DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
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The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryTERT-AMYL METHYL ETHERAppearance:White power Storage:2-8 ℃ or Others Package:according to customers' requirements Application:Pharmaceutical intermediates Transportation:By air(EMS or EUB or FedEx or TNT ect...) or by sea(FOB or CIF or CNF ect...)or
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inquirytert-Amyl methyl etherAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air
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Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
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TERT-AMYL METHYL ETHER Application:TERT-AMYL METHYL ETHER
High purity Butane,2-methoxy-2-methyl- 98% TOP1 supplier in ChinaAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:pharmaceutical intermediate Transportation:by air, by sea, by express
Cas:994-05-8
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Conditions | Yield |
---|---|
With sodium hydride; 1-n-butyl-2,3-dimethylimidazolium hexafluorophosphate at 25℃; for 2h; Williamson synthesis; | 87% |
With potassium hydride 1.)THF, 2 h, reflux, 2.) 0.5 h at 20 deg C, reflux, 1 h; Multistep reaction; |
methanol
tert-Amyl alcohol
A
2-methyl-but-2-ene
B
tert-Amyl methyl ether
C
2-Methyl-1-butene
Conditions | Yield |
---|---|
With Amberlyst-36 In 1,4-dioxane at 80℃; for 4h; Kinetics; Mechanism; Reagent/catalyst; Temperature; Autoclave; | A n/a B 71.37% C n/a |
UDCaT-6 at 120℃; Product distribution; Activation energy; Further Variations:; Catalysts; Temperatures; space time; | A n/a B 18% C n/a |
Conditions | Yield |
---|---|
In diethyl ether Heating; | 60% |
methanol
2,2-dimethyl-1-propyl phenyl selenide
A
tert-Amyl methyl ether
B
methyl t-butylmethyl ether
C
diphenyl diselenide
Conditions | Yield |
---|---|
With naphthalene-1,4-dicarbonitrile for 8h; Ambient temperature; Irradiation; | A 15% B 35% C 50% |
Conditions | Yield |
---|---|
With hydrogen; iodine at 100℃; under 60004.8 Torr; for 0.5h; | 42% |
With Amberlyst 15 at 49.9℃; Product distribution; Rate constant; Kinetics; various reaction conditions; | |
With sulfuric acid | |
With Amberlyst 15 at 49.9℃; |
Conditions | Yield |
---|---|
With tetrafluoroboric acid; dichloromethane | |
With boron trifluoride diethyl etherate | |
silica gel Ambient temperature; | 99 % Chromat. |
Conditions | Yield |
---|---|
With sodium hydroxide; sodium tetrahydroborate; mercury(II) diacetate Product distribution; other alcohols and mercuric salts; | |
aluminosilicate catalyst at 99.9℃; Equilibrium constant; other temp.; | |
With Amberlyst 16 at 49.9℃; under 5250.4 Torr; Equilibrium constant; Thermodynamic data; var. temp.; ΔH; |
Conditions | Yield |
---|---|
aluminosilicate catalyst at 99.9℃; Equilibrium constant; Thermodynamic data; other temp., ΔH, ΔG, ΔS; | |
With Amberlyst 16 at 49.9℃; under 5250.4 Torr; Equilibrium constant; Thermodynamic data; var. temp.; ΔH; | |
(i) Hg(OAc)2, (ii) aq. NaOH, NaBH4; Multistep reaction; |
methanol
2,2-dimethyl-1-propyl phenyl selenide
A
tert-Amyl methyl ether
B
methyl t-butylmethyl ether
Conditions | Yield |
---|---|
With naphthalene-1,4-dicarbonitrile Irradiation; |
methanol
C31H30N(1+)*BF4(1-)
A
2-methyl-but-2-ene
B
tert-Amyl methyl ether
Conditions | Yield |
---|---|
at 150℃; Yield given. Yields of byproduct given; |
methanol
C32H32N(1+)*BF4(1-)
A
2-methyl-but-2-ene
B
tert-Amyl methyl ether
Conditions | Yield |
---|---|
at 150℃; Rate constant; Thermodynamic data; ΔH(excit.). ΔS(excit.); |
deuteromethanol
C31H30N(1+)*BF4(1-)
A
2-methyl-but-2-ene
B
tert-Amyl methyl ether
Conditions | Yield |
---|---|
at 150℃; Yield given. Yields of byproduct given; |
methanol
2-methyl-but-2-ene
sulfuric acid
tert-Amyl methyl ether
Conditions | Yield |
---|---|
at 95℃; |
methanol
i-Amyl alcohol
A
2-methyl-but-2-ene
B
tert-Amyl methyl ether
C
2-Methyl-1-butene
D
3-Methyl-1-butene
Conditions | Yield |
---|---|
Stage #1: i-Amyl alcohol at 310 - 330℃; Stage #2: methanol With fibrous sulfonated cation exchanger at 90℃; under 6000.48 Torr; Title compound not separated from byproducts; |
methanol
tert-Amyl alcohol
A
2-methyl-but-2-ene
B
tert-Amyl methyl ether
C
