1,3-Bis(3-aminophenoxy)benzene supplier

Name
1,3-Bis(3-aminophenoxy)benzene
EINECS 234-082-6
CAS No. 10526-07-5
Article Data7
CAS DataBase
Density 1.243 g/cm³
Solubility Insoluble in water
Melting Point 108 °C
Formula C₁₈H₁₆N₂O₂
Boiling Point 479.9 °C at 760 mmHg
Molecular Weight 292.337
Flash Point 264.8 °C
Transport Information
Appearance
Safety 26-36/37/39
Risk Codes 20/21/22
Molecular Structure
Hazard Symbols 20/21/22:;
Synonyms Aniline,3,3'-(m-phenylenedioxy)di- (7CI,8CI);1,3-Bis(3-aminophenoxy)benzene;1,3-Bis(m-aminophenoxy)benzene;3,3'-(m-Phenylenedioxy)dianiline;3,3'-Phenylenedioxydianiline;3,3'-[1,3-Phenylenebis(oxy)]bis[aniline];3,3'-[m-Phenylenebis(oxy)]dianiline;APB;APB-N;
PSA 70.50000
LogP 5.59800

Synthetic route

: 54060-31-0
1,3-bis(3-nitrophenoxy)benzene

: 10526-07-5
1,3-bis (3-aminophenoxy)-benzene

Conditions

Conditions	Yield
With 5%-palladium/activated carbon; hydrogen In ethanol under 15001.5 Torr; for 8h;	94%

: 108-36-1
1,3-dibromobenzene

: 591-27-5
m-Hydroxyaniline

: 10526-07-5
1,3-bis (3-aminophenoxy)-benzene

Conditions

Conditions	Yield
With potassium hydroxide; copper at 200 - 280℃;

: 10526-07-5
1,3-bis (3-aminophenoxy)-benzene

: deuterated 1,3-bis(3-aminophenoxy)benzene

Conditions

Conditions	Yield
With water-d2; platinum on carbon; palladium 10% on activated carbon at 180℃; for 24h;	98%

: 10526-07-5
1,3-bis (3-aminophenoxy)-benzene

: 106-89-8
epichlorohydrin

: N,N,N,N-tetraglycidyl-1,3-bis(3-aminophenoxy)benzene

Conditions

Conditions	Yield
Stage #1: 1,3-bis (3-aminophenoxy)-benzene; epichlorohydrin With lanthanum nitrate hexahydrate In 1,2-dichloro-ethane; isopropyl alcohol at 70 - 87℃; for 3h; Stage #2: With sodium hydroxide In 1,2-dichloro-ethane; isopropyl alcohol at 70 - 75℃; for 0.75h;	96%

: 10526-07-5
1,3-bis (3-aminophenoxy)-benzene

: 1107-00-2
4,4'-(1,1,1,3,3,3-hexafluoroisopropylidene)diphthalic anhydride

polymer; monomer(s): 4,4\-(hexafluoroisopropylidene)diphthalic anhydride; 1,3-bis(3-aminophenoxy)benzene: polymer; monomer(s): 4,4\-(hexafluoroisopropylidene)diphthalic anhydride; 1,3-bis(3-aminophenoxy)benzene

