As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:617-84-5
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inquiryProduct description: Product name N,N-Diethylformamide CAS number 617-84-5 Assay ≥99% Appearance Colorless liquid Capacity 200mt/year Application Organic intermediate
Cas:617-84-5
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inquiryColorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on
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inquiryN,N-Diethylformamide with good quality and competitive price from Henan Tianfu Chemical: Henan Tianfu Chemical Co.,LTD was built in 2009 with an ISO certificate in the past 5 years, we have grown up as a famous fine chemicals supplier in china an
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
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inquiryAntimex Chemical Limied, was founded in 2001, we are specializing in manufacturing & researching of Active pharmaceutical Ingredients,Veterinary pharm APIs,cosmetic ingredients,and Intermediates. food additives,water treatment chemicals. Fluori
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inquiryN,N-Diethyl formamide (DEF) N, N-diethyl methylamine materialized properties Density: 0.908 g/mL at 25 degrees C (lit.) Boiling point: 176-177 degrees C (lit.) Melting point: 176-177 degrees C Flash point: 141 degrees F Refractive index: n20/D 1
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Cas:617-84-5
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inquiryN,N-Diethylformamide CAS:617-84-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interm
Cas:617-84-5
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Cas:617-84-5
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inquirysuperior quality moderate price & quick delivery Appearance:clear colorless to pale yellow liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Appli
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The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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Cas:617-84-5
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Cas:617-84-5
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inquiryProduct name: N,N-Diethylformamide CAS No.: 617-84-5 Molecule Formula:C5H11NO Molecule Weight:101.15 Purity: 99.0% Package: 200kg/drum Description:Colorless transparent liquid Manufacture Standards:Enterprise Standard TESTING IT
Cas:617-84-5
Min.Order:1 Kilogram
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inquiryChemical Name: N,N-Diethylformamide Molecular Fomula:C5H11NO Appearance: Yellow Liquid Appearance:Colorless Clear to light yellow Liquid Storage:Preserve in well-closed, light-resistant and airtight containers. Package:25KG/Drum Application:Agroch
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N,N-Diethylformamide Chemical Properties Melting point 176-177°C Boiling point 176-177 °C (lit.) density 0.908 g/mL at 25 °C (lit.) refractive index n20/D 1.434(lit.) Fp 141 °F storage temp. Store below +30°
Cas:617-84-5
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:617-84-5
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Type:Trading Company
inquiryConditions | Yield |
---|---|
With C21H24N2; phenylsilane In tetrahydrofuran at 20℃; under 750.075 - 2250.23 Torr; for 1.5h; Solvent; Concentration; Reagent/catalyst; Temperature; Time; Inert atmosphere; Glovebox; | 100% |
With phenylsilane at 25℃; under 37503.8 Torr; for 12h; Pressure; Temperature; Autoclave; | 100% |
With Zn(salen); phenylsilane; tetrabutylammomium bromide at 25℃; under 3750.38 Torr; for 15h; Reagent/catalyst; Autoclave; | 99% |
Conditions | Yield |
