Zhuozhou Wenxi import and Export Co., Ltd
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Cas:10025-93-1
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryQingdao Beluga Import and Export Co., LTD
Uranium(III) chloride. CAS:10025-93-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic in
Cas:10025-93-1
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryShandong Hanjiang Chemical Co., Ltd.
Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:10025-93-1
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co., Ltd.
Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:10025-93-1
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryHangzhou J&H Chemical Co., Ltd.
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:10025-93-1
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:10025-93-1
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryXi`an Eastling Biotech Co., Ltd.
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:Beijing or Guangzhou
Henan Tianfu Chemical Co., Ltd.
1.Our services：A.Supply sampleB.The packing also can be according the customers` requirmentC.Any inquiries will be replied within 24 hoursD.we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate.
Cas:10025-93-1
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryHebei Sankai Chemical Technology Co., Ltd
1. Product advantages? High purity, all above 98.5%, no impurities after dissolution? We will test each batch to ensure quality? OEM and private brand services designed for free? Various cap colors available? We can also provide MT1 peptide powder2.
Antimex Chemical Limied
Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Cas:10025-93-1
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryWuhan Circle Star Chem-medical Technology co.,Ltd.
good quality, competitive price, thoughtful after sale serviceAppearance:White to Off-White Solid Storage:Keep it in dry,shady and cool place Package:as your requirement Application:Pharma;Industry;Agricultural;chemical reaserch Transportation:by Sea
Henan Kanbei Chemical Co.,LTD
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Shanghai Chinqesen Biotechnology Co., Ltd.
Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen
ZHEJIANG JIUZHOU CHEM CO.,LTD
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Shanghai united Scientific Co.,Ltd.
United Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat
Cas:10025-93-1
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryShanghai Run-Biotech Co., Ltd.
Shanghai, Run-Biotech Co., Ltd is a leading domestic pharmaceutical, biopharmaceutical, and health care products R & D outsourcing services company. As an innovation-driven and customer-focused company, Run Biotech provides a broad and integrated por
Nanjing Raymon Biotech Co., Ltd.
Uranium chloride (UCl3)(8CI,9CI) Storage:keep in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/pharma intermediate Transportation:By Sea,by Air,By courier like DHL or Fedx. Port:Shanghai/Shenzhen
Chemical Co.Ltd
Uranium chloride (UCl3)(8CI,9CI)Appearance:Off white to slight yellow solid Storage:Stored in shaded, cool and dry places Package:1L 5L 10L 25L bottle Application:pharma intermediate Transportation:Handle with cares to avoid damaging the packages. Pr
Synthetic route
-
-
10026-10-5
uranium(IV) chloride
-
-
10025-93-1
uranium(III) chloride
| Conditions | Yield |
|---|---|
| With zinc redn. of UCl4 by metallic Zn at 450 to 480°C in vacuum;; | 86% |
| In neat (no solvent) on sublimation of UCl4, in part dissocn. and forming of UCl3 (not volatile ppte.);; | |
| With H redn. by hydrogen; using of absolutely pure H;; |
-
A
-
10025-93-1
uranium(III) chloride
| Conditions | Yield |
|---|---|
| In tetrahydrofuran Ar atm; 1 equiv. of amalgam, 20°C, 4.5 h; | A n/a B n/a C 85% |
-
-
265-49-6
benzocyclooctene
-
-
10026-10-5
uranium(IV) chloride
-
A
-
10025-93-1
uranium(III) chloride
-
B
-
87532-97-6
dibenzouranocene
| Conditions | Yield |
|---|---|
| With potassium In tetrahydrofuran under Ar; to a soln. of benzocyclooctatetraene potassium was added; mixt. stirred for 48 h, added to a soln. of UCl4 and refluxed for 2 days; evapn., washing a residue with hexane, extn. (THF); | A n/a B 20% |
| Conditions | Yield |
|---|---|
| In neat (no solvent) at 700°C for 7 days; |
| Conditions | Yield |
|---|---|
| in evacuated quartz tube at 1130 K for 1 h;; | |
