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Name:bifonazole CAS NO: 60628-96-8 Grade:Medical scientific research and export Molecular formula:C22H18N2 Molecular weight:310.3917 Product Quality 12 years of chemical raw materials Mature operation of the industry System stability Data
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inquirymoderate price & quick delivery Appearance:powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:antibacterial Transportation:BY SEA Port:Sha
(R,S)-1-<α-(4-Biphenylyl)benzyl>imidazole-4,5-dicarboxylic acid
bifonazole
Conditions | Yield |
---|---|
In diphenylether for 0.5h; Heating; | 98% |
Conditions | Yield |
---|---|
Stage #1: 4-benzylbiphenyl With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) In tetrachloromethane for 0.833333h; Inert atmosphere; Reflux; Stage #2: 1H-imidazole With potassium carbonate In acetonitrile for 1h; Reflux; | 77% |
Stage #1: 4-benzylbiphenyl With pyridine; tert.-butylhydroperoxide; iodine In decane; water at 80℃; for 12h; Schlenk technique; Inert atmosphere; Stage #2: 1H-imidazole With formic acid; toluene-4-sulfonic acid In water at 180 - 200℃; for 10h; Schlenk technique; Inert atmosphere; | 66% |
Conditions | Yield |
---|---|
With copper acetylacetonate; tetrabutylammomium bromide In toluene at 85℃; for 36h; | 52% |
Conditions | Yield |
---|---|
In 1-methyl-pyrrolidin-2-one Heating; | 12% |
Conditions | Yield |
---|---|
With bis(dicyclohexylphenylphosphine)nickel(II) chloride In diethyl ether at 80℃; for 15h; |
4-phenylbenzhydrol
bifonazole
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 96 percent / DEAD, Ph3P / tetrahydrofuran / 24 h / Ambient temperature 2: 85 percent / NaOH / ethanol / 24 h / Heating 3: 98 percent / diphenyl ether / 0.5 h / Heating View Scheme | |
Multi-step reaction with 2 steps 1.1: triethylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere 2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 0 °C / Inert atmosphere 2.2: 0 - 100 °C / Inert atmosphere View Scheme |
1-<α-(4-Biphenylyl)benzyl>imidazole-4,5-dicarbonitrile
bifonazole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 85 percent / NaOH / ethanol / 24 h / Heating 2: 98 percent / diphenyl ether / 0.5 h / Heating View Scheme |
4-(chlorophenylmethyl)-1,1'-biphenyl
1-(Trimethylsilyl)imidazole
bifonazole
Conditions | Yield |
---|---|
In acetonitrile |
Conditions | Yield |
---|---|
Stage #1: 1H-imidazole; 4-phenylbenzhydrol With ammonium bromide In water at 125 - 130℃; for 2h; Industrial scale; Stage #2: With ammonium bromide In water at 190 - 195℃; for 2h; Temperature; Industrial scale; |
trimethylphenylsilane
bifonazole
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: silver(I) 4-methylbenzenesulfonate; dichloro(N-(diphenylphosphino)-N-isopropyl-1,1-diphenylphosphinamine) digold(I); [bis(acetoxy)iodo]benzene / 1,1,1-trichloroethane / 2 h / 110 °C / Inert atmosphere; Schlenk technique 2.1: aluminum oxide; sodium tetrahydroborate / ethanol / 0.67 h / 20 °C / Inert atmosphere 3.1: triethylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere 4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 0 °C / Inert atmosphere 4.2: 0 - 100 °C / Inert atmosphere View Scheme |
(4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)phenyl)(phenyl)methanone
bifonazole
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: silver(I) 4-methylbenzenesulfonate; dichloro(N-(diphenylphosphino)-N-isopropyl-1,1-diphenylphosphinamine) digold(I); [bis(acetoxy)iodo]benzene / 1,1,1-trichloroethane / 2 h / 110 °C / Inert atmosphere; Schlenk technique 2.1: aluminum oxide; sodium tetrahydroborate / ethanol / 0.67 h / 20 °C / Inert atmosphere 3.1: triethylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere 4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 0 °C / Inert atmosphere 4.2: 0 - 100 °C / Inert atmosphere View Scheme |
biphenyl-4-yl-phenyl-methanone
bifonazole