Conditions

Conditions	Yield
In 1-methyl-pyrrolidin-2-one at 20℃; for 36h;	90%

: 98-01-1
furfural

: 10526-07-5
1,3-bis (3-aminophenoxy)-benzene

: C28H20N2O4

Conditions

Conditions	Yield
at 100℃; for 1.33333h; Sealed tube;	90%

: 10526-07-5
1,3-bis (3-aminophenoxy)-benzene

: 38775-52-9
diethyl 2,2'-(sulfonylbis(4,1-phenylene)bis(oxy))diacetate

: C68H52N4O16S2

Conditions

Conditions	Yield
In ethanol at 80℃; Solvent;	90%

: 10526-07-5
1,3-bis (3-aminophenoxy)-benzene

: 3,5-diaminobenzyl alcohol dihydrochloride

: 1107-00-2
4,4'-(1,1,1,3,3,3-hexafluoroisopropylidene)diphthalic anhydride

polymer, polyimide, Mw (GPC): ca. 10800, Mw/Mn (GPC): ca. 2.2; monomer(s): 1,3-bis(3-aminophenoxy)benzene; 3,5-diaminobenzyl alcohol dihydrochloride; 4,4'-(hexafluoroisopropylidene)diphthalic anhydride: polymer, polyimide, Mw (GPC): ca. 10800, Mw/Mn (GPC): ca. 2.2; monomer(s): 1,3-bis(3-aminophenoxy)benzene; 3,5-diaminobenzyl alcohol dihydrochloride; 4,4'-(hexafluoroisopropylidene)diphthalic anhydride

Conditions

Conditions	Yield
Stage #1: 1,3-bis (3-aminophenoxy)-benzene; 3,5-diaminobenzyl alcohol dihydrochloride; 4,4'-(1,1,1,3,3,3-hexafluoroisopropylidene)diphthalic anhydride In 1-methyl-pyrrolidin-2-one at 0℃; for 6h; Stage #2: With aniline In 1-methyl-pyrrolidin-2-one at 20℃; for 30h; Stage #3: In 1-methyl-pyrrolidin-2-one; toluene at 150℃; Further stages.;	87%

...Expand

: 98-54-4
para-tert-butylphenol

: 4461-52-3
methoxymethanol

: 10526-07-5
1,3-bis (3-aminophenoxy)-benzene

: C42H44N2O4

Conditions

Conditions	Yield
Stage #1: methoxymethanol; 1,3-bis (3-aminophenoxy)-benzene In methanol at 20℃; Inert atmosphere; Stage #2: para-tert-butylphenol In methanol at 90℃; for 6h; Inert atmosphere;	81%

...Expand

: 5470-96-2
quinoline 2-carbaldehyde

: 10526-07-5
1,3-bis (3-aminophenoxy)-benzene

: ((1E,1'E)-N,N'-((1,3-phenylenebis(oxy))bis(3,1-phenylene))bis(1-(quinolin-2-yl)methanimine))

Conditions

Conditions	Yield
In methanol for 11h;	53%

: 2657-87-6
3,4'-diaminodiphenyl ether

: 10526-07-5
1,3-bis (3-aminophenoxy)-benzene

: 1107-00-2
4,4'-(1,1,1,3,3,3-hexafluoroisopropylidene)diphthalic anhydride

: 119389-05-8
4-(2-phenylethynyl)phthalic anhydride

polymer, Mn 3491 Da, Mw 6667 Da, PDI 1.91; monomer(s): 4,4\-(hexafluoroisopropylidene)diphthalic anhydride; 3,4\-diaminodiphenyl ether; 1,3-bis(3-aminophenoxy)benzene; 4-(phenylethynyl)phthalic anhydride: polymer, Mn 3491 Da, Mw 6667 Da, PDI 1.91; monomer(s): 4,4\-(hexafluoroisopropylidene)diphthalic anhydride; 3,4\-diaminodiphenyl ether; 1,3-bis(3-aminophenoxy)benzene; 4-(phenylethynyl)phthalic anhydride

Conditions

Conditions	Yield
Stage #1: 3,4'-diaminodiphenyl ether; 1,3-bis (3-aminophenoxy)-benzene; 4,4'-(1,1,1,3,3,3-hexafluoroisopropylidene)diphthalic anhydride In 1-methyl-pyrrolidin-2-one at 20℃; for 10.33h; Stage #2: 4-(2-phenylethynyl)phthalic anhydride In 1-methyl-pyrrolidin-2-one; toluene Heating;	6.44 g

