sodium chlorite
A
sodium hypophosphite
Conditions | Yield |
---|---|
In water |
sodium chlorite
A
sodium hypophosphite
Conditions | Yield |
---|---|
In water |
water
A
sodium hypophosphite
C
hydrogen
D
phosphan
E
sodium hydroxide
Conditions | Yield |
---|---|
In water reaction of Na3P with H2O;; |
water
A
sodium hypophosphite
B
diphosphane
D
hydrogen
E
sodium hydroxide
Conditions | Yield |
---|---|
In water reaction by prepn. of PH3;; |
sodium dihydrogenphosphate
sodium hypophosphite
Conditions | Yield |
---|---|
In neat (no solvent) other Radiation; on irradiation with neutrons at -79°C for 30min (2*E+12 n/cm*cm*s);; in mixture with other products;; | |
In neat (no solvent) other Radiation; on irradiation with neutrons at -79°C for 30min (2*E+12 n/cm*cm*s);; in mixture with other products;; |
Conditions | Yield |
---|---|
With sodium hydroxide; water 100-250°C; product depending on temp.; |
phosphorous
sodium hypophosphite
Conditions | Yield |
---|---|
With sodium hydroxide; water 100°C; very slow reaction; |
phosphorous
sodium hydroxide
A
sodium hypophosphite
C
hydrogen
D
phosphan
Conditions | Yield |
---|---|
In sodium hydroxide on heating;; |
Conditions | Yield |
---|---|
In neat (no solvent) quantitative dehydration in vac. over P2O5 at 100°C;; | |
In neat (no solvent) quantitative dehydration in vac. over P2O5 at 100°C;; |
sodium hypophosphite
Conditions | Yield |
---|---|
With bromine In carbon disulfide excess of Br2; |
Conditions | Yield |
---|---|
With water In tetrahydrofuran-d8 Inert atmosphere; Schlenk technique; |
Conditions | Yield |
---|---|
Stage #1: sodium hypophosphite; ethene; acetic acid With tert-Butyl peroxybenzoate; pyrographite at 100 - 110℃; under 2250.23 - 3750.38 Torr; for 2.5h; Sealed tube; Inert atmosphere; Stage #2: aluminum(III) sulfate In water for 0.5h; pH=3; | 86.6% |
sodium hypophosphite
A
sodium dihydrogenphosphate
B
sodium phosphite
Conditions | Yield |
---|---|
With nickel on silica for 2h; Reflux; | A n/a B 53% |
sodium hypophosphite
4-Phenyl-1-butene
(4-phenylbutyl)phosphinic acid
Conditions | Yield |
---|---|
With triethyl borane In methanol at 20℃; for 4h; |
Conditions | Yield |
---|---|
With sodium hydroxide In water at 160 - 221℃; under 19135 Torr; for 0.633333h; Product distribution / selectivity; |
Conditions | Yield |
---|---|
With sodium acetate In not given 95-99°C , pH=5; | |
With Na acetate In not given 95-99°C , pH=5; |
Conditions | Yield |
---|---|
With Na3C6H5O7 In water Ni layer formed on Al2O3 in soln. of NiSO4*7H2O, NaH2PO2 and sodium citrate at 80 °C (pH=5) for 15 h; | |
With sodium acetate; boric acid; ammonium chloride In not given | |
With Na acetate; H3BO3; NH4Cl In not given |
Conditions | Yield |
---|---|
With sodium citrate In not given 92-98°C; | |
With Na citrate; Na lactate In not given 92-98°C; |
sodium hypophosphite
Conditions | Yield |
---|---|
In neat (no solvent) thermic decompn.;; | |
In neat (no solvent) thermic decompn.;; |
sodium hypophosphite
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: PH3, NaPO3, H2; on heating to 275°C;; | |
In neat (no solvent) byproducts: PH3, NaPO3, Na3PO4; on heating to 500°C;; | |
With mercury(II) oxide In water 10-15°C, several days;; |
sodium hypophosphite
Conditions | Yield |
---|---|
thermal decompn.; small amt. of red P formed; |
sodium hypophosphite
perchloric acid
water
A