2-Methyl-1-butene
D
3-Methyl-1-butene
Conditions | Yield |
---|---|
Dowex msm 31 at 70℃; under 6000.48 Torr; Product distribution; Further Variations:; Catalysts; Temperatures; |
methanol
2-methyl-but-2-ene
A
tert-Amyl alcohol
B
tert-Amyl methyl ether
Conditions | Yield |
---|---|
With Amberlyst(R) 15; water at 40℃; |
Conditions | Yield |
---|---|
With phenolic resin containing sulfonic groups In toluene at 79.84℃; under 2250.23 Torr; Autoclave; Inert atmosphere; |
Conditions | Yield |
---|---|
Stage #1: tert-Amyl methyl ether; cabergoline at 41 - 50℃; for 0.25h; Stage #2: cabergoline at 0 - 27℃; for 16.5h; | 88.8% |
tert-Amyl methyl ether
2-allyl-4-methylphenol
2-allyl-6-tert-amyl-4-methylphenol
Conditions | Yield |
---|---|
tin(IV) chloride In dichloromethane Ambient temperature; | 88% |
tert-Amyl methyl ether
[IrH2(bis(2-(diisopropylphosphino)-4-methylphenyl)amide)]
Conditions | Yield |
---|---|
With norbornene In further solvent(s) byproducts: norbornane, H2; (inert atm.); keeping mixt. of iridium compd. and norbornene in tert-amyl methyl ether at room temp. for 2 h, heating for 20 min; evapn., dissolving in pentane, filtration, drying, NMR and MS; | 87% |
2-allyl-6-methylphenol
tert-Amyl methyl ether
2-allyl-4-tert-amyl-6-methylphenol
Conditions | Yield |
---|---|
tin(IV) chloride In dichloromethane for 16h; Ambient temperature; | 82% |
tert-Amyl methyl ether
3-n-Pentadecylphenol
2-tert-amyl-5-n-pentadecylphenol
Conditions | Yield |
---|---|
tin(IV) chloride In dichloromethane for 16h; Ambient temperature; | 80% |
Conditions | Yield |
---|---|
tin(IV) chloride In dichloromethane for 16h; Ambient temperature; | 73% |
tert-Amyl methyl ether
2,2,2-trichloroethyl 2-(4-bromophenyl)-2-diazoacetate
Conditions | Yield |
---|---|
With dirhodium tetrakis[(R)-(1-(biphenyl)-2,2-diphenylcyclopropanecarboxylate)] In dichloromethane at 0℃; enantioselective reaction; | 70% |
4-allylguaiacol
tert-Amyl methyl ether
4-allyl-2-tert-amyl-6-methoxyphenol
Conditions | Yield |
---|---|
tin(IV) chloride In dichloromethane for 16h; Ambient temperature; | 65% |
Conditions | Yield |
---|---|
With γ-Al2O3 at 250℃; flow reactor; | A 51% B 49 % Chromat. |
With NaX zeolite at 200℃; flow reactor; | A 78 % Chromat. B 22% |
With γ-Al2O3 at 300℃; Product distribution; variation of temperatures and reagent; | A 52 % Chromat. B 48 % Chromat. |
[N-(trifluoromethylsulfonyl)imino][4-(trifluoromethyl)phenyl]-λ3-bromane
tert-Amyl methyl ether
N-[(1,1-dimethylpropoxy)methyl]trifluoromethanesulfonamide
Conditions | Yield |
---|---|
at 20℃; for 2h; Inert atmosphere; regioselective reaction; | 51% |
Conditions | Yield |
---|---|
tin(IV) chloride In dichloromethane for 16h; Ambient temperature; | 35% |
Conditions | Yield |
---|---|
aluminosilicate catalyst at 99.9℃; Equilibrium constant; other temp.; | |
With acid at 59.85℃; Equilibrium constant; |
tert-Amyl methyl ether
A
formaldehyd
B
2-methyl-2-butanol nitrate
C
tert-pentyl formate
Conditions | Yield |
---|---|
With nitrate radical In gas at -16.1 - 89.9℃; under 750.06 Torr; Mechanism; Kinetics; |
Conditions | Yield |
---|---|
aluminosilicate catalyst at 99.9℃; Equilibrium constant; Thermodynamic data; other temp., ΔG0m, ΔS0m, ΔH0m; | |
With acid at 59.85℃; Equilibrium constant; |
tert-Amyl methyl ether
A
methanol
B
2-methyl-but-2-ene
C
2-Methyl-1-butene
D
3-Methyl-1-butene
Conditions | Yield |
---|---|
KU-23 sulfonic acid ion exchange resin at 69.9℃; Equilibrium constant; Product distribution; other temperatures; |
Conditions | Yield |
---|---|
With methanol; Amberlyst 16 at 49.9℃; under 5250.4 Torr; Equilibrium constant; var. temp.; | |
With Amberlyst 15 In methanol at 24.85℃; Equilibrium constant; Further Variations:; Temperatures; Decomposition; |
Conditions | Yield |
---|---|
With methanol; Amberlyst 16 at 49.9℃; under 5250.4 Torr; Equilibrium constant; var. temp.; | |
With Amberlyst 15 In methanol at 24.85℃; Equilibrium constant; Further Variations:; Temperatures; Decomposition; |
tert-Amyl methyl ether
A
methanol
B
2-methyl-but-2-ene
C
propene
D
ethene
E
2-Methyl-1-butene
F
isobutene
Conditions | Yield |
---|---|
With oxygen at 300℃; Mechanism; Rate constant; anti-knock effect; oxidative degradation; |
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