...Expand

: 2657-87-6
3,4'-diaminodiphenyl ether

: 10526-07-5
1,3-bis (3-aminophenoxy)-benzene

: 1107-00-2
4,4'-(1,1,1,3,3,3-hexafluoroisopropylidene)diphthalic anhydride

: 119389-05-8
4-(2-phenylethynyl)phthalic anhydride

polymer, Mn 5367 Da, Mw 11056 Da, PDI 2.06; monomer(s): 4,4\-(hexafluoroisopropylidene)diphthalic anhydride; 3,4\-diaminodiphenyl ether; 1,3-bis(3-aminophenoxy)benzene; 4-(phenylethynyl)phthalic anhydride: polymer, Mn 5367 Da, Mw 11056 Da, PDI 2.06; monomer(s): 4,4\-(hexafluoroisopropylidene)diphthalic anhydride; 3,4\-diaminodiphenyl ether; 1,3-bis(3-aminophenoxy)benzene; 4-(phenylethynyl)phthalic anhydride

Conditions

Conditions	Yield
Stage #1: 3,4'-diaminodiphenyl ether; 1,3-bis (3-aminophenoxy)-benzene; 4,4'-(1,1,1,3,3,3-hexafluoroisopropylidene)diphthalic anhydride In 1-methyl-pyrrolidin-2-one at 20℃; for 10.33h; Stage #2: 4-(2-phenylethynyl)phthalic anhydride In 1-methyl-pyrrolidin-2-one; toluene Heating;	6.39 g

...Expand

: 2657-87-6
3,4'-diaminodiphenyl ether

: 10526-07-5
1,3-bis (3-aminophenoxy)-benzene

: 119389-05-8
4-(2-phenylethynyl)phthalic anhydride

: 4,4-(2,2,2-trifluoro-1-phenylethylidene)bis(phthalic anhydride)

polymer, Mn 3215 Da, Mw 5855 Da, PDI 1.82; monomer(s): 4,4\-(2,2,2-trifluoro-1-phenylethylidene)diphthalic anhydride; 3,4\-diaminodiphenyl ether; 1,3-bis(3-aminophenoxy)benzene; 4-(phenylethynyl)phthalic anhydride: polymer, Mn 3215 Da, Mw 5855 Da, PDI 1.82; monomer(s): 4,4\-(2,2,2-trifluoro-1-phenylethylidene)diphthalic anhydride; 3,4\-diaminodiphenyl ether; 1,3-bis(3-aminophenoxy)benzene; 4-(phenylethynyl)phthalic anhydride

Conditions

Conditions	Yield
Stage #1: 3,4'-diaminodiphenyl ether; 1,3-bis (3-aminophenoxy)-benzene; 4,4-(2,2,2-trifluoro-1-phenylethylidene)bis(phthalic anhydride) In 1-methyl-pyrrolidin-2-one at 20℃; for 10.33h; Stage #2: 4-(2-phenylethynyl)phthalic anhydride In 1-methyl-pyrrolidin-2-one; toluene Heating;	6.4 g

...Expand

: 2657-87-6
3,4'-diaminodiphenyl ether

: 10526-07-5
1,3-bis (3-aminophenoxy)-benzene

: 119389-05-8
4-(2-phenylethynyl)phthalic anhydride

: 4,4-(2,2,2-trifluoro-1-phenylethylidene)bis(phthalic anhydride)

polymer, Mn 5301 Da, Mw 11769 Da, PDI 2.16; monomer(s): 4,4\-(2,2,2-trifluoro-1-phenylethylidene)diphthalic anhydride; 3,4\-diaminodiphenyl ether; 1,3-bis(3-aminophenoxy)benzene; 4-(phenylethynyl)phthalic anhydride: polymer, Mn 5301 Da, Mw 11769 Da, PDI 2.16; monomer(s): 4,4\-(2,2,2-trifluoro-1-phenylethylidene)diphthalic anhydride; 3,4\-diaminodiphenyl ether; 1,3-bis(3-aminophenoxy)benzene; 4-(phenylethynyl)phthalic anhydride