---|---|
With potassium tetrachloroaurate(III); potassium carbonate In water; acetonitrile at 40℃; for 12h; | 98% |
With sodium hydroxide In water at 25℃; for 6h; | 91% |
With potassium iodide In water Ambient temperature; electrolysis; | 85% |
N-<(trimethylsilyl)methyl>-N,N-diethylamine
N-formyldiethylamine
Conditions | Yield |
---|---|
With copper(I) bromide In acetonitrile at 25℃; for 4h; chemoselective reaction; | 94% |
Conditions | Yield |
---|---|
With Thiamine hydrochloride at 80℃; for 0.5h; | 90% |
With sulfated polyborate In neat (no solvent) at 70℃; for 0.333333h; | 86% |
With silica gel for 0.0236111h; microwave irradiation; | 80% |
N-formyldiethylamine
Conditions | Yield |
---|---|
With hydrogenchloride; diethyl ether In diethyl ether at -78℃; for 0.5h; | 85% |
Conditions | Yield |
---|---|
With Cu/Al2O3; dihydrogen peroxide In water at 25℃; for 24h; Green chemistry; | 83% |
4-tert-butyl-2-(2-nitrophenylazo)phenol
A
2-Methyl-1H-benzimidazole
B
N-formyldiethylamine
C
2-(5-tert-butyl-2-hydroxyphenyl)benzotriazole
D
2-nitro-aniline
Conditions | Yield |
---|---|
With carbon monoxide; triethylamine In 1,2-dichloro-benzene at 200℃; under 60800 Torr; for 8h; Further byproducts given; | A n/a B n/a C 63% D 82% |
bis(diethylamin)nickeldibromid
diethylamine
A
N-formyldiethylamine
B
N,N,N',N'-tetraethylurea
C
N,N,N',N'-tetraethyloxamide
D
diethylamine hydrobromide
E
tetracarbonyl nickel
Conditions | Yield |
---|---|
With carbon monoxide In tetrahydrofuran; diethyl ether reaction in THF/Et2O = 2/1 soln., room temp., under CO (1 bar); | A 7% B 0.5% C 80% D n/a E n/a |
Conditions | Yield |
---|---|
With manganese(IV) oxide; oxygen In chlorobenzene at 100℃; under 4500.45 Torr; for 4h; Autoclave; Green chemistry; | 80% |
With Eosin Y In ethanol at 23℃; Irradiation; | 16% |
With pyridine; copper(II) bis(trifluoromethanesulfonate) In acetonitrile at 130℃; under 7500.75 - 30003 Torr; Catalytic behavior; Reagent/catalyst; Pressure; Temperature; Autoclave; |
Conditions | Yield |
---|---|
Ambient temperature; | 78% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 0.15h; | 78% |
trimethylsilyl formate
(diethylamino)triethylsilane
A
N-formyldiethylamine
B
Hexamethyldisiloxane
C
1,1,1-triethyl-3,3,3-trimethyl-disiloxane
D
hexaethyl disiloxane
Conditions | Yield |
---|---|
With N-Methylformamide at 20℃; for 2h; | A 72.5% B 13.6% C n/a D 23.8% |
With N-Methylformamide at 20℃; for 2h; Product distribution; Mechanism; various amides as catalysts, other temperature, other time; | A 72.5% B 13.6% C n/a D 23.8% |
trimethylsilyl formate
A
N-formyldiethylamine
B
Hexamethyldisiloxane
C
1,1,1-triethyl-3,3,3-trimethyl-disiloxane
D
hexaethyl disiloxane
Conditions | Yield |
---|---|
With N-Methylformamide; (diethylamino)triethylsilane at 20℃; for 2h; | A 72.5% B 13.6% C n/a D 23.8% |
(diethylamino)triethylsilane
A
N-formyldiethylamine
B
Hexamethyldisiloxane
C
1,1,1-triethyl-3,3,3-trimethyl-disiloxane
D
hexaethyl disiloxane
Conditions | Yield |
---|---|
With N-Methylformamide; trimethylsilyl formate at 20℃; for 2h; | A 72.5% B 13.6% C n/a D 23.8% |
Conditions | Yield |
---|---|
With dioxo[bis(sulfato-κO)]molybdenum In ethanol for 5h; Reflux; Green chemistry; | 70% |
diethylamine
2,2-Dichloro-3-oxo-butyraldehyde
A
N-formyldiethylamine
B
1,1-Dichloroacetone
Conditions | Yield |
---|---|
In tetrachloromethane for 12h; Ambient temperature; | A 68% B 60% |
carbon monoxide
diethylamine
A
N-formyldiethylamine
B
N,N,N',N'-tetraethylurea
C
N,N,N',N'-tetraethyloxamide
Conditions | Yield |
---|---|
With (Et2NH)2CuBr; (Et2NH)2NiBr In tetrahydrofuran under 15001.2 Torr; for 16h; Ambient temperature; | A n/a B n/a C 66% |
carbon monoxide
