Hazard Codes | F,C |
Risk Statements | 11-34 |
Safety Statements | 16-26-36/37/39-45 |
RIDADR | UN 2924 3/PG 2 |
WGK Germany | 3 |
(5-fluoroindol-3-yl)dimethylsulfonium perchlorate
di-n-propylamine
A
N-methyldipropylamine
Conditions | Yield |
---|---|
for 1h; Inert atmosphere; Reflux; | A n/a B 98.5% |
Conditions | Yield |
---|---|
at 107℃; for 1h; Inert atmosphere; | A 98.1% B n/a |
(5-methylindol-3-yl)dimethylsulfonium perchlorate
di-n-propylamine
A
5-methyl-3-(methylthio)-1H-indole
B
N-methyldipropylamine
Conditions | Yield |
---|---|
for 1h; Inert atmosphere; Reflux; | A 96.6% B n/a |
(2-methylthioindol-3-yl)dimethylsulfonium perchlorate
di-n-propylamine
A
N-methyldipropylamine
B
2,3-bis(methylthio)indole
Conditions | Yield |
---|---|
for 1h; Inert atmosphere; Reflux; | A n/a B 96.5% |
(5-nitroindol-3-yl)dimethylsulfonium perchlorate
di-n-propylamine
A
N-methyldipropylamine
B
3-methylthio-5-nitroindole
Conditions | Yield |
---|---|
for 1h; Inert atmosphere; Reflux; | A n/a B 94.4% |
(4-bromoindol-3-yl)dimethylsulfonium perchlorate
di-n-propylamine
A
N-methyldipropylamine
B
4-bromo-3-methylthioindole
Conditions | Yield |
---|---|
for 1h; Inert atmosphere; Reflux; | A n/a B 93.1% |
Conditions | Yield |
---|---|
With zinc(II) tetrahydroborate; zinc(II) chloride In tetrahydrofuran for 8h; Ambient temperature; | 92% |
With formic acid | |
With formic acid Eschweiler-Clarke reaction; Reflux; | |
With potassium hydroxide In water at 80℃; for 2h; Time; Temperature; |
(indol-3-yl)methylphenylsulfonium perchlorate
di-n-propylamine
A
3-phenylthioindole
B
N-methyldipropylamine
Conditions | Yield |
---|---|
for 1h; Inert atmosphere; Reflux; | A 90.1% B n/a |
Conditions | Yield |
---|---|
for 1h; Inert atmosphere; Reflux; | A n/a B 87.3% |
(5-cyanoindol-3-yl)dimethylsulfonium perchlorate
di-n-propylamine
A
N-methyldipropylamine
B
3-methylthioindole-5-carbonitrile
Conditions | Yield |
---|---|
for 1h; Inert atmosphere; Reflux; | A n/a B 84.6% |
(5-bromoindol-3-yl)dimethylsulfonium perchlorate
di-n-propylamine
A
N-methyldipropylamine
Conditions | Yield |
---|---|
for 1h; Inert atmosphere; Reflux; | A n/a B 84.5% |
(2-carboethoxyindol-3-yl)dimethylsulfonium perchlorate
di-n-propylamine
A
N-methyldipropylamine
B
ethyl 3-methylthio-1H-indole-2-carboxylate
Conditions | Yield |
---|---|
for 1h; Inert atmosphere; Reflux; | A n/a B 81.9% |
(5-methoxyindol-3-yl)dimethylsulfonium perchlorate
di-n-propylamine
A
N-methyldipropylamine
B
5-methoxy-3-methylthioindole
Conditions | Yield |
---|---|
for 1h; Inert atmosphere; Reflux; | A n/a B 81.7% |
di-n-propylamine
A
N-methyldipropylamine
B
2,3-bis(methylthio)-5-nitroindole
Conditions | Yield |
---|---|
for 2h; Inert atmosphere; Reflux; | A n/a B 76.9% |
ethylmagnesium bromide
3-methyl-1,5,3-dioxazepane
N-methyldipropylamine
Conditions | Yield |
---|---|
35% |
Conditions | Yield |
---|---|
With water |
Conditions | Yield |
---|---|
With ethanol; acetic acid; platinum Hydrogenation; |
Methyltrimethoxyphosphonium tetrafluoroborate
di-n-propylamine
N-methyldipropylamine
Conditions | Yield |
---|---|
for 12h; Ambient temperature; | 51 % Chromat. |
nitromethane
ethanol
acetic acid
propionaldehyde
N-methyldipropylamine
Conditions | Yield |
---|---|
in Gegenwart von Platinoxyd; analoge Reaktion mit Nitrobenzol; |
ethene
dimethyl amine
A
formic acid
B
N,N-dimethylaminopropane
C
N-methyldipropylamine
Conditions | Yield |
---|---|
at 120 - 125℃; under 139746 - 147102 Torr; | |
at 120 - 125℃; under 139746 - 147102 Torr; |
ethene
water
methylamine
A
N-methyldipropylamine
B
methyl-n-propylamine
Conditions | Yield |
---|---|
at 120 - 140℃; under 125036 - 132391 Torr; | |
at 120 - 140℃; under 125036 - 132391 Torr; |
Conditions | Yield |
---|---|
With iron pentacarbonyl; water at 120 - 140℃; under 125036 - 147102 Torr; | |