phosphonic Acid
B
phosphoric acid
Conditions | Yield |
---|---|
In perchloric acid Kinetics; excess hypophosphite, 0.1-2.5 M HClO4, I=2.5 M (NaClO4), 35-55°C (H3PO5 generated in situ or prepd. on treatment of K4P2O8 with 1.0 M HClO4 at 45°C for 4 h); not isolated, reaction followed by titrimetry of peroxo-group; |
sodium hypophosphite
water
A
sodium phosphite
B
hydrogen
C
nitric acid
D
silver
Conditions | Yield |
---|---|
With ethoxylated alkylphenols mixt. In cyclohexane; water mixing AgNO3 and NaH2PO2 microemulsions at room temp.; detd. by x-ray scattering and electron spectroscopy; |
sodium hypophosphite
water
A
sodium phosphite
B
nitric acid
C
silver
Conditions | Yield |
---|---|
With ethoxylated alkylphenols mixt. In cyclohexane; water mixing AgNO3 and NaH2PO2 microemulsions at room temp.; detd. by x-ray scattering and electron spectroscopy; |
Conditions | Yield |
---|---|
With sulfuric acid In water Kinetics; 25°C, pH 2-4; without isolation; UV (350 nm), polarography; |
sodium hypophosphite
Conditions | Yield |
---|---|
In water heating a soln. of Cr(NO3)3 and NaH2PO2 at 100°C; |
sodium hypophosphite
nickel diacetate
nickel
Conditions | Yield |
---|---|
With sodium acetate In not given activated by PdCl2; | |
With Na acetate In not given activated by PdCl2; |
Conditions | Yield |
---|---|
With formic acid; hydrogen iodide by reduction with mixture of HI, HCCOH and NaH2PO2; |
sodium hypophosphite
Conditions | Yield |
---|---|
With Na3(C6H5O7) In water electroless plating (Cu substrate, 60-90°C, pH 7-11 by NaOH/H2SO4, 10 min); X-ray diffraction, scanning electron microscopy; |
sodium hypophosphite
Conditions | Yield |
---|---|
With Na3(C6H5O7) In water electroless plating (Cu substrate, 60-90°C, pH 7-11 by NaOH/H2SO4, 10 min); X-ray diffraction, scanning electron microscopy; |
sodium hypophosphite
Conditions | Yield |
---|---|
With Na3(C6H5O7) In water electroless plating (Cu substrate, 60-90°C, pH 7-11 by NaOH/H2SO4, 10 min); X-ray diffraction, scanning electron microscopy; |
sodium hypophosphite
Conditions | Yield |
---|---|
With Na3(C6H5O7) In water electroless plating (Cu substrate, 60-90°C, pH 7-11 by NaOH/H2SO4, 10 min); X-ray diffraction, scanning electron microscopy; |
sodium hypophosphite
Conditions | Yield |
---|---|
With Na3(C6H5O7) In water electroless plating (Cu substrate, 60-90°C, pH 7-11 by NaOH/H2SO4, 10 min); X-ray diffraction, scanning electron microscopy; |
sodium hypophosphite
Conditions | Yield |
---|---|
With Na3(C6H5O7) In water electroless plating (Cu substrate, 60-90°C, pH 7-11 by NaOH/H2SO4, 10 min); X-ray diffraction, scanning electron microscopy; |
sodium hypophosphite
Conditions | Yield |
---|---|
With Na3(C6H5O7) In water electroless plating (Cu substrate, 60-90°C, pH 7-11 by NaOH/H2SO4, 10 min); X-ray diffraction, scanning electron microscopy; |
sodium hypophosphite
Conditions | Yield |
---|---|
With Na3(C6H5O7) In water electroless plating (Cu substrate, 60-90°C, pH 7-11 by NaOH/H2SO4, 10 min); X-ray diffraction, scanning electron microscopy; |
Conditions | Yield |
---|---|
With water In water byproducts: HNO3; aq. solns. mixed; diluted, stored, filtered, washed with water, dried; |
Conditions | Yield |
---|---|
palladium dichloride In water | |
In ammonia byproducts: Co phosphide; pptn. of mixture;; |
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