diethylamine
A
N-formyldiethylamine
B
N,N,N',N'-tetraethyloxamide
Conditions | Yield |
---|---|
With (Et2NH)2CuBr; (Et2NH)2NiBr In tetrahydrofuran under 15001.2 Torr; for 16h; Ambient temperature; | A n/a B 66% |
Conditions | Yield |
---|---|
With copper(l) iodide; N,N,N,N,-tetramethylethylenediamine; oxygen In dimethyl sulfoxide at 100℃; for 24h; Sealed tube; | A n/a B 66% |
Conditions | Yield |
---|---|
With sodium ethanolate at 50℃; Riemer-Tiemann reaction; Inert atmosphere; | 62% |
With potassium tert-butylate; water; benzene | |
With sodium hydroxide |
Conditions | Yield |
---|---|
In ethyl acetate for 1h; Ambient temperature; | 62% |
sec.-butyllithium
N,N-diethylcarbamyl chloride
A
N-formyldiethylamine
B
2-methyl-butyric acid diethylamide
Conditions | Yield |
---|---|
Stage #1: sec.-butyllithium With CuCN In tetrahydrofuran at -30℃; for 0.5h; Stage #2: N,N-diethylcarbamyl chloride In tetrahydrofuran at -30 - 0℃; for 2h; | A 11 % Chromat. B 62% |
N,N-diethylthioformamide
N-formyldiethylamine
Conditions | Yield |
---|---|
With triphenyltin(IV) hydroxide In benzene-d6 at 90℃; for 8h; | 60% |
Conditions | Yield |
---|---|
With tetracarbonyl nickel In toluene at 180℃; for 24h; | 55% |
With 1,3-bis-(2,6-diisopropylphenyl)-imidazol-2-ylidene In methanol at 0 - 130℃; under 22502.3 Torr; for 36h; Autoclave; | 12.1% |
In tetrahydrofuran under 760 Torr; for 24h; Product distribution; Mechanism; Ambient temperature; other conditions: other catalyst, other times, addition of complexing agents, addition of LiBr; |
diethylamine
A
N-formyldiethylamine
B
(1E,2E)-N,3-diphenylprop-2-en-1-imine
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran at 0℃; for 3h; | A 50% B n/a |
carbon monoxide
acetylene
A
4-butanolide
B
N-formyldiethylamine
C
tetraethyl-butynediamide
D
N,N-diethylpropiolamide
Conditions | Yield |
---|---|
In tetrahydrofuran; diethyl ether under 750.06 Torr; Ambient temperature; | A 8.9 % Chromat. B 2.4 % Chromat. C 45% D 11% |
Conditions | Yield |
---|---|
12% |
Conditions | Yield |
---|---|
durch folgendes Erwaermen; |
N-formyldiethylamine
1,1-dichloromethyl-N,N-diethylamine
Conditions | Yield |
---|---|
With thionyl chloride In dichloromethane at 20℃; for 2h; Inert atmosphere; | 100% |
With (pentachloroethyl)phosphorimidic trichloride In benzene |
N-formyldiethylamine
(tert-butyldimethylsilyl)(phenyl)methanone
N-(p-methoxybenzylidene)diphenylphosphinamide
Conditions | Yield |
---|---|
Stage #1: N-formyldiethylamine; (tert-butyldimethylsilyl)(phenyl)methanone With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 0.333333h; Brook Silaketone Rearrangement; Inert atmosphere; Schlenk technique; Stage #2: N-(p-methoxybenzylidene)diphenylphosphinamide In tetrahydrofuran at -78℃; for 0.5h; Brook Silaketone Rearrangement; Inert atmosphere; Schlenk technique; diastereoselective reaction; | 100% |
N-formyldiethylamine
N-(p-methoxybenzylidene)diphenylphosphinamide
Conditions | Yield |
---|---|
Stage #1: N-formyldiethylamine; tert-butyldimethylsilyl 4-fluorophenyl ketone With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 0.333333h; Brook Silaketone Rearrangement; Inert atmosphere; Schlenk technique; Stage #2: N-(p-methoxybenzylidene)diphenylphosphinamide In tetrahydrofuran at -78℃; for 0.5h; Brook Silaketone Rearrangement; Inert atmosphere; Schlenk technique; diastereoselective reaction; | 100% |
N-formyldiethylamine
N-(p-methoxybenzylidene)diphenylphosphinamide
Conditions | Yield |
---|---|
Stage #1: N-formyldiethylamine; C17H28OSi With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 0.333333h; Brook Silaketone Rearrangement; Inert atmosphere; Schlenk technique; Stage #2: N-(p-methoxybenzylidene)diphenylphosphinamide In tetrahydrofuran at -78℃; for 0.5h; Brook Silaketone Rearrangement; Inert atmosphere; Schlenk technique; diastereoselective reaction; | 100% |
