DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:936-44-7
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:936-44-7
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
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Cas:936-44-7
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiry1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ
Cas:936-44-7
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiry3-PHENYLPYRROLIDINE CAS:936-44-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interme
Cas:936-44-7
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:936-44-7
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Triumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Business Custom Synthesis: Trading(Raw Mater
Cas:936-44-7
Min.Order:0 Metric Ton
FOB Price: $18.0 / 20.0
Type:Lab/Research institutions
inquiryOur advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We have s
Cas:936-44-7
Min.Order:10 Kilogram
Negotiable
Type:Trading Company
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:936-44-7
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryEstablished in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
Cas:936-44-7
Min.Order:10 Gram
Negotiable
Type:Lab/Research institutions
inquiry3-PHENYLPYRROLIDINE Basic information Product Name: 3-PHENYLPYRROLIDINE Synonyms: TIMTEC-BB SBB010168;ASINEX-REAG BAS 03334576;3-PHENYLPYRROLIDINE;Pyrrolidine, 3-phenyl-;3AAX-0-0;(Pyrrolidin-3-yl)benzene CAS: 936-44-7 MF: C10H13N MW:
factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:936-44-7
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryWe Huarong Pharm can provide Customized Synthesis & Process R&D & APIs and intermediates Production & Quality Research & Registration Application, especially our GMP validation service which complies with SFDA, FDA, WHO and EU EMPA. O
Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:936-44-7
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:936-44-7
Min.Order:1 Metric Ton
FOB Price: $1.5
Type:Trading Company
inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in
Cas:936-44-7
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryWe are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
Cas:936-44-7
Min.Order:1 Metric Ton
FOB Price: $1.0
Type:Trading Company
inquiryWe produce carbomer by our own factory,carbomer 940 is our best seller.It is used for cosmetic and medical.And we also become agent for lubrizol.Our carbomer 940 get high viscosity and good transparency.The price will depond on the market,surely supp
Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:936-44-7
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier
Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
Cas:936-44-7
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiryAcmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
Cas:936-44-7
Min.Order:1 bottle
Negotiable
Type:Lab/Research institutions
inquiry1. Product advantages? High purity, all above 98.5%, no impurities after dissolution? We will test each batch to ensure quality? OEM and private brand services designed for free? Various cap colors available? We can also provide MT1 peptide powder2.
Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
4-phenyl-2,3-dihydro-1H-pyrrole
3-phenylpyrrolidine
Conditions | Yield |
---|---|
With palladium 10% on activated carbon; hydrogen In methanol at 20℃; for 3h; | 98% |
Conditions | Yield |
---|---|
With ammonium formate; palladium on activated charcoal In methanol | 91% |
With palladium on activated charcoal; ammonium formate In methanol Yield given; | |
With ammonium formate; palladium on activated charcoal In methanol Ambient temperature; |
8-thia-9-azatricyclo[7.2.1.02,7]dodeca-2(7),3,5-triene 8,8-dioxide
3-phenylpyrrolidine
Conditions | Yield |
---|---|