Conditions

Conditions	Yield
Stage #1: 3,4'-diaminodiphenyl ether; 1,3-bis (3-aminophenoxy)-benzene; 4,4-(2,2,2-trifluoro-1-phenylethylidene)bis(phthalic anhydride) In 1-methyl-pyrrolidin-2-one at 20℃; for 10.33h; Stage #2: 4-(2-phenylethynyl)phthalic anhydride In 1-methyl-pyrrolidin-2-one; toluene Heating;	5.5 g

...Expand

: 2657-87-6
3,4'-diaminodiphenyl ether

: 10526-07-5
1,3-bis (3-aminophenoxy)-benzene

: 119389-05-8
4-(2-phenylethynyl)phthalic anhydride

: 4,4-(2,2,2-trifluoro-1-phenylethylidene)bis(phthalic anhydride)

polymer; monomer(s): 4,4\-(2,2,2-trifluoro-1-phenylethylidene)diphthalic anhydride; 3,4\-diaminodiphenyl ether; 1,3-bis(3-aminophenoxy)benzene; 4-(phenylethynyl)phthalic anhydride: polymer; monomer(s): 4,4\-(2,2,2-trifluoro-1-phenylethylidene)diphthalic anhydride; 3,4\-diaminodiphenyl ether; 1,3-bis(3-aminophenoxy)benzene; 4-(phenylethynyl)phthalic anhydride

Conditions

Conditions	Yield
Stage #1: 3,4'-diaminodiphenyl ether; 1,3-bis (3-aminophenoxy)-benzene; 4,4-(2,2,2-trifluoro-1-phenylethylidene)bis(phthalic anhydride) In 1-methyl-pyrrolidin-2-one at 20℃; for 10.33h; Stage #2: 4-(2-phenylethynyl)phthalic anhydride In 1-methyl-pyrrolidin-2-one; toluene Heating;	6.9 g

...Expand

: 2657-87-6
3,4'-diaminodiphenyl ether

: 2420-87-3
3,3',4,4'-biphenyltetracarboxylic anhydride

: 10526-07-5
1,3-bis (3-aminophenoxy)-benzene

: 119389-05-8
4-(2-phenylethynyl)phthalic anhydride

polymer, Mn 3491 Da, Mw 6796 Da, PDI 1.94; monomer(s): 3,3\,,4,4\-biphenylenetetracarboxylic dianhydride; 3,4\-diaminodiphenyl ether; 1,3-bis(3-aminophenoxy)benzene; 4-(phenylethynyl)phthalic anhydride: polymer, Mn 3491 Da, Mw 6796 Da, PDI 1.94; monomer(s): 3,3\,,4,4\-biphenylenetetracarboxylic dianhydride; 3,4\-diaminodiphenyl ether; 1,3-bis(3-aminophenoxy)benzene; 4-(phenylethynyl)phthalic anhydride

Conditions

Conditions	Yield
Stage #1: 3,4'-diaminodiphenyl ether; 3,3',4,4'-biphenyltetracarboxylic anhydride; 1,3-bis (3-aminophenoxy)-benzene In 1-methyl-pyrrolidin-2-one at 20℃; for 6.33h; Stage #2: 4-(2-phenylethynyl)phthalic anhydride In 1-methyl-pyrrolidin-2-one; toluene at 20 - 140℃;	9.34 g

...Expand

: 2657-87-6
3,4'-diaminodiphenyl ether

: 2420-87-3
3,3',4,4'-biphenyltetracarboxylic anhydride

: 10526-07-5
1,3-bis (3-aminophenoxy)-benzene

: 119389-05-8
4-(2-phenylethynyl)phthalic anhydride

polymer, Mn 8383 Da, Mw 14496 Da, PDI 1.73; monomer(s): 3,3\,,4,4\-biphenylenetetracarboxylic dianhydride; 3,4\-diaminodiphenyl ether; 1,3-bis(3-aminophenoxy)benzene; 4-(phenylethynyl)phthalic anhydride: polymer, Mn 8383 Da, Mw 14496 Da, PDI 1.73; monomer(s): 3,3\,,4,4\-biphenylenetetracarboxylic dianhydride; 3,4\-diaminodiphenyl ether; 1,3-bis(3-aminophenoxy)benzene; 4-(phenylethynyl)phthalic anhydride