N-formyldiethylamine
N-(p-methoxybenzylidene)diphenylphosphinamide
Conditions | Yield |
---|---|
Stage #1: N-formyldiethylamine; C15H24OSi With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 0.333333h; Brook Silaketone Rearrangement; Inert atmosphere; Schlenk technique; Stage #2: N-(p-methoxybenzylidene)diphenylphosphinamide In tetrahydrofuran at -78℃; for 0.5h; Brook Silaketone Rearrangement; Inert atmosphere; Schlenk technique; diastereoselective reaction; | 100% |
N-formyldiethylamine
ethyl acetoacetate
3-diethylcarbamoyloxybut-2-enoic acid ethyl ester
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; copper(l) chloride In water at 20 - 70℃; for 0.75h; Green chemistry; stereoselective reaction; | 99% |
With tert.-butylhydroperoxide; copper nanoparticles on black carbon In water; N,N-dimethyl-formamide at 80℃; for 5h; Inert atmosphere; | 80% |
With tert.-butylhydroperoxide In water at 80℃; for 4h; Inert atmosphere; stereoselective reaction; | 70% |
With tert.-butylhydroperoxide; copper(ll) bromide In water at 80℃; for 3h; stereoselective reaction; | 68% |
With tert.-butylhydroperoxide; copper(II) oxide In water at 20℃; for 4h; Sonication; |
N-formyldiethylamine
o-hydroxyacetophenone
diethylcarbamic acid 2-acetylphenyl ester
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; copper(l) chloride In water at 20 - 70℃; for 0.75h; Green chemistry; | 99% |
With tert.-butylhydroperoxide at 70℃; for 0.5h; | 95% |
With tert.-butylhydroperoxide; copper diacetate In water at 80℃; for 3h; | 84% |
N-formyldiethylamine
ethyl 3-oxo-3-phenylpropionate
3-diethylcarbamoyloxy-3-phenylacrylic acid ethyl ester
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; copper(l) chloride In water at 20 - 70℃; for 0.75h; Green chemistry; stereoselective reaction; | 99% |
With tert.-butylhydroperoxide; copper(ll) bromide In water at 80℃; for 3h; stereoselective reaction; | 80% |
N-formyldiethylamine
acetoacetic acid methyl ester
3-diethylcarbamoyloxybut-2-enoic acid methyl ester
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; copper(l) chloride In water at 20 - 70℃; for 0.5h; Green chemistry; stereoselective reaction; | 99% |
With tert.-butylhydroperoxide; copper nanoparticles on black carbon In water; N,N-dimethyl-formamide at 80℃; for 5h; Inert atmosphere; | 84% |
With tert.-butylhydroperoxide; copper(ll) bromide In water at 80℃; for 3h; stereoselective reaction; | 66% |
With tert.-butylhydroperoxide; copper(II) oxide In water at 20℃; for 4h; Sonication; |
N-formyldiethylamine
1-Chloromethylnaphthalene
1-<(N,N-diethylamino)methyl>naphthalene
Conditions | Yield |
---|---|
With NHC-Pd(II)-Im; sodium hydroxide In water at 50℃; for 3h; Inert atmosphere; Schlenk technique; | 99% |
With potassium hydroxide In water at 50℃; for 3h; Green chemistry; | 85% |
N-formyldiethylamine
P,P-diphenyl-N-(phenylmethylene)phosphinic amide
(tert-butyldimethylsilyl)(phenyl)methanone
Conditions | Yield |
---|---|
Stage #1: N-formyldiethylamine; (tert-butyldimethylsilyl)(phenyl)methanone With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 0.333333h; Brook Silaketone Rearrangement; Inert atmosphere; Schlenk technique; Stage #2: P,P-diphenyl-N-(phenylmethylene)phosphinic amide In tetrahydrofuran at -78℃; for 0.5h; Brook Silaketone Rearrangement; Inert atmosphere; Schlenk technique; diastereoselective reaction; | 99% |
N-formyldiethylamine
toluene-4-sulfonamide
(E)-N'-((4-methylphenyl)sulfonyl)-N,N-diethylformimidamide
Conditions | Yield |
---|---|