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: aluminum oxide; sodium tetrahydroborate / ethanol / 0.67 h / 20 °C / Inert atmosphere 2.1: triethylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere 3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 0 °C / Inert atmosphere 3.2: 0 - 100 °C / Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
Stage #1: 1H-imidazole With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃; for 2h; Inert atmosphere; Stage #2: [1,1'-biphenyl]-4-yl(phenyl)methyl methanesulfonate In N,N-dimethyl-formamide; mineral oil at 0 - 100℃; Inert atmosphere; | 61.9 mg |
Diphenylmethane
bifonazole
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: dichloromethane / -40 - 20 °C / Schlenk technique; Inert atmosphere 2: bis(tri-t-butylphosphine)palladium(0); sodium hydrogencarbonate / dichloromethane; N,N-dimethyl-formamide / 12 h / 50 °C / Inert atmosphere; Schlenk technique 3: 2,2'-azobis(isobutyronitrile); N-Bromosuccinimide / tetrachloromethane / 0.83 h / Inert atmosphere; Reflux 4: potassium carbonate / acetonitrile / 1 h / Reflux View Scheme | |
Multi-step reaction with 3 steps 1.1: dichloromethane / -40 - 20 °C / Inert atmosphere; Schlenk technique 2.1: sodium hydrogencarbonate; bis(tri-t-butylphosphine)palladium(0) / dichloromethane; N,N-dimethyl-formamide / 12 h / 50 °C / Inert atmosphere; Schlenk technique; Sealed tube 3.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 0.83 h / Inert atmosphere; Reflux 3.2: 1 h / Reflux View Scheme |
bifonazole
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: bis(tri-t-butylphosphine)palladium(0); sodium hydrogencarbonate / dichloromethane; N,N-dimethyl-formamide / 12 h / 50 °C / Inert atmosphere; Schlenk technique 2: 2,2'-azobis(isobutyronitrile); N-Bromosuccinimide / tetrachloromethane / 0.83 h / Inert atmosphere; Reflux 3: potassium carbonate / acetonitrile / 1 h / Reflux View Scheme |
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile for 1h; Reflux; | 47.9 mg |
4-benzylbiphenyl
bifonazole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 2,2'-azobis(isobutyronitrile); N-Bromosuccinimide / tetrachloromethane / 0.83 h / Inert atmosphere; Reflux 2: potassium carbonate / acetonitrile / 1 h / Reflux View Scheme |
2-phenyl-4,4,5,5-tetramethyl-1,3,2-dioxoborole
bifonazole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sodium hydrogencarbonate; bis(tri-t-butylphosphine)palladium(0) / dichloromethane; N,N-dimethyl-formamide / 12 h / 50 °C / Inert atmosphere; Schlenk technique; Sealed tube 2.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 0.83 h / Inert atmosphere; Reflux 2.2: 1 h / Reflux View Scheme |
bifonazole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: tetrahydrofuran / 0.08 h / 20 °C / Schlenk technique; Inert atmosphere 1.2: 12.03 h / 70 °C / Schlenk technique; Inert atmosphere; Glovebox 2.1: iodine; pyridine; tert.-butylhydroperoxide / water; decane / 12 h / 80 °C / Schlenk technique; Inert atmosphere 2.2: 10 h / 180 - 200 °C / Schlenk technique; Inert atmosphere View Scheme |
p-benzylaniline
bifonazole
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: triethylamine / dichloromethane / 12.5 h / -78 - 20 °C / Schlenk technique; Inert atmosphere 2.1: tetrahydrofuran / 0.08 h / 20 °C / Schlenk technique; Inert atmosphere 2.2: 12.03 h / 70 °C / Schlenk technique; Inert atmosphere; Glovebox 3.1: iodine; pyridine; tert.-butylhydroperoxide / water; decane / 12 h / 80 °C / Schlenk technique; Inert atmosphere 3.2: 10 h / 180 - 200 °C / Schlenk technique; Inert atmosphere View Scheme |
tetrafluoroboric acid diethyl ether
sodium tetrafluoroborate
thianthrene-5-oxide
bifonazole
Conditions | Yield |
---|---|
Stage #1: tetrafluoroboric acid diethyl ether; thianthrene-5-oxide; bifonazole With trifluoroacetic anhydride In acetonitrile at 0 - 25℃; for 18h; Schlenk technique; Stage #2: sodium tetrafluoroborate In dichloromethane; water | 95% |
Ethyl 4-bromobenzoate
bifonazole
Conditions | Yield |
---|---|
With potassium acetate; palladium diacetate at 150℃; for 16h; Inert atmosphere; Schlenk technique; | 90% |
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid; 2,3,7,8-tetrafluorothianthrene; trifluoroacetic anhydride In acetonitrile at 0 - 25℃; regioselective reaction; | 87% |
