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Cas:827-94-1
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inquiryStock products, own laboratory Product number 35650 English Name 2,6-Dibromo-4-nitroaniline CAS Number 827-94-1 Purity 98% Molecular form
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inquiryProduct Description Product website: http://www.finerchem.com/pro01en/id/1813.html Product Name 2,6-Dibromo-4-nitroaniline CAS No. 827-94-1
Cas:827-94-1
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inquiry2,6-Dibromo-4-nitroaniline CAS: 827-94-1 Specification Product name 2,6-Dibromo-4-nitroaniline CAS No.: 827-94-1 molecular formula: C6H4Br2N2O2 Molecular Weight: 295.92 Purity
Cas:827-94-1
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inquiryProduct name: 2,6-Dibromo-4-Nitroaniline CAS No.:827-94-1 Molecule Formula:C6H4Br2N2O2 Molecule Weight:295.91 Purity: 98% Package: 25kg/bag Description:Yellow powder Manufacture Standards:Enterprise Standard TESTING ITEMS
Cas:827-94-1
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inquiry2,6-Dibromo-4-nitroaniline Basic information Product Name: 2,6-Dibromo-4-nitroaniline Synonyms: TIMTEC-BB SBB007584;2,6-dibromo-4-nitro-anilin;2,6-dibromo-4-nitro-benzenamin;2,6-Dibromo-4-nitroaniL;AKOS B015999;2,6-DIBROMO-P-NITROANILINE;2,6-D
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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Conditions | Yield |
---|---|
With bromine In acetic acid | 98% |
With N-Bromosuccinimide; lithium perchlorate; silica gel In dichloromethane at 20℃; for 0.0833333h; | 98% |
With hydrogenchloride; brominating reagent In dichloromethane; water at 28℃; for 0.75 - 1h; | 98.7% |
2-bromo-4-nitroaniline
2,6-dibromo-4-nitroaniline
Conditions | Yield |
---|---|
With bromine In tetrachloromethane at 20℃; Cooling with ice; | 87% |
With bromine; acetic acid |
Conditions | Yield |
---|---|
With dihydrogen peroxide; potassium bromide In water; acetonitrile | A 13% B 84% |
With N-Bromosuccinimide In water at 20℃; for 8h; | |
With sodium persulfate; copper(ll) sulfate pentahydrate; sodium bromide In water; acetonitrile at 7 - 25℃; for 24h; Overall yield = 98 percent; Overall yield = 1.5 g; regioselective reaction; | A 2 %Chromat. B 98 %Chromat. |
2,6-dibromo-N-nitroaniline
2,6-dibromo-4-nitroaniline
Conditions | Yield |
---|---|
With trifluoroacetic acid-d1 In chloroform-d1 at 30℃; Rate constant; Mechanism; kinetic isotope effect; | |
With sulfuric acid; acetic acid |
2,6-dibromo-N-nitroaniline
A
2,6-dibromo-4-nitroaniline
B
2,4-dibromo-6-nitroaniline
Conditions | Yield |
---|---|
With hydrogenchloride; ethanol | |
With hydrogenchloride; acetic acid | |
With sulfuric acid; acetic acid | |
With ethanol; sulfuric acid |
2,4,6-tribromo-N-nitro-aniline
2,6-dibromo-4-nitroaniline
Conditions | Yield |
---|---|
With sulfuric acid; acetic acid at 20 - 30℃; |
2,4,6-tribromo-N-nitro-aniline
A
2,6-dibromo-4-nitroaniline
B
2,4-dibromo-6-nitroaniline
Conditions | Yield |
---|---|
With hydrogenchloride; water | |