Stage #1: 8-thia-9-azatricyclo[7.2.1.02,7]dodeca-2(7),3,5-triene-8,8-dioxide With ammonia; lithium In tetrahydrofuran at -78℃; for 4.5h; Stage #2: With ammonium chloride In tetrahydrofuran at -78 - 20℃; for 16h; | 90% |
Stage #1: 8-thia-9-azatricyclo[7.2.1.02,7]dodeca-2(7),3,5-triene-8,8-dioxide With titanium(IV) isopropylate; chloro-trimethyl-silane; magnesium In tetrahydrofuran at 80 - 100℃; for 15h; Inert atmosphere; Stage #2: With sodium fluoride; sodium hydroxide In tetrahydrofuran; diethyl ether; water at 20℃; for 0.5h; Inert atmosphere; |
tert-butyl 3-phenylpyrrolidine-1-carboxylate
3-phenylpyrrolidine
Conditions | Yield |
---|---|
Stage #1: tert-butyl 3-phenylpyrrolidine-1-carboxylate With hydrogenchloride In ethyl acetate for 2h; Stage #2: With potassium carbonate In diethyl ether; water | 87% |
(+-)-phenylsuccinonitrile
3-phenylpyrrolidine
Conditions | Yield |
---|---|
With acetic acid; platinum Hydrogenation; |
3-Phenyl-pyrrolidine-1-carboxylic acid methyl ester
3-phenylpyrrolidine
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol for 48h; Heating; | |
With hydrogenchloride In methanol Heating; |
3-phenylpyrrolidine
Conditions | Yield |
---|---|
With sodium; butan-1-ol |
3-phenylpyrrolidine
Conditions | Yield |
---|---|
With sulfuric acid at 18 - 60℃; bei der elektrolytischen Reduktion; |
Conditions | Yield |
---|---|
Hydrogenation; |
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: 85 percent / triethylamine / CH2Cl2 / 3 h / 0 - 20 °C 2.1: 95 percent / di(tricyclohexylphosphine)(benzylidene)ruthenium dichloride / CH2Cl2 / 15 h / 20 °C 3.1: 87 percent / Pd(OAc)2; triphenylphosphine; K2CO3 / dimethylformamide / 15 h / 110 °C 4.1: 93 percent / H2 / Pd/C / ethanol / 15 h / 20 °C 5.1: lithium; NH3 / tetrahydrofuran / 4.5 h / -78 °C 5.2: 90 percent / NH4Cl / tetrahydrofuran / 16 h / -78 - 20 °C View Scheme |
8-thia-9-azatricyclo[7.2.1.02,7]dodeca-2(7),3,5,10-tetraene-8,8-dioxide
3-phenylpyrrolidine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: 93 percent / H2 / Pd/C / ethanol / 15 h / 20 °C 2.1: lithium; NH3 / tetrahydrofuran / 4.5 h / -78 °C 2.2: 90 percent / NH4Cl / tetrahydrofuran / 16 h / -78 - 20 °C View Scheme |
1-(2-bromobenzenesulfonyl)-2,5-dihydro-1H-pyrrole
3-phenylpyrrolidine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: 87 percent / Pd(OAc)2; triphenylphosphine; K2CO3 / dimethylformamide / 15 h / 110 °C 2.1: 93 percent / H2 / Pd/C / ethanol / 15 h / 20 °C 3.1: lithium; NH3 / tetrahydrofuran / 4.5 h / -78 °C 3.2: 90 percent / NH4Cl / tetrahydrofuran / 16 h / -78 - 20 °C View Scheme |
N,N-diallyl-2-bromobenzenesulfonamide
3-phenylpyrrolidine
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: 95 percent / di(tricyclohexylphosphine)(benzylidene)ruthenium dichloride / CH2Cl2 / 15 h / 20 °C 2.1: 87 percent / Pd(OAc)2; triphenylphosphine; K2CO3 / dimethylformamide / 15 h / 110 °C 3.1: 93 percent / H2 / Pd/C / ethanol / 15 h / 20 °C 4.1: lithium; NH3 / tetrahydrofuran / 4.5 h / -78 °C 4.2: 90 percent / NH4Cl / tetrahydrofuran / 16 h / -78 - 20 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1.) CuBr*MeS2 / 1.) Et2O, cyclohexane, 0 deg C, 1 h, 2.) Et2O, cyclohexane, 0 deg C, 15 min 2: ammonium formate / 10 percent Pd/C / methanol / Ambient temperature View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: i-Pr2NEt, Ag2CO3, P(o-Tol)3 / Pd(OAc)2 / dimethylformamide / 100 °C 2: HCO2NH4 / Pd/C / methanol / 4 h / Heating 3: aq. HCl / methanol / Heating View Scheme |
3-Phenyl-2,3-dihydro-pyrrole-1-carboxylic acid methyl ester
3-phenylpyrrolidine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: HCO2NH4 / Pd/C / methanol / 4 h / Heating 2: aq. HCl / methanol / Heating View Scheme | |
Multi-step reaction with 2 steps 1: 89 percent / HCO2NH4 / Pd/C / methanol / 4 h / Heating 2: conc. HCl (8 N) / ethanol / 48 h / Heating View Scheme |
styrene
3-phenylpyrrolidine
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 48 percent / LDA 2: 99 percent / Me3SiI / CCl4 3: 1.) NaHCO3; 2.) t-BuOK / 1.) MeOH; 2.) t-BuOH 4: HCOONH4, 10percent Pd-C / methanol View Scheme |