| In neat (no solvent, solid phase) at 800°C for 7 d; | |
| In neat (no solvent) fused in evacuated ampule at 860-870°C for 1 h; slowly cooled, elem. anal.; | |
| In neat (no solvent) 400°C, several h; heating (615°C); |
| Conditions | Yield |
|---|---|
| In not given equilibrium; | |
| In not given equilibrium; |
-
-
82360-21-2
potassium 6,6-dimethylcyclohexadienide
-
-
10026-10-5
uranium(IV) chloride
-
A
-
10025-93-1
uranium(III) chloride
| Conditions | Yield |
|---|---|
| In tetrahydrofuran under Ar; evapn. of solvent, extn. (pentane), pentane evapd. off: (Me2C6H5)2; |
| Conditions | Yield |
|---|---|
| In neat (no solvent) at 250-300°C;; | |
| In neat (no solvent) at 250-300°C;; |
| Conditions | Yield |
|---|---|
| In neat (no solvent) byproducts: Ag; Ar atmosphere; heating (sealed tantalum crucible, 1172-1223 K); sublimation; |
-
-
10025-93-1
uranium(III) chloride
| Conditions | Yield |
|---|---|
| With zinc In hydrogenchloride on redn. of UO2Cl2 by Zn;; not isolated;; | |
| With Zn In hydrogenchloride on redn. of UO2Cl2 by Zn;; not isolated;; |
| Conditions | Yield |
|---|---|
| In neat (no solvent, solid phase) byproducts: LiCl; at 700°C for 7 d; |
-
-
10025-93-1
uranium(III) chloride
| Conditions | Yield |
|---|---|
| With H2; HCl In neat (no solvent) hydriding of metal (470 K), conversion to trichloride with gaseouc HCl (470 K); sublimation (ca. 1170 K); |
| Conditions | Yield |
|---|---|
| In melt byproducts: Cd; formation in LiCl-NaCl-CaCl2-BaCl2 melt (455°C, 30 min); not isolated; | |
| With LiCl; KCl In melt (Ar); in glove box; prepd. in LiCl-KCl melt at 773 K; ref.: D. S. Poa, Z. Tomczuk, R. K. Steunenberg. J. Electrochem. Soc.,135, 1161(1988); |
| Conditions | Yield |
|---|---|
| With H2 In neat (no solvent) hydriding metal with H2 at 473 K, converting it to UCl3 with HCl at 473 K; subliming under high vacuum at 1173 K; |
-
-
7647-01-0
hydrogenchloride
-
-
1333-74-0
hydrogen
-
A
-
10025-93-1
uranium(III) chloride
-
B
-
10026-10-5
uranium(IV) chloride
| Conditions | Yield |
|---|---|
| U reacted with hydrogen at 250°C to yield UH3, whichis dehydrogeated at 330°C in a stream of dry Ar, the obtained powder reacted with HCl gas at 250°C; |
| Conditions | Yield |
|---|---|
| on heating U3O8 in mixture with S2Cl2 vapor and S in excess;; | 0% |
| on heating U3O8 in mixture with S2Cl2 vapor and S in excess;; | 0% |
| Conditions | Yield |
|---|---|
| In hydrogenchloride Electrolysis; electrolysis of a soln. of UO3 in HCl (d: 1.12, 15%) in a stream of CO2 with diaphragma and Hg cathode (110V, 1.5 up to 2 A); liquid at anode: HCl (d: 1.12); when react. soln. is getting green brown colored: 0.75 up to 1A, further electrolysis untill; react. soln. is getting red colored; redn.;; | |
| In hydrogenchloride Electrolysis; electrolysis of a soln. of UO3 in HCl (d: 1.12, 15%) in a stream of CO2 with diaphragma and Hg cathode (110V, 1.5 up to 2 A); liquid at anode: HCl (d: 1.12); when react. soln. is getting green brown colored: 0.75 up to 1A, further electrolysis untill; react. soln. is getting red colored; redn.;; |
| Conditions | Yield |
|---|---|
| In not given Ar atm.; |
| Conditions | Yield |
|---|---|
| In not given react. at 523K, distn. of UCl4 at 813K; |
-
-
10025-93-1
uranium(III) chloride
| Conditions | Yield |
|---|---|
| In neat (no solvent) non-static high vac. system:heating slowly from 20-300 ° C, 1E-5 - 1E-7 Pa; | |
| With NH4Cl In neat (no solvent) moisture- and oxygen-free conditions, thermal high vac. decompn., in a sealed quartz tube, 1.5-fold excess of NH4Cl, pumped off to ca. 1E-6 Pa, 25-80°C for 7 h, temp. slowly raised to 400°C; elem. anal.; |
| Conditions | Yield |
|---|---|
| With hydrogenchloride uranium hydride heating with HCl forms UCl3 and UCl4 at 623-673 K; treated the sample with purified H2 at 600 to 793 the UCl4 impurity was converted into UCl3; treated the sample with purified H2 at 600 to 793 K the UCl4 impurity was converted into UCl3; characterized by X-ray diffraction and elem. anal.; |
-
-
10025-93-1
uranium(III) chloride
| Conditions | Yield |
|---|---|
| In tetrahydrofuran byproducts: AlCl3, benzene; decompn. in THF soln.; | |
| In tetrahydrofuran byproducts: AlCl3, benzene; decompn. in THF soln.; |
-
-
10025-93-1
uranium(III) chloride
| Conditions | Yield |
|---|---|