Conditions

Conditions	Yield
Stage #1: 3,4'-diaminodiphenyl ether; 3,3',4,4'-biphenyltetracarboxylic anhydride; 1,3-bis (3-aminophenoxy)-benzene In 1-methyl-pyrrolidin-2-one at 20℃; for 6.33h; Stage #2: 4-(2-phenylethynyl)phthalic anhydride In 1-methyl-pyrrolidin-2-one; toluene at 20 - 140℃;	14.5 g

...Expand

: 2657-87-6
3,4'-diaminodiphenyl ether

: 2420-87-3
3,3',4,4'-biphenyltetracarboxylic anhydride

: 10526-07-5
1,3-bis (3-aminophenoxy)-benzene

: 119389-05-8
4-(2-phenylethynyl)phthalic anhydride

polymer; monomer(s): 3,3\,,4,4\-biphenylenetetracarboxylic dianhydride; 3,4\-diaminodiphenyl ether; 1,3-bis(3-aminophenoxy)benzene; 4-(phenylethynyl)phthalic anhydride: polymer; monomer(s): 3,3\,,4,4\-biphenylenetetracarboxylic dianhydride; 3,4\-diaminodiphenyl ether; 1,3-bis(3-aminophenoxy)benzene; 4-(phenylethynyl)phthalic anhydride

Conditions

Conditions	Yield
Stage #1: 3,4'-diaminodiphenyl ether; 3,3',4,4'-biphenyltetracarboxylic anhydride; 1,3-bis (3-aminophenoxy)-benzene In 1-methyl-pyrrolidin-2-one at 20℃; for 6.33h; Stage #2: 4-(2-phenylethynyl)phthalic anhydride In 1-methyl-pyrrolidin-2-one; toluene at 20 - 140℃;	6.9 g

...Expand

: 10526-07-5
1,3-bis (3-aminophenoxy)-benzene

: 119389-05-8
4-(2-phenylethynyl)phthalic anhydride

: 4,4-(2,2,2-trifluoro-1-phenylethylidene)bis(phthalic anhydride)

polymer, Mn 5406 Da, Mw 11055 Da, PDI 2.11; monomer(s): 4,4\-(2,2,2-trifluoro-1-phenylethylidene)diphthalic anhydride; 1,3-bis(3-aminophenoxy)benzene; 4-(phenylethynyl)phthalic anhydride: polymer, Mn 5406 Da, Mw 11055 Da, PDI 2.11; monomer(s): 4,4\-(2,2,2-trifluoro-1-phenylethylidene)diphthalic anhydride; 1,3-bis(3-aminophenoxy)benzene; 4-(phenylethynyl)phthalic anhydride

Conditions

Conditions	Yield
Stage #1: 1,3-bis (3-aminophenoxy)-benzene; 4,4-(2,2,2-trifluoro-1-phenylethylidene)bis(phthalic anhydride) In 1-methyl-pyrrolidin-2-one at 20℃; for 6.33h; Stage #2: 4-(2-phenylethynyl)phthalic anhydride In 1-methyl-pyrrolidin-2-one; toluene Heating;	6.45 g

...Expand

: 2657-87-6
3,4'-diaminodiphenyl ether

: 2420-87-3
3,3',4,4'-biphenyltetracarboxylic anhydride

: 10526-07-5
1,3-bis (3-aminophenoxy)-benzene

: 119389-05-8
4-(2-phenylethynyl)phthalic anhydride

polymer; monomer(s); 3,3',4,4'-biphenyltetracarboxylic dianhydride; 3,4'-oxydianiline; 1,3-bis(3-aminophenoxy)benzene; 4-phenylethynylphthalic anhydride: polymer; monomer(s); 3,3',4,4'-biphenyltetracarboxylic dianhydride; 3,4'-oxydianiline; 1,3-bis(3-aminophenoxy)benzene; 4-phenylethynylphthalic anhydride