3-phenyl-N-(1'-tert-butoxy-2'-butyl)pyrrolidine
3-phenylpyrrolidine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 99 percent / Me3SiI / CCl4 2: 1.) NaHCO3; 2.) t-BuOK / 1.) MeOH; 2.) t-BuOH 3: HCOONH4, 10percent Pd-C / methanol View Scheme |
3-phenyl-N-(1'-hydroxy-2'-butyl)-pyrrolidine
3-phenylpyrrolidine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1.) NaHCO3; 2.) t-BuOK / 1.) MeOH; 2.) t-BuOH 2: HCOONH4, 10percent Pd-C / methanol View Scheme | |
Multi-step reaction with 3 steps 1: NaHCO3 / methanol / 20 °C 2: t-BuOK / 2-methyl-propan-2-ol / Heating 3: 91 percent / ammonium formate / 10percent Pd/C / methanol View Scheme |
3-phenylpyrrolidine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: t-BuOK / 2-methyl-propan-2-ol / Heating 2: 91 percent / ammonium formate / 10percent Pd/C / methanol View Scheme |
erythro-2,3-dibromo-3-phenylpropanoic acid
3-phenylpyrrolidine
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: ethanolic KOH-solution 2: sulfuric acid 3: aqueous ethanol 4: platinum; acetic acid / Hydrogenation View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aqueous ethanol 2: platinum; acetic acid / Hydrogenation View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: sulfuric acid 2: aqueous ethanol 3: platinum; acetic acid / Hydrogenation View Scheme |
3-phenylpyrrolidine
Conditions | Yield |
---|---|
With ammonia In methanol |
3-phenylpyrrolidine
Conditions | Yield |
---|---|
Stage #1: (+/-)-(1S,10R,11R)-epoxy-8-thia-9-azatricyclo[7.2.1.0(2,7)]dodeca-2(7),3,5-triene-8,8-dioxide With ammonia; lithium at -78℃; Stage #2: With sodium tetrahydroborate |
Conditions | Yield |
---|---|
With borane-THF In tetrahydrofuran at 0℃; for 3.5h; Inert atmosphere; Reflux; |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: tetrahydrofuran / 20 °C / Inert atmosphere 2: hydrogenchloride / water / 12 h / Reflux 3: palladium 10% on activated carbon; hydrogen / methanol / 3 h / 20 °C View Scheme |
3-phenylpyrrolidine
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: N,N-dimethyl-formamide / 18 h / 20 °C 2.1: Oxone / methanol / 48 h / 20 °C 3.1: magnesium; titanium(IV) isopropylate; chloro-trimethyl-silane / tetrahydrofuran / 15 h / 80 - 100 °C / Inert atmosphere 3.2: 0.5 h / 20 °C / Inert atmosphere 3.3: 15 h / 0 °C 4.1: magnesium; titanium(IV) isopropylate; chloro-trimethyl-silane / tetrahydrofuran / 15 h / 80 - 100 °C / Inert atmosphere 4.2: 0.5 h / 20 °C / Inert atmosphere View Scheme |
3-phenylpyrrolidine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: Oxone / methanol / 48 h / 20 °C 2.1: magnesium; titanium(IV) isopropylate; chloro-trimethyl-silane / tetrahydrofuran / 15 h / 80 - 100 °C / Inert atmosphere 2.2: 0.5 h / 20 °C / Inert atmosphere 2.3: 15 h / 0 °C 3.1: magnesium; titanium(IV) isopropylate; chloro-trimethyl-silane / tetrahydrofuran / 15 h / 80 - 100 °C / Inert atmosphere 3.2: 0.5 h / 20 °C / Inert atmosphere View Scheme |
3-phenylpyrrolidine
4-bromophenyl chloroformate
4-bromophenyl 3-phenylpyrrolidine-1-carboxylate
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; for 1h; | 95% |
3-phenylpyrrolidine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In butan-1-ol at 160℃; for 4h; Microwave irradiation; Inert atmosphere; | 95% |
Conditions | Yield |
---|---|
at 105℃; for 16h; | 94% |
Conditions | Yield |
---|---|
With potassium carbonate; sodium iodide In N,N-dimethyl-formamide Heating; | 92% |
3-phenylpyrrolidine
6-(4-formylphenoxy)pyridine-3-carboxamide
Conditions | Yield |
---|---|
With sodium tris(acetoxy)borohydride; acetic acid In 1,2-dichloro-ethane at 20℃; for 24h; | 88% |
3-phenylpyrrolidine
2-chloro-3-methyl-6-(pyridin-4-yl)pyrimidin-4(3H)-one
Conditions | Yield |
---|---|
With triethylamine for 1h; Heating / reflux; | 88% |
Conditions | Yield |
---|---|
With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide | 88% |
