3-Nitrobenzyl alcohol supplier

: 99-61-6
3-nitro-benzaldehyde

: 619-25-0
3-Nitrobenzyl alcohol

Conditions

Conditions	Yield
With magnesium(II) perchlorate; polymer-bound NADH (2a) In acetonitrile; benzene at 80℃; for 120h; Further byproducts given;	100%
With sodium tetrahydroborate In ethanol at 20℃; for 0.5h; Inert atmosphere;	100%
With sodium tetrahydroborate In ethanol at 0 - 20℃;	99%

: 18483-95-9
2-<3-Nitro-benzyloxy>-tetrahydro-pyran

: 619-25-0
3-Nitrobenzyl alcohol

Conditions

Conditions	Yield
With aluminium trichloride; 2-(3-nitrophenyl)-1,3-dioxolane; 1-benzyl-4-aza-1-azoniabicyclo[2.2.2]octane dichromate for 0.05h;	100%
With silica triflate In methanol for 0.133333h; Heating;	95%
With 1-benzyl-4-aza-1-azoniabicyclo[2.2.2]octane dichromate In dichloromethane for 0.0569444h; Irradiation;	93%

: 62673-14-7
trimethyl(3-nitrobenzyloxy)silane

: 619-25-0
3-Nitrobenzyl alcohol

Conditions

Conditions	Yield
With aluminium trichloride; 2-(3-nitrophenyl)-1,3-dioxolane; 1-benzyl-4-aza-1-azoniabicyclo[2.2.2]octane dichromate for 0.05h;	100%
With bismuth(lll) trifluoromethanesulfonate In methanol at 20℃; for 0.0666667h;	97%
With Oxone In methanol for 0.4h; Heating;	96%

: C28H24BN4O12(1-)*Na(1+)

: 619-25-0
3-Nitrobenzyl alcohol

Conditions

Conditions	Yield
With water	100%

: 121-90-4
m-nitrobenzoic acid chloride

: 619-25-0
3-Nitrobenzyl alcohol

Conditions

Conditions	Yield
With N-methylpyrrolidine zinc borohydride In tetrahydrofuran at 20℃; for 0.666667h;	98%
With (1,4-diazabicyclo{2.2.2}-octane)zinc(II) tetrahydoborate In tetrahydrofuran for 0.08h; Ambient temperature;	90%

: 1058649-37-8
3-nitro-1-[(ethoxymethoxy)methyl]benzene

: 619-25-0
3-Nitrobenzyl alcohol

Conditions

Conditions	Yield
phosphotungstic acid In ethanol for 2h; Heating;	97%

: 256334-95-9
tert-butyl-dimethyl-(3-nitro-benzyloxy)-silane

: 619-25-0
3-Nitrobenzyl alcohol

Conditions

Conditions	Yield
With Decaborane In methanol at 20℃; for 5h;	93%

: 50-00-0
formaldehyd

: 13331-27-6
m-nitrobenzene boronic acid

: 619-25-0
3-Nitrobenzyl alcohol

Conditions

Conditions	Yield
With C62H74Cl2N4Pd2S2; caesium carbonate In tetrahydrofuran; water at 50℃; for 2h; Inert atmosphere; Sealed tube;	93%
With di-μ-chloro-bis{2-[3-(2,6-diisopropylphenyl)imidazolin-2-ylidene]-(3-phenylthio)phenyl-κ2C,C’}dipalladium(II) In tetrahydrofuran; water at 70℃; for 2h; Inert atmosphere; Sealed tube; Alkaline conditions;	91%
With bis(η3-allyl-μ-chloropalladium(II)); 1-(2-bromophenyl)-3-(2,6-diisopropylphenyl)-4,5-dihydroimidazolinium chloride In tetrahydrofuran; water at 100℃; for 2h; Inert atmosphere; Sealed tube;	73%

: 99-61-6
3-nitro-benzaldehyde

A: 619-25-0
3-Nitrobenzyl alcohol

B: 121-92-6
3-nitrobenzoic acid

Conditions

Conditions	Yield
Stage #1: 3-nitro-benzaldehyde With potassium hydroxide In water at 20℃; Cannizzaro reaction; Stage #2: With hydrogenchloride In water	A 92% B 80%
With potassium hydroxide at 20℃; for 0.166667h; solvent-free Cannizzaro reaction;	A 33% B 53%
With N,N,N',N'-tetramethylguanidine In water at 100℃; for 10h; Cannizzaro reaction;	A 42% B 43%