With sulfuric acid; water | |
With ethanol; sulfuric acid |
1,3-dibromo-2-methoxy-5-nitrobenzene
2,6-dibromo-4-nitroaniline
Conditions | Yield |
---|---|
With ethanol; ammonia at 180℃; |
Conditions | Yield |
---|---|
With ethanol; ammonia at 150℃; |
2,4,6-tribromoaniline
A
2,4,6-tribromo-N-nitro-aniline
B
2,6-dibromo-4-nitroaniline
Conditions | Yield |
---|---|
With nitric acid; acetic acid |
Conditions | Yield |
---|---|
With nitric acid; acetic acid |
bromine
4-nitro-aniline
A
2,6-dibromo-4-nitroaniline
B
2-bromo-4-nitroaniline
2,4,6-tribromo-N-nitro-aniline
sulfuric acid
acetic acid
2,6-dibromo-4-nitroaniline
Conditions | Yield |
---|---|
wendet man die Schwefelsaeure in geringer Verduennung an; | |
at 20 - 30℃; |
2,6-dibromo-N-nitroaniline
A
2,6-dibromo-4-nitroaniline
B
2,4-dibromo-6-nitroaniline
hydrogenchloride
ethanol
2,4,6-tribromo-N-nitro-aniline
A
2,6-dibromo-4-nitroaniline
B
2,4-dibromo-6-nitroaniline
C
bromine
hydrogenchloride
2,4,6-tribromo-N-nitro-aniline
water
A
2,6-dibromo-4-nitroaniline
B
2,4-dibromo-6-nitroaniline
C
bromine
hydrogenchloride
2,4,6-tribromo-N-nitro-aniline
acetic acid
A
2,6-dibromo-4-nitroaniline
B
2,4-dibromo-6-nitroaniline
C
bromine
2,6-dibromo-4-nitroaniline
Conditions | Yield |
---|---|
With hydrogenchloride |
1,3-dibromo-2-methoxy-5-nitrobenzene
ammonia
2,6-dibromo-4-nitroaniline
Conditions | Yield |
---|---|
at 180℃; |
Conditions | Yield |
---|---|
at 120℃; |
2,4,6-tribromoaniline
nitric acid
acetic acid
A
2,4,6-tribromo-N-nitro-aniline
B
2,6-dibromo-4-nitroaniline
Conditions | Yield |
---|---|
und Erwaermen 20-30 Minuten auf dem Wasserbade; |
Conditions | Yield |
---|---|
With ethanol; sulfuric acid |
2-bromo-4-nitroaniline
bromine
acetic acid
2,6-dibromo-4-nitroaniline
nitroaminophenylarsonic acid
2,6-dibromo-4-nitroaniline
2,6-dibromo-4-nitroaniline
4-methylphenylboronic acid
2,6-bis(4-methylphenyl)-4-nitroaniline
Conditions | Yield |
---|---|
With potassium phosphate tribasic heptahydrate; palladium diacetate In water; N,N-dimethyl-formamide at 80℃; for 0.25h; Suzuki Coupling; | 99% |
2,6-dibromo-4-nitroaniline
4-fluoroboronic acid
2,6-bis(4-fluorophenyl)-4-nitroaniline
Conditions | Yield |
---|---|
With potassium phosphate tribasic heptahydrate; palladium diacetate In water; N,N-dimethyl-formamide at 80℃; for 0.333333h; Suzuki Coupling; | 99% |
2,6-dibromo-4-nitroaniline
4-formylphenylboronic acid,
2,6-bis(4-formylphenyl)-4-nitroaniline
Conditions | Yield |
---|---|
With potassium phosphate tribasic heptahydrate; palladium diacetate In water; N,N-dimethyl-formamide at 80℃; for 1h; Suzuki Coupling; | 98% |
Conditions | Yield |
---|---|
With sulfuric acid; sodium nitrite In ethanol | 97% |
With sulfuric acid; sodium nitrite In ethanol for 3h; Heating; | 94% |
With sulfuric acid; sodium nitrite In ethanol for 3.25h; Heating / reflux; | 93% |
2,6-dibromo-4-nitroaniline
1,4-diamino-3,5-dibromobenzene
Conditions | Yield |
---|---|
Stage #1: 2,6-dibromo-4-nitroaniline With tin(ll) chloride In tetrahydrofuran; ethanol at 50℃; for 16h; Inert atmosphere; Stage #2: With sodium hydroxide In tetrahydrofuran; ethanol at 25℃; for 2.5h; Inert atmosphere; | 97% |