Conditions

Conditions	Yield
Stage #1: 3,4'-diaminodiphenyl ether; 3,3',4,4'-biphenyltetracarboxylic anhydride; 1,3-bis (3-aminophenoxy)-benzene; 4-(2-phenylethynyl)phthalic anhydride In 1-methyl-pyrrolidin-2-one Stage #2: In 1-methyl-pyrrolidin-2-one; toluene Heating; Further stages.;

...Expand

: 4-(1-naphthylethynyl)phthalic anhydride

: 2657-87-6
3,4'-diaminodiphenyl ether

: 2420-87-3
3,3',4,4'-biphenyltetracarboxylic anhydride

: 10526-07-5
1,3-bis (3-aminophenoxy)-benzene

polymer; monomer(s); 3,3',4,4'-biphenyltetracarboxylic dianhydride; 3,4'-oxydianiline; 1,3-bis(3-aminophenoxy)benzene; 4-(1-naphthylethynyl)phthalic anhydride: polymer; monomer(s); 3,3',4,4'-biphenyltetracarboxylic dianhydride; 3,4'-oxydianiline; 1,3-bis(3-aminophenoxy)benzene; 4-(1-naphthylethynyl)phthalic anhydride

Conditions

Conditions	Yield
Stage #1: 4-(1-naphthylethynyl)phthalic anhydride; 3,4'-diaminodiphenyl ether; 3,3',4,4'-biphenyltetracarboxylic anhydride; 1,3-bis (3-aminophenoxy)-benzene In 1-methyl-pyrrolidin-2-one Stage #2: In 1-methyl-pyrrolidin-2-one; toluene Heating; Further stages.;

...Expand

: 2657-87-6
3,4'-diaminodiphenyl ether

: 2420-87-3
3,3',4,4'-biphenyltetracarboxylic anhydride

: 10526-07-5
1,3-bis (3-aminophenoxy)-benzene

: 170804-03-2
4-(1-phenylethynyl)-1,8-naphthalic anhydride

polymer; monomer(s); 3,3',4,4'-biphenyltetracarboxylic dianhydride; 3,4'-oxydianiline; 1,3-bis(3-aminophenoxy)benzene; 4-phenylethynyl-1,8-naphthalic anhydride: polymer; monomer(s); 3,3',4,4'-biphenyltetracarboxylic dianhydride; 3,4'-oxydianiline; 1,3-bis(3-aminophenoxy)benzene; 4-phenylethynyl-1,8-naphthalic anhydride

Conditions

Conditions	Yield
Stage #1: 3,4'-diaminodiphenyl ether; 3,3',4,4'-biphenyltetracarboxylic anhydride; 1,3-bis (3-aminophenoxy)-benzene; 4-(1-phenylethynyl)-1,8-naphthalic anhydride In 1-methyl-pyrrolidin-2-one Stage #2: In 1-methyl-pyrrolidin-2-one; toluene Heating; Further stages.;

...Expand

: 446833-79-0
4-(1-naphthylethynyl)-1,8-naphthalic anhydride

: 2657-87-6
3,4'-diaminodiphenyl ether

: 2420-87-3
3,3',4,4'-biphenyltetracarboxylic anhydride

: 10526-07-5
1,3-bis (3-aminophenoxy)-benzene

polymer; monomer(s); 3,3',4,4'-biphenyltetracarboxylic dianhydride; 3,4'-oxydianiline; 1,3-bis(3-aminophenoxy)benzene; 4-(1-naphthylethynyl)-1,8-naphthalic anhydride: polymer; monomer(s); 3,3',4,4'-biphenyltetracarboxylic dianhydride; 3,4'-oxydianiline; 1,3-bis(3-aminophenoxy)benzene; 4-(1-naphthylethynyl)-1,8-naphthalic anhydride