: 618-95-1
methyl 3-nitrobenzoate

: 619-25-0
3-Nitrobenzyl alcohol

Conditions

Conditions	Yield
With sodium tetrahydroborate; ethanol; cerium(III) chloride heptahydrate at 20℃; for 24h; chemospecific reaction;	91%
With sodium tetrahydroborate; zinc phthalocyanine In PEG-400 at 100℃; for 10h;	90%
With sodium tetrahydroborate In 1,4-dioxane; water for 2h; Ambient temperature;	80%

: 121-92-6
3-nitrobenzoic acid

: 619-25-0
3-Nitrobenzyl alcohol

Conditions

Conditions	Yield
With zinc(II) tetrahydroborate In tetrahydrofuran for 4h; Heating;	90%
Stage #1: 3-nitrobenzoic acid With 1,3,5-trichloro-2,4,6-triazine; potassium carbonate; triphenylphosphine In neat (no solvent) for 0.0833333h; Green chemistry; Stage #2: With sodium tetrahydroborate In neat (no solvent) for 0.0833333h; Green chemistry;	71%
Stage #1: 3-nitrobenzoic acid With sodium aminodiboranate In tetrahydrofuran at 20℃; Stage #2: With water	70%

: 21388-97-6
3-nitrobenzyl acetate

: 619-25-0
3-Nitrobenzyl alcohol

Conditions

Conditions	Yield
With cucumber juice at 30 - 35℃; for 6h; Inert atmosphere; Green chemistry;	90%

: 69859-37-6
m-nitrobenzoic anhydride

A: 619-25-0
3-Nitrobenzyl alcohol

B: 121-92-6
3-nitrobenzoic acid

Conditions

Conditions	Yield
With methanol; sodium tetrahydroborate In tetrahydrofuran for 1h; Ambient temperature;	A 82% B 84%

: 142509-31-7
1-((methoxymethoxy)methyl)-3-nitrobenzene

: 619-25-0
3-Nitrobenzyl alcohol

Conditions

Conditions	Yield
phosphotungstic acid In ethanol for 2h; Heating;	82%

: C13H13NO3Si

: 619-25-0
3-Nitrobenzyl alcohol

Conditions

Conditions	Yield
With sodium hydroxide In water Schlenk technique; Inert atmosphere;	68%
With sodium hydroxide In water

: 64-17-5
ethanol

: 99-61-6
3-nitro-benzaldehyde

A: 618-98-4
ethyl 3-nitrobenzoate

B: 619-25-0
3-Nitrobenzyl alcohol

Conditions

Conditions	Yield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; benzyl chloride at 90℃; for 0.5h; Microwave irradiation;	A 67% B 17%

...Expand

: 645-09-0
3-nitrobenzamide

: 619-25-0
3-Nitrobenzyl alcohol

Conditions

Conditions	Yield
With C24H20ClN2OPRu; potassium tert-butylate; hydrogen In tetrahydrofuran at 110℃; under 10640.7 Torr; for 36h; Inert atmosphere; Schlenk technique;	66%

: 87199-15-3
[3-(hydroxymethyl)phenyl]boronic acid

: 619-25-0
3-Nitrobenzyl alcohol

Conditions

Conditions	Yield
With copper(I) oxide; ammonium hydroxide; oxygen; sodium nitrite In water at 25℃; for 36h;	50%

: 19479-81-3
(3-nitrophenyl)diazomethane

A: 619-25-0
3-Nitrobenzyl alcohol

B: 27183-43-3
di(3-nitrobenzyl) ether

C: 455-94-7
1-(fluoromethyl)-3-nitrobenzene

Conditions

Conditions	Yield
With tetrafluoroboric acid In dichloromethane for 0.166667h;	A 24% B 6% C 49%

...Expand

: 134361-00-5
3,3-dimethyl-2-butanone lithium enolate

: 99-61-6
3-nitro-benzaldehyde

A: 619-25-0
3-Nitrobenzyl alcohol

B: 56578-57-5
(E)-4,4-dimethyl-1-(3-nitrophenyl)pent-1-en-3-one

C: 1-hydroxy-4,4-dimethyl-1-(3-nitrophenyl)pentan-3-one

D: 121-92-6
3-nitrobenzoic acid

Conditions

Conditions	Yield
In neat (no solvent, solid phase) at 20℃; for 0.5h;	A n/a B 6% C 16% D n/a

...Expand

: 1342295-75-3
Br(1-)*C9H21N2O(1+)