Conditions | Yield |
---|---|
Stage #1: trifluorormethanesulfonic acid; 2,3,7,8-tetrafluorothianthrene-S-oxide; bifonazole With trifluoroacetic anhydride In acetonitrile at 0 - 25℃; for 3h; Sealed tube; Stage #2: sodium triflate In ethanol; dichloromethane; water | 87% |
4'-Bromopropiophenone
bifonazole
Conditions | Yield |
---|---|
With potassium acetate; palladium diacetate at 150℃; for 16h; Inert atmosphere; Schlenk technique; | 77% |
4-bromo-benzaldehyde
bifonazole
Conditions | Yield |
---|---|
With potassium acetate; palladium diacetate at 150℃; for 16h; Inert atmosphere; Schlenk technique; | 77% |
3-bromo-1-trifluoromethylbenzene
bifonazole
Conditions | Yield |
---|---|
With potassium acetate; palladium diacetate at 150℃; for 16h; Inert atmosphere; Schlenk technique; | 71% |
p-trifluoromethylphenyl bromide
bifonazole
Conditions | Yield |
---|---|
With potassium acetate; palladium diacetate at 150℃; for 16h; Inert atmosphere; Schlenk technique; | 66% |
Conditions | Yield |
---|---|
With trifluoroacetic anhydride In acetonitrile at -40 - 25℃; for 2h; Schlenk technique; Glovebox; Inert atmosphere; | 65% |
4-bromoisoquinoline
bifonazole
Conditions | Yield |
---|---|
With potassium acetate; palladium diacetate at 150℃; for 16h; Inert atmosphere; Schlenk technique; | 63% |
4-bromobenzenecarbonitrile
bifonazole
Conditions | Yield |
---|---|
With potassium acetate; palladium diacetate at 150℃; for 16h; Inert atmosphere; Schlenk technique; | 61% |
3-cyanobromobenzene
bifonazole
Conditions | Yield |
---|---|
With potassium acetate; palladium diacetate at 150℃; for 16h; Inert atmosphere; Schlenk technique; | 61% |
2-Acetyl-5-bromothiophene
bifonazole
Conditions | Yield |
---|---|
With potassium acetate; palladium diacetate at 150℃; for 16h; Inert atmosphere; Schlenk technique; | 59% |
o-cyanobromobenzene
bifonazole
Conditions | Yield |
---|---|
With potassium acetate; palladium diacetate at 150℃; for 16h; Inert atmosphere; Schlenk technique; | 58% |
para-bromotoluene
bifonazole
Conditions | Yield |
---|---|
With cesium acetate; palladium diacetate at 150℃; for 48h; Inert atmosphere; Schlenk technique; | A 58% B n/a |
1-bromo-4-methoxy-benzene
bifonazole
Conditions | Yield |
---|---|
With cesium acetate; palladium diacetate at 150℃; for 48h; Inert atmosphere; Schlenk technique; | A 57% B n/a |
bromobenzene
bifonazole
Conditions | Yield |
---|---|
With cesium acetate; palladium diacetate at 150℃; for 48h; Inert atmosphere; Schlenk technique; | A 55% B n/a |
bifonazole
Conditions | Yield |
---|---|
With air In chloroform treatment of Co-complex with rac-bifonazole; XRD, UV-Vis; | 46% |
o-trifluoromethylphenyl bromide
bifonazole
Conditions | Yield |
---|---|
With potassium acetate; palladium diacetate at 150℃; for 16h; Inert atmosphere; Schlenk technique; | 45% |
3-Chloropyridine
bifonazole
Conditions | Yield |
---|---|
With potassium acetate; palladium diacetate at 150℃; for 16h; Inert atmosphere; Schlenk technique; | 45% |
bifonazole
para-nitrophenyl bromide
Conditions | Yield |
---|---|
With potassium acetate; palladium diacetate at 150℃; for 16h; Inert atmosphere; Schlenk technique; | 43% |
1-Bromonaphthalene
bifonazole
Conditions | Yield |
---|---|
With potassium acetate; palladium diacetate at 150℃; for 16h; Inert atmosphere; Schlenk technique; | 42% |
5-bromopyrimidine
bifonazole
Conditions | Yield |
---|---|
With potassium acetate; palladium diacetate at 150℃; for 16h; Inert atmosphere; Schlenk technique; | 41% |
2-bromonaphthalene
bifonazole
Conditions | Yield |
---|---|
With potassium acetate; palladium diacetate at 150℃; for 16h; Inert atmosphere; Schlenk technique; | 39% |
1-bromo-4-tert-butylbenzene
bifonazole
Conditions | Yield |
---|---|
With potassium acetate; palladium diacetate at 150℃; for 16h; Inert atmosphere; Schlenk technique; | 34% |
1,2-(methylenedioxy)-4-bromobenzene
bifonazole
Conditions | Yield |
---|---|
With potassium acetate; palladium diacetate at 150℃; for 16h; Inert atmosphere; Schlenk technique; | 28% |
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