With diazoacetic acid ethyl ester; zinc trifluoromethanesulfonate In cyclohexane for 12h; Reflux; stereoselective reaction; | 99% |
With thionyl chloride In chloroform at 60℃; for 3h; | 96% |
N-formyldiethylamine
4-chlorobenzo[d]thiazol-2-amine
N,N-diethyl-N',N''-bis(4-chloro-2-benzothiazolyl)triaminomethane
Conditions | Yield |
---|---|
With benzenesulfonyl chloride In pyridine | 98% |
N-formyldiethylamine
m-methoxybenzyl chloride
N,N-diethyl-3-(methoxyl)benzenemethanamine
Conditions | Yield |
---|---|
With NHC-Pd(II)-Im; sodium hydroxide In water at 50℃; for 3h; Inert atmosphere; Schlenk technique; | 98% |
With potassium hydroxide In water at 50℃; for 3h; Green chemistry; | 92% |
Conditions | Yield |
---|---|
With silver trifluoromethanesulfonate at 130℃; for 2h; Inert atmosphere; Schlenk technique; | 98% |
With silver hexafluoroantimonate In N,N-dimethyl-formamide at 80℃; for 20h; Inert atmosphere; | 86% |
Conditions | Yield |
---|---|
With ammonium iodide at 90℃; for 0.25h; Reagent/catalyst; Temperature; Time; Microwave irradiation; | 97% |
With iodine In neat (no solvent) at 80℃; for 2h; Schlenk technique; Green chemistry; | 80% |
N-formyldiethylamine
Conditions | Yield |
---|---|
With water In dichloromethane at 60℃; for 24h; | 97% |
N-formyldiethylamine
2-(2-methylbenzyl)benzoic acid
N,N-diethyl-2-(2-methylbenzyl)benzamide
Conditions | Yield |
---|---|
With thionyl chloride for 20h; | 96% |
4,4'-benzene-1,4-diylbis(1H-pyrazole)
N-formyldiethylamine
Conditions | Yield |
---|---|
In further solvent(s) mixt. Co(OTf)2, 1,4-benzenedipyridyl and HCONEt2 in sealed evacuated tube was heated at 150°C for 6 days; ppt. was filtered, washed with HCONEt2 and dried in vacuo for 30 min; elem. anal.; | 95% |
In further solvent(s) react. in N,N-diethylformamide at 130°C; |
N-formyldiethylamine
benzene-1,3,5-tricarboxylic acid
tetraethylammonium bromide
Conditions | Yield |
---|---|
In further solvent(s) C6H3(COOH)3, (C2H5)4NBr, In(NO3)3*xH2O in N,N-diethylformamide was heated at 120°C for 4 days, cooled to room temp.; washed with ethanol; elem. anal.; | 95% |
N-formyldiethylamine
Dimethylphenylsilane
phenyldimethylsilyloxymethyldiethylamine
Conditions | Yield |
---|---|
With CpMn(CO)3 for 16h; Irradiation; | 95% |
N-formyldiethylamine
N-(p-methoxybenzylidene)diphenylphosphinamide
Conditions | Yield |
---|---|
Stage #1: N-formyldiethylamine; (tert-butyldimethylsilyl)(naphthalen-2-yl)methanone With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 0.333333h; Brook Silaketone Rearrangement; Inert atmosphere; Schlenk technique; Stage #2: N-(p-methoxybenzylidene)diphenylphosphinamide In tetrahydrofuran at -78℃; for 0.5h; Brook Silaketone Rearrangement; Inert atmosphere; Schlenk technique; diastereoselective reaction; | 95% |
Conditions | Yield |
---|---|
With lithium diisopropyl amide In tetrahydrofuran at 25℃; for 0.0166667h; | 95% |
1,3-Benzothiazole
N-formyldiethylamine
N,N-diethylbenzo[d]thiazol-2-amine
Conditions | Yield |
---|---|
With silver(I) acetate; sodium t-butanolate In neat (no solvent) at 120℃; for 5h; Inert atmosphere; | 95% |
N-formyldiethylamine
3-Phenylpropionic acid
N,N-diethyl-3-phenylpropanamide
Conditions | Yield |
---|---|
With sulfur trioxide pyridine complex at 160℃; Schlenk technique; Inert atmosphere; | 95% |
N-formyldiethylamine
N-(1-phenyl)sulfamide
Conditions | Yield |
---|---|
With trichlorophosphate In dichloromethane at 40℃; for 9h; | 95% |
4,4'-bis-(1H-imidazol-1-yl)biphenyl
N-formyldiethylamine
2′,3′,5′,6′-tetramethyl(1,1′:4′,1″-terphenyl)-4,4″-dicarboxylic acid
Conditions | Yield |
---|---|
at 120℃; for 24h; Sealed tube; | 95% |
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