: 99-61-6
3-nitro-benzaldehyde

A: 619-25-0
3-Nitrobenzyl alcohol

: 96875-03-5
trans-N,N-diethyl-3-(3-nitrophenyl)oxirane-2-carboxamide

C: 121-92-6
3-nitrobenzoic acid

Conditions

Conditions	Yield
Stage #1: Br(1-)*C9H21N2O(1+) With sodium hydroxide In dichloromethane; water at 0℃; for 0.0833333h; Inert atmosphere; Stage #2: 3-nitro-benzaldehyde In dichloromethane; water at 0 - 25℃; for 24h; Inert atmosphere; diastereoselective reaction;	A n/a B 12% C n/a

...Expand

: 67-56-1
methanol

: 56-23-5
tetrachloromethane

: 99-61-6
3-nitro-benzaldehyde

A: 619-25-0
3-Nitrobenzyl alcohol

B: 121-92-6
3-nitrobenzoic acid

Conditions

Conditions	Yield
Disproportionierung;

...Expand

: 50-00-0
formaldehyd

: 99-61-6
3-nitro-benzaldehyde

: 619-25-0
3-Nitrobenzyl alcohol

Conditions

Conditions	Yield
With potassium hydroxide

: 99-61-6
3-nitro-benzaldehyde

: 100-52-7
benzaldehyde

A: 619-25-0
3-Nitrobenzyl alcohol

B: 121-92-6
3-nitrobenzoic acid

...Expand

: 99-61-6
3-nitro-benzaldehyde

: 2269-22-9
aluminum tri-sec-butoxide

: 78-92-2, 15892-23-6
iso-butanol

: 619-25-0
3-Nitrobenzyl alcohol

...Expand

: 619-23-8
3-Nitrobenzyl chloride

: 619-25-0
3-Nitrobenzyl alcohol

Conditions

Conditions	Yield
With 2-nitropropane; tetra(n-butyl)ammonium hydroxide In dichloromethane

: 77934-67-9
2-Methyl-benzoic acid 3-nitro-benzyl ester

A: 118-90-1
ortho-methylbenzoic acid

B: 619-25-0
3-Nitrobenzyl alcohol

Conditions

Conditions	Yield
With water in alkaline medium In acetone Rate constant; Ambient temperature;

: (4-Nitro-phenyl)-acetic acid 3-nitro-benzyl ester

A: 104-03-0
4-nitrobenzeneacetic acid

B: 619-25-0
3-Nitrobenzyl alcohol

Conditions

Conditions	Yield
In hexane; chloroform Rate constant; Ambient temperature; antibody IgG 27H9 as catalyst; 15percent Bicine buffer (pH = 9.0);

: 619-25-0
3-Nitrobenzyl alcohol

: 1877-77-6
3-aminobenzenemethanol

Conditions

Conditions	Yield
With C37H23Cl2N7Pd2(2+)*2F6P(1-); hydrogen; sodium cyanoborohydride In methanol at 50℃; under 760.051 Torr; for 6h;	100%
With hydrazine hydrate In water at 110℃; Sealed tube; Green chemistry;	99%
With hydrogen In 2-methyltetrahydrofuran; water at 40℃; under 15001.5 Torr; for 24h; chemoselective reaction;	98%

: 619-25-0
3-Nitrobenzyl alcohol

: 619-23-8
3-Nitrobenzyl chloride

Conditions

Conditions	Yield
With 1,3,5-trichloro-2,4,6-triazine; dimethyl sulfoxide at 20℃; for 0.25h; chemoselective reaction;	100%
With oxalyl dichloride In dichloromethane at 20℃; Appel Halogenation; Reflux;	93%
With dimethyl sulfoxide; N-phenyl-benzimidoyl chloride In chloroform at 20℃; for 24h; Temperature; Time;	87%

: 619-25-0
3-Nitrobenzyl alcohol

: 121-92-6
3-nitrobenzoic acid

Conditions

Conditions	Yield
With peracetic acid; C23H27INO5 In acetic acid at 30℃; for 48h;	100%
With tetra-N-butylammonium tribromide In acetonitrile at 20℃; for 24h; Irradiation;	98%
With sodium hypochlorite; water at 25℃; for 0.583333h;	97%

: 619-25-0
3-Nitrobenzyl alcohol

: 322474-21-5
N,N'-bis-Boc-S-methyl-isothiourea

: C19H27N3O6S

Conditions

Conditions	Yield
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran Ambient temperature;	100%