With hydrazine hydrate; Ru-carbon In ethanol for 2h; Heating; | 95% |
With iron; acetic acid at 20℃; Inert atmosphere; | 80% |
Conditions | Yield |
---|---|
With acetic acid; isopentyl nitrite at 0 - 5℃; | 97% |
2,6-dibromo-4-nitroaniline
(3,4-difluorophenyl)boronic acid
2,6-bis(3,4-difluorophenyl)-4-nitroaniline
Conditions | Yield |
---|---|
With potassium phosphate tribasic heptahydrate; palladium diacetate In water; N,N-dimethyl-formamide at 80℃; for 0.416667h; Suzuki Coupling; | 97% |
2,6-dibromo-4-nitroaniline
2-Bromoacetyl bromide
2-bromo-N-(2,6-dibromo-4-nitrophenyl)acetamide
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20 - 60℃; | 96% |
2,6-dibromo-4-nitroaniline
phenylboronic acid
5'-nitro-1,1':3',1''-terphenyl-2'-ylamine
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In 1,2-dimethoxyethane; ethanol; water for 14h; Heating; | 95% |
With potassium phosphate tribasic heptahydrate; palladium diacetate In water; N,N-dimethyl-formamide at 80℃; for 1h; Suzuki Coupling; | 94% |
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In ethanol; benzene for 48h; Suzuki reaction; Heating; | 55% |
2,6-dibromo-4-nitroaniline
4-tert-butylphenylboronic acid
Conditions | Yield |
---|---|
With tetrabutylammomium bromide; palladium diacetate; sodium carbonate In water at 150℃; for 0.5h; Suzuki Coupling; Inert atmosphere; | 94% |
2,6-dibromo-4-nitroaniline
4-n-methylphenylacetylene
4-nitro-2,6-bis-p-tolylethynyl-phenylamine
Conditions | Yield |
---|---|
With triethylamine; tetrakis(triphenylphosphine) palladium(0) In benzene at 70℃; for 22h; Sonogashira coupling; | 92% |
Conditions | Yield |
---|---|
Stage #1: 2,6-dibromo-4-nitroaniline With tert.-butylnitrite; naphthalene-1,5-disulfonate In 1,2-dimethoxyethane at 20℃; for 1h; Stage #2: m-acetylamino-N,N-diethylanilne With sodium carbonate; naphthalene-1,5-disulfonate In water at 0℃; for 0.166667h; pH=4 - 6; | 90.45% |
Stage #1: 2,6-dibromo-4-nitroaniline With naphthalene-1,5-disulfonate In ethyl acetate at 50℃; for 0.166667h; Stage #2: With tert.-butylnitrite In ethyl acetate at 25℃; for 0.333333h; Stage #3: m-acetylamino-N,N-diethylanilne With hydrogenchloride In water at 0 - 5℃; for 0.1h; |
2,6-dibromo-4-nitroaniline
Conditions | Yield |
---|---|
With tetrafluoroboric acid; acetic acid; isopentyl nitrite In water at 20℃; for 0.0833333h; | 89% |
Conditions | Yield |
---|---|
With indium; acetic acid In toluene at 80℃; for 6h; Inert atmosphere; | A 88% B 2% |
2,6-dibromo-4-nitroaniline
1,3-dibromo-2,5-dinitrobenzene
Conditions | Yield |
---|---|
With dihydrogen peroxide; trifluoroacetic acid at 72℃; for 0.5h; | 85% |
With dihydrogen peroxide; trifluoroacetic acid |
2,6-dibromo-4-nitroaniline
1,3-dibromo-2-iodo-5-nitrobenzene
Conditions | Yield |
---|---|
Stage #1: 2,6-dibromo-4-nitroaniline With sulfuric acid; sodium nitrite In acetic acid at 20℃; for 4h; Stage #2: With iodine; potassium iodide In water; acetic acid at 20℃; for 12h; | 80% |