| In neat (no solvent) in non-static vac. (1-10*0.000001 kPa), temp. increasing from 20 to 300°C; |
-
-
10025-93-1
uranium(III) chloride
| Conditions | Yield |
|---|---|
| byproducts: water; heating the UCl3*7H2O dimer in a non-static high vacuum system at 25, 60 and 100°C, final heat treatment at about 200°C; IR spectroscopy; |
| Conditions | Yield |
|---|---|
| In gas byproducts: Ca(g); 1967 - 2181 K; mass spectrometry; |
-
-
10025-93-1
uranium(III) chloride
| Conditions | Yield |
|---|---|
| In neat (no solvent) byproducts: water; 600 - 700 K, vac.; |
-
-
10025-93-1
uranium(III) chloride
| Conditions | Yield |
|---|---|
| In neat (no solvent) byproducts: water; 600 - 700 K, vac.; |
-
-
10025-93-1
uranium(III) chloride
| Conditions | Yield |
|---|---|
| In neat (no solvent) byproducts: water; 600 - 700 K, vac.; |
-
-
10025-93-1
uranium(III) chloride
| Conditions | Yield |
|---|---|
| In neat (no solvent) byproducts: water; 600 - 700 K, vac.; |
-
-
10025-93-1
uranium(III) chloride
-
-
1493-13-6
trifluorormethanesulfonic acid
| Conditions | Yield |
|---|---|
| In neat (no solvent) Ar atmosphere, 180°C (3 d); distillation of TfOH, drying (150°C, vacuum, 60 h); | 100% |
| Conditions | Yield |
|---|---|
| In neat (no solvent) Ar atmosphere, 120°C (3 d); distillation of TfOH, drying (120°C, vacuum, 30 h); elem. anal.; | 96% |
-
-
10025-93-1
uranium(III) chloride
| Conditions | Yield |
|---|---|
| In tetrahydrofuran byproducts: NaCl; (N2); stirring for 6 h; removal of solvent (reduced pressure); warming to 50-60°C for 1.5 h (reduced pressure); extn. of solid (diethyl ether); filtration and concn. of ext.; cooling to -80°C; elem. anal.; | 50% |
| Conditions | Yield |
|---|---|
| With potassium In tetrahydrofuran glovebox, under N2 or Ar: addn. of potassium (69.5mmol) to a dry and degassed THF soln. of indene and further addn. of a stoichiometric amt. of UCl3 when react. was complete, stirring of mixture at room temp. for 4d at room temp.;; on removal of solvent in vacuo and extraction of the brown residue with pentane for 8 days; elem. anal.;; | 35% |
-
-
10025-93-1
uranium(III) chloride
-
-
78869-46-2
(η5-MeC5H4)3U(tetrahydrofuran)
| Conditions | Yield |
|---|---|
| In tetrahydrofuran crystn. (hexane/THF); | 33% |
| Conditions | Yield |
|---|---|
| In benzene refluxing for 7 d, drying; extn. with benzene; | 10% |
-
-
10025-93-1
uranium(III) chloride
-
-
7647-14-5
sodium chloride
| Conditions | Yield |
|---|---|
| In neat (no solvent) a well ground stoichiometric mixture of CsCl, NaCl and UCl3 sealed in a quartz tube under vacuum; the mixture next heated at 400°C for 3 days; | |
| In melt fusion of stoichiometric amts. of UCl3, CsCl and NaCl at 1073 - 1173 K in sealed tube; | |
| In melt melting a mixt. of CsCl, NaCl and UCl3 at 1050 K for 1 h (Ar) under periodic stirring in evacuated quartz capsules; |
| Conditions | Yield |
|---|---|
| In neat (no solvent) heating (high vacuum, quartz tube, 1070-1170 K); |
| Conditions | Yield |
|---|---|
| In melt Electrolysis; electrolysis of molten CaCl2, BaF2 or BaCl2 with UCl3 at 900-1050 °C, (0.4-5A, current density: 0.1-1 A/cm*cm), Ni cathode, U anode);; the alloy is dropping from the cathode to the bottom;; | |
| In melt Electrolysis; electrolysis of molten CaCl2, BaF2 or BaCl2 with UCl3 at 900-1050 °C, (0.4-5A, current density: 0.1-1 A/cm*cm), Ni cathode, U anode);; the alloy is dropping from the cathode to the bottom;; |
| Conditions | Yield |
|---|---|
| byproducts: HCl, H2; 450°C; anhydrous HF; |
-
-
10025-93-1
uranium(III) chloride
| Conditions | Yield |
|---|---|
| With water In water byproducts: H; dissolving of UCl3 in H2O, purple react. soln., immediately evolving of H, changing to green colored, then forming of ppte. of uranium(IV)hydroxide (probably);; | |
| With H2O In water byproducts: H; dissolving of UCl3 in H2O, purple react. soln., immediately evolving of H, changing to green colored, then forming of ppte. of uranium(IV)hydroxide (probably);; |
-
-
10025-93-1
uranium(III) chloride
| Conditions | Yield |
|---|---|
| With ammonia In hydrogenchloride | |
| With NH3 In hydrogenchloride |
-
-
10025-93-1
uranium(III) chloride
| Conditions | Yield |
|---|---|
| With H3PO4 or H2C2O4 In hydrogenchloride pptg. of U(IV)salts;; | |
| With H3PO4 or H2C2O4 In hydrogenchloride pptg. of U(IV)salts;; |
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