: 619-25-0
3-Nitrobenzyl alcohol

: 126799-84-6
1-azidomethyl-3-nitrobenzene

Conditions

Conditions	Yield
With 2-azido-1,3-dimethyl-4,5-dihydro-1H-imidazol-3-ium hexafluorophosphate (V); 1,8-diazabicyclo[5.4.0]undec-7-ene In tetrahydrofuran at 20℃; for 1h;	100%
Stage #1: 3-Nitrobenzyl alcohol With 1H-imidazole; iodine; triphenylphosphine at 20℃; for 0.166667h; Stage #2: With sodium azide In dimethyl sulfoxide at 20℃; for 0.5h; chemoselective reaction;	82%
Multi-step reaction with 2 steps 1: phosphorus tribromide / diethyl ether / 0.5 h / 0 °C 2: sodium azide / dimethyl sulfoxide / 12 h / 20 °C View Scheme

: 619-25-0
3-Nitrobenzyl alcohol

: 99-61-6
3-nitro-benzaldehyde

Conditions

Conditions	Yield
With Montmorillonite K10; ferric nitrate In hexane at 60℃; for 3h;	99%
With tert.-butylhydroperoxide; V/SiO2 In decane; tert-butyl alcohol at 25℃; for 3h;	99.8%
With 4-methyl-morpholine; chromium(VI) oxide; hydrogenchloride In diethyl ether; chloroform at 65℃; for 0.0833333h; microwave irradiation;	99%

: 619-25-0
3-Nitrobenzyl alcohol

: 3958-57-4
1-bromomethyl-3-nitrobenzene

Conditions

Conditions	Yield
With trimethylsilyl bromide In neat (no solvent) at 20℃; for 24h; Green chemistry; chemoselective reaction;	99%
With 1H-imidazole; iodine In dichloromethane at 20℃; for 0.25h;	98%
With Oxalyl bromide In dichloromethane at 20℃; Appel Halogenation; Reflux;	91%

: 619-25-0
3-Nitrobenzyl alcohol

: 619-24-9
3-nitrobenzonitrile

Conditions

Conditions	Yield
Stage #1: 3-Nitrobenzyl alcohol With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tert-butylhypochlorite In dichloromethane at 20℃; for 1h; Inert atmosphere; Stage #2: With ammonia; iodine In dichloromethane; water at 20℃; for 2h; Inert atmosphere;	99%
With ammonium hydroxide; iodine at 60℃; for 3h;	92%
With ammonium hydroxide; iodine at 60℃; for 3h;	92%

: 99-34-3
3,5-dinitrobenzoic acid

: 619-25-0
3-Nitrobenzyl alcohol

: 3-nitrobenzyl 3,5-dinitrobenzoate

Conditions

Conditions	Yield
With [bis(acetoxy)iodo]benzene; triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 20℃; for 16h; Mitsunobu reaction; Inert atmosphere;	99%

: 619-25-0
3-Nitrobenzyl alcohol

: 108-24-7
acetic anhydride

: 21388-97-6
3-nitrobenzyl acetate

Conditions

Conditions	Yield
With bismuth(lll) trifluoromethanesulfonate In acetonitrile at 20℃; for 0.0833333h;	98%
K5 In acetonitrile at 20℃; for 0.25h;	98%
With decamolybdodivanadogermanic acid nanoparticles at 24.84℃; for 0.0916667h; Neat (no solvent);	94%

: 619-25-0
3-Nitrobenzyl alcohol

: 64-19-7
acetic acid

: 21388-97-6
3-nitrobenzyl acetate

Conditions

Conditions	Yield
With bismuth(III) chloride for 1.16667h; Heating;	98%
With K5 for 0.75h; Heating;	96%
With zirconium hydrogen sulfate In hexane at 20℃; for 1.4h;	95%

: 67-56-1
methanol

: 619-25-0
3-Nitrobenzyl alcohol

: 618-95-1
methyl 3-nitrobenzoate

Conditions

Conditions	Yield
With sodium carbonate; palladium; silver(l) oxide at 80℃; for 48h; Molecular sieve;	98%
Stage #1: 3-Nitrobenzyl alcohol In toluene at 80℃; for 2h; Sonication; Stage #2: methanol With Oxone In toluene for 1.5h; Sonication;	90%
With dibromamine-T; potassium carbonate In acetonitrile at 20℃; for 0.5h; Reagent/catalyst; Solvent;	88%