Conditions

Conditions	Yield
Stage #1: 4-(1-naphthylethynyl)-1,8-naphthalic anhydride; 3,4'-diaminodiphenyl ether; 3,3',4,4'-biphenyltetracarboxylic anhydride; 1,3-bis (3-aminophenoxy)-benzene In various solvent(s) at 20℃; for 12h; Stage #2: With isoquinoline In various solvent(s) for 8h; Heating; Further stages.;

...Expand

: 393570-77-9
[2,4-bis(3-aminophenoxy)phenyl]diphenylphosphine oxide

: 1823-59-2
4,4'-oxydiphthalic dianhydride

: 10526-07-5
1,3-bis (3-aminophenoxy)-benzene

polymer, elong = 5.0%; monomer(s): [2,4-bis(3-aminophenoxy)phenyl]diphenylphosphine oxide; 4,4'-oxydiphthalic dianhydride; 1,3-bis(3-aminophenoxy)benzene: polymer, elong = 5.0%; monomer(s): [2,4-bis(3-aminophenoxy)phenyl]diphenylphosphine oxide; 4,4'-oxydiphthalic dianhydride; 1,3-bis(3-aminophenoxy)benzene

Conditions

Conditions	Yield
Stage #1: [2,4-bis(3-aminophenoxy)phenyl]diphenylphosphine oxide; 4,4'-oxydiphthalic dianhydride; 1,3-bis (3-aminophenoxy)-benzene In 1-methyl-pyrrolidin-2-one at 23℃; Stage #2: With pyridine; acetic anhydride In 1-methyl-pyrrolidin-2-one at 23℃; Further stages.;

...Expand

: 393570-77-9
[2,4-bis(3-aminophenoxy)phenyl]diphenylphosphine oxide

: 10526-07-5
1,3-bis (3-aminophenoxy)-benzene

: 1107-00-2
4,4'-(1,1,1,3,3,3-hexafluoroisopropylidene)diphthalic anhydride

polymer, elong = 4.1%; monomer(s): [2,4-bis(3-aminophenoxy)phenyl]diphenylphosphine oxide; 6FDA; 1,3-bis(3-aminophenoxy)benzene: polymer, elong = 4.1%; monomer(s): [2,4-bis(3-aminophenoxy)phenyl]diphenylphosphine oxide; 6FDA; 1,3-bis(3-aminophenoxy)benzene

Conditions

Conditions	Yield
Stage #1: [2,4-bis(3-aminophenoxy)phenyl]diphenylphosphine oxide; 1,3-bis (3-aminophenoxy)-benzene; 4,4'-(1,1,1,3,3,3-hexafluoroisopropylidene)diphthalic anhydride In 1-methyl-pyrrolidin-2-one at 23℃; Stage #2: With pyridine; acetic anhydride In 1-methyl-pyrrolidin-2-one at 23℃; Further stages.;

...Expand

: 1823-59-2
4,4'-oxydiphthalic dianhydride

: 10526-07-5
1,3-bis (3-aminophenoxy)-benzene

: 119389-05-8
4-(2-phenylethynyl)phthalic anhydride

A poly(4,4'-oxydiphthalic acid dianhydride-co-1,3-bis(3-aminophenoxy)benzene-co-4-phenylethynylphthalic anhydride): poly(4,4'-oxydiphthalic acid dianhydride-co-1,3-bis(3-aminophenoxy)benzene-co-4-phenylethynylphthalic anhydride)

B: 2387-23-7
1,3-Dicyclohexylurea

Conditions

Conditions	Yield
Stage #1: 4,4'-oxydiphthalic dianhydride; 1,3-bis (3-aminophenoxy)-benzene; 4-(2-phenylethynyl)phthalic anhydride In 1-methyl-pyrrolidin-2-one at 20℃; for 3h; Stage #2: With dicyclohexyl-carbodiimide In 1-methyl-pyrrolidin-2-one at 5 - 20℃; for 4h;