With nitrosylsulfuric acid; sulfuric acid Diazotization.Behandlung der Diazoniumsalz-Loesung mit KI in Wasser; | |
ueber die Diazoverbindung; | |
With sulfuric acid; acetic acid Diazotization.Behandlung der Diazoniumsalz-Loesung mit KI in Wasser; | |
Multi-step reaction with 3 steps 1: 97 percent / i-pentyl nitrite; HOAc / 0 - 5 °C 2: 94 percent / aq. NaOH / 0.5 h / 0 - 5 °C 3: 79 percent / aq. HI / acetonitrile / 13 h / 60 °C View Scheme |
2,6-dibromo-4-nitroaniline
(1R,2R)-N,N-dimethylcyclohexane-1,2-diamine
1,1'-carbonyldiimidazole
C15H20Br2N4O3
Conditions | Yield |
---|---|
Stage #1: 2,6-dibromo-4-nitroaniline With potassium hydride In tetrahydrofuran at 0℃; for 0.25h; Inert atmosphere; Stage #2: 1,1'-carbonyldiimidazole In tetrahydrofuran; 1,4-dioxane at 0 - 20℃; Inert atmosphere; Stage #3: (1R,2R)-N,N-dimethylcyclohexane-1,2-diamine In tetrahydrofuran; 1,4-dioxane at 20℃; for 20h; Inert atmosphere; | 80% |
2,6-dibromo-4-nitroaniline
2-(2'-anthraquinonylamino-3'-hydroxy)-4-anilino-6-chloro-s-triazine
C29H17Br2N7O5
Conditions | Yield |
---|---|
In nitrobenzene at 60 - 65℃; for 5h; | 80% |
Conditions | Yield |
---|---|
Stage #1: 2,6-dibromo-4-nitroaniline With hydrogen bromide; sodium nitrite In water at 0℃; for 2h; Stage #2: With urea for 0.333333h; Stage #3: With hydrogen bromide; copper(I) bromide at 0℃; for 2.25h; | 75% |
With nitric acid Diazotization.Faellen mit Brom-Bromkalium in Bromwasserstoffsaeure und Kochen des Reaktionsprodukts mit Alkohol; | |
With hydrogen bromide Behandeln mit Natriumnitrit; |
2,6-dibromo-4-nitroaniline
3,4,5-trifluorophenylboronic acid
2,6-bis(3,4,5-trifluorophenyl)-4-nitroaniline
Conditions | Yield |
---|---|
With potassium phosphate tribasic heptahydrate; palladium diacetate In water; N,N-dimethyl-formamide at 80℃; for 0.333333h; Suzuki Coupling; | 75% |
2,6-dibromo-4-nitroaniline
2-bromo-p-phenylenediamine
Conditions | Yield |
---|---|
With ammonium chloride; zinc In ethanol for 12h; Heating; | 67% |
Conditions | Yield |
---|---|
Stage #1: 2-oxo-2H-chromene-3-carboxylic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 0.5h; Stage #2: 2,6-dibromo-4-nitroaniline With triethylamine In dichloromethane at 20℃; for 12h; | 66% |
Conditions | Yield |
---|---|
With indium; acetic acid In toluene for 8h; Inert atmosphere; Reflux; | 63% |
2-octadecyloxy-1-naphthol
2-Methylpentane
sulfuric acid
2,6-dibromo-4-nitroaniline
sodium acetate trihydrate
Conditions | Yield |
---|---|
With sodium acetate; sodium nitrite In dichloromethane; chloroform; phosphorus pentoxide; acetic acid | 55.5% |
Conditions | Yield |
---|---|
With magnesium sulfate; toluene-4-sulfonic acid In toluene for 24h; Paal-Knorr Pyrrole Synthesis; Reflux; Inert atmosphere; | 13% |
chloroform
2,6-dibromo-4-nitroaniline
A
2,6-Dibromo-4-nitrophenyl isocyanide
B
N-(2,6-Dibromo-4-nitrophenyl)formamide
Conditions | Yield |
---|---|
With potassium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; water In dichloromethane at 20℃; Addition; Hydrolysis; | A 8% B n/a |
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