: 619-25-0
3-Nitrobenzyl alcohol

: 999-97-3
1,1,1,3,3,3-hexamethyl-disilazane

: 62673-14-7
trimethyl(3-nitrobenzyloxy)silane

Conditions

Conditions	Yield
With P2O5/silica gel In dichloromethane at 20℃; for 0.166667h;	98%
With Nafion SAC-13 at 20℃; for 0.0833333h;	97%
With potassium bromide In acetonitrile at 20℃; for 0.3h;	95%

: 619-25-0
3-Nitrobenzyl alcohol

: 1035459-75-6
ammonium m-nitrobenzyl H-phosphonate

Conditions

Conditions	Yield
With pyridine; diphenyl phosphite for 1h;	98%

: 1076-38-6
4-hydroxy[1]benzopyran-2-one

: 619-25-0
3-Nitrobenzyl alcohol

: 3,3'-((3-nitrophenyl)methylene)bis(4-hydroxy-2H-chromen-2-one)

Conditions

Conditions	Yield
With ammonium cerium (IV) nitrate; 1,2-dimethyl-3-[4-(1,2-dimethyl-1H-imidazol-3-ium-3-yl)butyl]-1H-imidazol-3-ium dibromide In neat (no solvent) at 20℃; for 0.333333h; Green chemistry;	98%

: 619-25-0
3-Nitrobenzyl alcohol

: 93-97-0
benzoic acid anhydride

: 38612-16-7
Benzoeseure-(3-nitrobenzylester)

Conditions

Conditions	Yield
With bismuth(lll) trifluoromethanesulfonate In acetonitrile for 0.416667h; Heating;	97%

: 619-25-0
3-Nitrobenzyl alcohol

: 1147550-11-5
ammonium thiocyanate

: 66907-51-5
3-nitrobenzyl thiocyanate

Conditions

Conditions	Yield
With fluorosulfonyl fluoride; sodium carbonate In ethyl acetate at 20℃; for 5h;	97%
With fluorosulfonyl fluoride; sodium carbonate In tetrahydrofuran at 20℃; for 5h;	93%

: 619-25-0
3-Nitrobenzyl alcohol

: 137-07-5
2-amino-benzenethiol

: 22868-33-3
2-(3-nitrophenyl)benzothiazole

Conditions

Conditions	Yield
With tetrabutyl phosphonium bromide In water at 80℃; for 2h; Catalytic behavior;	97%

: 619-25-0
3-Nitrobenzyl alcohol

: 4039-32-1
lithium hexamethyldisilazane

: 62673-14-7
trimethyl(3-nitrobenzyloxy)silane

Conditions

Conditions	Yield
With N-chlorosaccharin In neat (no solvent) at 20℃; for 0.0166667h;	96%

: 110-87-2
3,4-dihydro-2H-pyran

: 619-25-0
3-Nitrobenzyl alcohol

: 18483-95-9
2-<3-Nitro-benzyloxy>-tetrahydro-pyran

Conditions

Conditions	Yield
With titanium(IV) salophen trifluoromethanesulfonate In dichloromethane at 20℃; for 0.0166667h; chemoselective reaction;	95%
With silica triflate In hexane at 20℃; for 0.1h;	90%
With 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione In hexane at 20℃; for 0.366667h;	85%
With pyridine hydrochloride at 20℃; for 0.0666667h; Neat (no solvent);	75%

: 619-25-0
3-Nitrobenzyl alcohol

: 109-94-4
formic acid ethyl ester

: 3-nitrobenzyl formate

Conditions

Conditions	Yield
With bismuth(lll) trifluoromethanesulfonate for 1h; Heating;	95%
With K5 for 0.75h; Heating;	94%

: 619-25-0
3-Nitrobenzyl alcohol

: 859146-54-6
(3'-nitrobenzyl)-3-nitrobenzoate

Conditions

Conditions	Yield
With iodine; potassium carbonate In tert-butyl alcohol at 20℃; for 16h;	95%
With iodine; potassium carbonate In tert-butyl alcohol at 50℃; for 9h;	61%

: 619-25-0
3-Nitrobenzyl alcohol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 256334-95-9
tert-butyl-dimethyl-(3-nitro-benzyloxy)-silane

Conditions

Conditions	Yield
With ferric hydrogen sulphate; triethylamine at 20℃; for 5h; Inert atmosphere; chemoselective reaction;	95%
With 1H-imidazole In dichloromethane at 0 - 20℃; for 2h;	90%
With 1H-imidazole In dichloromethane at 0 - 20℃; for 3h;	87%

Product Name

3-Nitrobenzyl alcohol

Synthetic route

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