃; for 3h; Inert atmosphere; | 93% |
2-(3-bromo-phenyl)-4,6-diphenyl-1,3,5-triazine
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In 1,4-dioxane; water for 17h; Inert atmosphere; Reflux; | 96% |
2-(3-bromo-phenyl)-4,6-diphenyl-1,3,5-triazine
Conditions | Yield |
---|---|
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0) In 1,2-dimethoxyethane; water; toluene for 16h; Inert atmosphere; Reflux; | 95% |
2-(3-bromo-phenyl)-4,6-diphenyl-1,3,5-triazine
3-chlorophenylboronic acid
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water at 80℃; for 12h; Inert atmosphere; | 95% |
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water at 80℃; for 12h; Inert atmosphere; | 95% |
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water at 80℃; for 12h; Inert atmosphere; | 95% |
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene at 110℃; for 15h; Inert atmosphere; | 95% |
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene for 3h; Reflux; | 95% |
Conditions | Yield |
---|---|
In toluene for 12h; Inert atmosphere; Reflux; | 94% |
((3-(dibenzo[b,d]thiophen-4-yl)phenyl)boronic acid)
2-(3-bromo-phenyl)-4,6-diphenyl-1,3,5-triazine
Conditions | Yield |
---|---|
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0) In tetrahydrofuran; water for 1h; Suzuki-Miyaura Coupling; Reflux; Inert atmosphere; | 93% |
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0) In tetrahydrofuran; water at 80℃; for 15h; Inert atmosphere; | 81.5% |
2-(3-bromo-phenyl)-4,6-diphenyl-1,3,5-triazine
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; sodium t-butanolate In toluene for 12h; Reflux; Inert atmosphere; | 92% |
2-(3-bromo-phenyl)-4,6-diphenyl-1,3,5-triazine
Conditions | Yield |
---|---|
With palladium diacetate; caesium carbonate; triphenylphosphine In tetrahydrofuran for 19h; Inert atmosphere; Reflux; | 91% |
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate In 5,5-dimethyl-1,3-cyclohexadiene at 145℃; for 3h; Inert atmosphere; | 90% |
2-(3-bromo-phenyl)-4,6-diphenyl-1,3,5-triazine
Conditions | Yield |
---|---|
With bis(tri-t-butylphosphine)palladium(0); sodium t-butanolate In 5,5-dimethyl-1,3-cyclohexadiene for 4h; Inert atmosphere; Reflux; | 90% |
2-(3-bromo-phenyl)-4,6-diphenyl-1,3,5-triazine
anthracene-9-boronic acid
Conditions | Yield |
---|---|
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate In ethanol; water; toluene for 22h; Inert atmosphere; Reflux; | 90% |
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate In ethanol; water; toluene for 18h; Inert atmosphere; Reflux; | 90% |
2-(3-bromo-phenyl)-4,6-diphenyl-1,3,5-triazine
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water for 12h; Reflux; Inert atmosphere; | 90% |
2-(3-bromo-phenyl)-4,6-diphenyl-1,3,5-triazine
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In 1,2-dimethoxyethane; water for 14h; Inert atmosphere; Reflux; | 89% |
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene for 5h; Inert atmosphere; Reflux; | 89% |
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene for 5h; Inert atmosphere; Reflux; | 89% |
Conditions | Yield |
---|---|
Stage #1: 2-(3-bromophenyl)-4,6-diphenyl-[1,3,5]triazine; C22H15N With sodium t-butanolate In 5,5-dimethyl-1,3-cyclohexadiene for 0.5h; Heating; Stage #2: With bis(tri-t-butylphosphine)palladium(0) In 1-methyl-pyrrolidin-2-one; 5,5-dimethyl-1,3-cyclohexadiene for 2h; Buchwald-Hartwig Coupling; Reflux; | 88.4% |
2-(3-bromo-phenyl)-4,6-diphenyl-1,3,5-triazine
Conditions | Yield |
---|---|
With 18-crown-6 ether; tri-tert-butyl phosphine; palladium diacetate; potassium carbonate In 5,5-dimethyl-1,3-cyclohexadiene; toluene for 4h; Inert atmosphere; Reflux; | 88% |
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In ethanol; water; toluene for 12h; Inert atmosphere; Reflux; | 88% |
2-(3-bromo-phenyl)-4,6-diphenyl-1,3,5-triazine
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In ethanol; water for 16h; Suzuki Coupling; Reflux; | 87% |
2-(3-bromo-phenyl)-4,6-diphenyl-1,3,5-triazine
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In water; toluene for 8h; Heating; | 87% |
Conditions | Yield |
---|---|
With bis(tri-t-butylphosphine)palladium(0); sodium t-butanolate In 5,5-dimethyl-1,3-cyclohexadiene for 11h; Inert atmosphere; Reflux; | 87% |
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In 1,2-dimethoxyethane; water at 95℃; for 6h; Inert atmosphere; | 87% |
2-(3-bromo-phenyl)-4,6-diphenyl-1,3,5-triazine
Conditions | Yield |
---|---|
Stage #1: 2-(3-bromophenyl)-4,6-diphenyl-[1,3,5]triazine With n-butyllithium In tetrahydrofuran at -78℃; for 1h; Inert atmosphere; Stage #2: With iodine In tetrahydrofuran at -78 - 20℃; for 1h; Inert atmosphere; | 87% |
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene at 110℃; for 5h; Inert atmosphere; | 86.49% |
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