...Expand

: 4461-52-3
methoxymethanol

: 10526-07-5
1,3-bis (3-aminophenoxy)-benzene

: 108-39-4
3-methyl-phenol

: C36H32N2O4

Conditions

Conditions	Yield
Stage #1: methoxymethanol; 1,3-bis (3-aminophenoxy)-benzene at 50℃; Inert atmosphere; Stage #2: 3-methyl-phenol at 90℃; for 6h; Inert atmosphere;	160 g

...Expand

: 1823-59-2
4,4'-oxydiphthalic dianhydride

: 10526-07-5
1,3-bis (3-aminophenoxy)-benzene

: C52H34N4O9

Conditions

Conditions	Yield
at 220℃; Inert atmosphere;

1,3-Bis(3-aminophenoxy)benzene Specification

The IUPAC name of Benzenamine,3,3'-[1,3-phenylenebis(oxy)]bis- is 3-[3-(3-aminophenoxy)phenoxy]aniline . With the CAS registry number 10526-07-5, it is also named as 3,3'-(m-Phenylenebis(oxy))dianiline ; 1,3-Bis(3-aminophenoxy)benzene ; 1,3-Phenylenebis(3-oxyaniline) ; 3,3'-[1,3-Phenylenebis(oxy)]dianiline . The product's categories are aromatic hydrocarbons (substituted) & derivatives, miscellaneous, diphenyl ethers (for high-performance polymer research), functional materials and reagent for high-performance polymer research.

The Benzenamine,3,3'-[1,3-phenylenebis(oxy)]bis- is harmful by inhalation, in contact with skin and if swallowed. In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. If you want to contact this product, you must wear suitable protective clothing, gloves and eye/face protection.

The other characteristics of this product can be summarized as: (1)ACD/LogP: 3.05 ; (2)# of Rule of 5 Violations: 0 ; (3)ACD/LogD (pH 5.5): 3.02 ; (4)ACD/LogD (pH 7.4): 3.05 ; (5)ACD/BCF (pH 5.5): 115.02 ; (6)ACD/BCF (pH 7.4): 122.02 ; (7)ACD/KOC (pH 5.5): 1021.71 ; (8)ACD/KOC (pH 7.4): 1083.9 ; (9)#H bond acceptors: 4 ; (10)#H bond donors: 4 ; (11)#Freely Rotating Bonds: 6 ; (12)Index of Refraction: 1.667 ; (13)Molar Refractivity: 87.61 cm³; (14)Molar Volume: 235.1 cm³ ; (15)Polarizability: 34.73×10^-24 cm³; (16)Surface Tension: 55.2 dyne/cm ; (17)Enthalpy of Vaporization: 74.43 kJ/mol ; (18)Vapour Pressure: 2.27E-09 mmHg at 25°C ; (19)Rotatable Bond Count: 4 ; (20)Exact Mass: 292.121178 ; (21)MonoIsotopic Mass: 292.121178 ; (22)Topological Polar Surface Area: 70.5 ; (23)Heavy Atom Count: 22.

People can use the following data to convert to the molecule structure. SMILES: O(c1cc(N)ccc1)c3cccc(Oc2cccc(N)c2)c3; InChI: InChI=1/C18H16N2O2/c19-13-4-1-6-15(10-13)21-17-8-3-9-18(12-17)22-16-7-2-5-14(20)11-16/h1-12H,19-20H2; InChIKey: DKKYOQYISDAQER-UHFFFAOYAA. Benzenamine,3,3'-[1,3-phenylenebis(oxy)]bis- has many suppliers, such as Changzhou Sunlight Pharmaceutical Co., Ltd.. The price of this product changes with the market.

Product Name

1,3-Bis(3-aminophenoxy)benzene

Synthetic route

1,3-Bis(3-aminophenoxy)benzene Specification

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