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 50℃; for 12h; | 78% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 15h; | 74% |
With triethylamine |
3-phenylpyrrolidine
bis(trichloromethyl) carbonate
Conditions | Yield |
---|---|
Stage #1: bis(trichloromethyl) carbonate With pyridine In dichloromethane at -78℃; for 2h; Stage #2: 3-phenylpyrrolidine In dichloromethane at -78 - 20℃; for 1h; | 73% |
With triethylamine In dichloromethane at 0 - 20℃; for 2h; |
3-phenylpyrrolidine
6-bromo-2-(chloromethyl)thieno[3,2-d]pyrimidin-4(3H)-one
6-bromo-2-[(3-phenylpyrrolidin-1-yl)methyl]thieno[3,2-d]pyrimidin-4(3H)-one
Conditions | Yield |
---|---|
With potassium carbonate; sodium iodide at 70℃; for 1h; | 72% |
3-phenylpyrrolidine
N-[4-bromobutyl]saccharin
Conditions | Yield |
---|---|
With triethylamine In acetonitrile for 12h; Heating; | 66% |
3-phenylpyrrolidine
5-(5-methylfuran-2-yl)-3-(methylsulfonyl)-1,2,4-triazine
5-(5-methylfuran-2-yl)-3-(3-phenylpyrrolidin-1-yl)-1,2,4-triazine
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20℃; Inert atmosphere; | 63% |
3-phenylpyrrolidine
Conditions | Yield |
---|---|
In neat (no solvent) at 170℃; for 24h; Sealed tube; | 59% |
3-phenylpyrrolidine
(3-(bromomethyl)phenyl)(piperidin-1-yl)methanone
Conditions | Yield |
---|---|
With triethylamine In acetonitrile for 12h; Ambient temperature; | 57% |
Conditions | Yield |
---|---|
Stage #1: 3-phenylpyrrolidine; 2,6-Dichloro-N-(cyclopropylmethyl)pyrimidine-4-carboxamide With N-ethyl-N,N-diisopropylamine In methanol at 0℃; Stage #2: N-Methyl-N-phenethylamine With N-ethyl-N,N-diisopropylamine In butan-1-ol at 160℃; for 4h; Inert atmosphere; | 57% |
3-phenylpyrrolidine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl-formamide at 20℃; for 1h; Time; | 55% |
Conditions | Yield |
---|---|
In dimethyl sulfoxide at 70℃; for 0.5h; | 50.4% |
3-phenylpyrrolidine
formaldehyd
1-prop-2-ynyl-pyrrolidin-2-one
1-[4-(3-Phenyl-pyrrolidin-1-yl)-but-2-ynyl]-pyrrolidin-2-one
Conditions | Yield |
---|---|
With acetic acid; copper(l) chloride In 1,4-dioxane at 50℃; for 8h; | 50% |
3-phenylpyrrolidine
2-(4-methylpiperazin-1-yl)ethyl 4-nitrophenyl carbonate
2-(4-methylpiperazin-1-yl)ethyl 3-phenylpyrrolidine-1-carboxylate
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 4h; | 48% |
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl-formamide Inert atmosphere; | 42% |
3-phenylpyrrolidine
2-(4-bromobutyl)-1-isoindolinone
Conditions | Yield |
---|---|
With triethylamine In acetonitrile for 12h; Ambient temperature; | 41% |
3-phenylpyrrolidine
Conditions | Yield |
---|---|
Stage #1: 4-((2-(difluoromethoxy)benzyl)(2-(methylamino)-2-oxoethyl)carbamoyl)-1H-pyrrole-2-carboxylic acid With triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide for 0.5h; Stage #2: 3-phenylpyrrolidine In N,N-dimethyl-formamide at 20℃; for 16h; | 36% |
3-phenylpyrrolidine
phenyl 2-(5-chloro-1H-indol-3-yl)ethylcarbamate
N-(2-(5-chloro-1H-indol-3-yl)ethyl)-3-phenylpyrrolidine-1-carboxamide
Conditions | Yield |
---|---|
Stage #1: 3-phenylpyrrolidine With sodium hydride In tetrahydrofuran; mineral oil at 20℃; for 0.0833333h; Stage #2: phenyl 2-(5-chloro-1H-indol-3-yl)ethylcarbamate In tetrahydrofuran; mineral oil at 20℃; | 35% |
3-phenylpyrrolidine
1-(1-(4-chlorobenzyl)-1H-indole-2-carbonyl)piperidine-4-carboxylic acid
(1-(4-chlorobenzyl)-1H-indol-2-yl)(4-(3-phenylpyrrolidine-1-carbonyl)piperidin-1-yl)methanone
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 36h; | 32% |
3-phenylpyrrolidine
7-chloro-3-(cyclopropylmethyl)-8-(trifluoromethyl)-[1,2,4]triazolo[4,3-a]pyridine
3-(cyclopropylmethyl)-7-(3-phenyl-1-pyrrolidinyl)-8-(trifluoromethyl)-1,2,4-triazolo[4,3-a]pyridine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In acetonitrile at 180℃; for 0.333333h; Microwave irradiation; | 32% |
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