With iron pentacarbonyl; water at 120 - 140℃; under 125036 - 147102 Torr; |
Conditions | Yield |
---|---|
With iron pentacarbonyl; water at 120 - 140℃; under 125036 - 147102 Torr; | |
With iron pentacarbonyl; water at 120 - 140℃; under 125036 - 147102 Torr; |
Conditions | Yield |
---|---|
With ethene; carbon monoxide at 130℃; under 147102 Torr; |
ammonia
tri-n-propyl-methylammonium chloride
A
tri-n-propylamine
B
propene
C
methane
D
N-methyldipropylamine
Conditions | Yield |
---|---|
at -78℃; Mechanism; |
tri-n-propyl-methylammonium iodide
ammonia
A
tri-n-propylamine
B
propene
C
methane
D
N-methyldipropylamine
Conditions | Yield |
---|---|
at -33℃; Mechanism; |
Conditions | Yield |
---|---|
With hydrogen In 1,2-dimethoxyethane at 160℃; under 22502.3 Torr; for 20h; Inert atmosphere; Autoclave; Molecular sieve; |
Conditions | Yield |
---|---|
With Iridium(II)-coordinated mesoporous (4-[5-(4-aminophenyl)-4'-methyl-[1,1'-biphenyl]-3-yl]aniline)-modified Tröger’s base-functionalized polymer at 110℃; for 24h; | 60 %Chromat. |
With potassium phosphate; tris(2-diphenylphosphinoethyl)phosphine; cobalt acetylacetonate at 140℃; for 24h; Inert atmosphere; Autoclave; | > 99 %Chromat. |
N-methyldipropylamine
24-nor-23-iodo-3α,12α-dihydroxy-7-deoxy-5β-cholane
Conditions | Yield |
---|---|
In acetonitrile for 6h; Heating; | 75% |
Conditions | Yield |
---|---|
In acetonitrile for 12h; Reflux; | 74% |
N-methyldipropylamine
2-bromoethanol
N-(2-hydroxyethyl)-N-methyl-N-propylpropan-1-ammoniumbromide
Conditions | Yield |
---|---|
In acetonitrile for 4h; Reflux; | 68% |
5-methyl-1,3-benzoxazole
N-methyldipropylamine
5-methyl-N,N-dipropylbenzo[d]oxazol-2-amine
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide; acetic acid In water; acetonitrile at 100℃; for 0.333333h; Microwave irradiation; Green chemistry; | 57% |
benzoxazole
N-methyldipropylamine
N,N-dipropylbenzo[d]oxazol-2-amine
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide; acetic acid In water; acetonitrile at 100℃; for 0.333333h; Microwave irradiation; Green chemistry; | 55% |
4-toluenesulfonyl azide
N-methyldipropylamine
(E)-N'-((4-methylphenyl)sulfonyl)-N,N-dipropylformimidamide
Conditions | Yield |
---|---|
With 4-nitroacenaphthene In dichloromethane at 20℃; for 12h; Irradiation; | 32% |
Conditions | Yield |
---|---|
With diethyl ether |
N-methyldipropylamine
1-Chloro-1,1,2,2,3,3,4,4,5,5,6,6-dodecafluoro-6-iodo-hexane
A
1-chloro-1H,6H-dodecafluoro-hexane
B
<2-methyl-2-(ω-chlorododecafluoro-n-hexyl)vinyl>-n-propylmethylamine
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0) In hexane at 60℃; for 0.5h; |
Molecular Structure:
Molecular Formula: C7H17N
Molecular Weight: 115.2166
IUPAC Name: N-Methyl-N-propylpropan-1-amine
Synonyms of N-Methyldipropylamine (CAS NO.3405-42-3): Methyl di-n-propylamine ; 1-Propanamine, N-methyl-N-propyl- ; 1-Propanamine,N-methyl-N-propyl- ; Dipropylamine,N-methyl- ; Dipropylmethylamine ; Methyl dipropyl amine ; Methyldipropylamine
CAS NO: 3405-42-3
Product Categories: Polyamines ; Amines ; C7 ; Nitrogen Compounds
Index of Refraction: 1.418
Molar Refractivity: 38.2 cm3
Molar Volume: 151.3 cm3
Surface Tension: 24.3 dyne/cm
Density: 0.761 g/cm3
Flash Point: 11.2 °C
Enthalpy of Vaporization: 35.51 kJ/mol
Boiling Point: 116.7 °C at 760 mmHg
Vapour Pressure of N-Methyldipropylamine (CAS NO.3405-42-3): 18 mmHg at 25°C
Hazard Codes of N-Methyldipropylamine (CAS NO.3405-42-3): F,C
Risk Statements: 11-34
R11: Highly flammable.
R34: Causes burns.
Safety Statements: 16-26-36/37/39-45
S16: Keep away from sources of ignition.
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
S36/37/39: Wear suitable protective clothing, gloves and eye/face protection.
S45: In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.)
RIDADR: UN 2924 3/PG 2
WGK Germany: 3
HazardClass: CORROSIVE
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