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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Pharmaceutical Grade CAS 10026-10-5 with competitive price

Cas:10026-10-5

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Shanghai Upbio Tech Co.,Ltd

1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ

Uranium chloride (UCl4)

Cas:10026-10-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Qingdao Beluga Import and Export Co., LTD

URANIUM CHLORIDE CAS:10026-10-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interme

URANIUM CHLORIDE CAS:10026-10-5

Cas:10026-10-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Uranium chloride (UCl4)

Cas:10026-10-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Uranium chloride (UCl4)

Cas:10026-10-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Uranium chloride (UCl4)

Cas:10026-10-5

Min.Order:0

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

Uranium chloride (UCl4)

Cas:10026-10-5

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

Uranium chloride (UCl4)

Cas:10026-10-5

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

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Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

Uranium chloride (UCl4)

Cas:10026-10-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

Uranium chloride (UCl4)

Cas:10026-10-5

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

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Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

Uranium chloride (UCl4)

Cas:10026-10-5

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

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Xi`an Eastling Biotech Co., Ltd.

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:Beijing or Guangzhou

URANIUM CHLORIDE

Cas:10026-10-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Henan Tianfu Chemical Co., Ltd.

1.Our services:A.Supply sampleB.The packing also can be according the customers` requirmentC.Any inquiries will be replied within 24 hoursD.we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate.

Uranium chloride (UCl4)

Cas:10026-10-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

Uranium chloride (UCl4)

Cas:10026-10-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hunan Longxianng Runhui Trading Co.,Ltd

Uranium chloride (UCl4) Application:10026-10-5 Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount. By air(airport to airport) or by sea LCL/FCL for large amount.

Uranium chloride (UCl4)

Cas:10026-10-5

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

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Hubei Langyou International Trading Co., Ltd

Uranium chloride (UCl4) Application:Uranium chloride (UCl4)

Uranium chloride (UCl4)

Cas:10026-10-5

Min.Order:0

Negotiable

Type:Other

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ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

URANIUM CHLORIDE

Cas:10026-10-5

Min.Order:0

Negotiable

Type:Trading Company

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HuBei Ipure Biotech CO.,ltd

HuBei ipure is a diversified product production and operation enterprise, with API, pharma intermediates, and other fine chemicals as well as R&D and pigments development and sales as one of the large enterprises, with more than 130 acres of pl

Uranium chloride (UCl4) CAS NO.10026-10-5

Cas:10026-10-5

Min.Order:1 Kilogram

FOB Price: $1.0 / 2.0

Type:Trading Company

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Hubei Jusheng Technology Co., Ltd.,

1,Best Quality: Our products have exported to Germany, Spain, UK, USA, Australia, Middle East, and so on other countries, and we have got very good feedback from our customers.so

Uranium chloride (UCl4)

Cas:10026-10-5

Min.Order:10 Gram

FOB Price: $1.0 / 2.0

Type:Trading Company

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Shanghai Run-Biotech Co., Ltd.

Shanghai, Run-Biotech Co., Ltd is a leading domestic pharmaceutical, biopharmaceutical, and health care products R & D outsourcing services company. As an innovation-driven and customer-focused company, Run Biotech provides a broad and integrated por

Uranium(IV) chloride

Cas:10026-10-5

Min.Order:0

Negotiable

Type:Trading Company

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Wuhan Demeikai Biotechnology Co., Ltd

Uranium chloride (UCl4)

Uranium chloride (UCl4)

Cas:10026-10-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Taizhou volsen chemical Co., Ltd

We are a trading company aiming at providing high-quality services to customers. Established for many years, with good reputation in the industry Storage:Sealed and preserved Application:Fine chemical intermediates, used as the main raw material for

Uranium chloride (UCl4)

Cas:10026-10-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

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changchun tuocai technology co.,ltld

Uranium chloride (UCl4)

Uranium chloride (UCl4)

Cas:10026-10-5

Min.Order:0

Negotiable

Type:Trading Company

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Hangzhou Fenjun Chemical Co Ltd.

Uranium chloride (UCl4) Application:Uranium chloride (UCl4)

Uranium chloride (UCl4)

Cas:10026-10-5

Min.Order:0

Negotiable

Type:Trading Company

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Hebei Ruishun Trade Co.,Ltd

Supply top quality products with a reasonable price Application:api

10026-10-5

Cas:10026-10-5

Min.Order:0

Negotiable

Type:Trading Company

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Synthetic route

uranyl nirate hexahydrate

uranyl nirate hexahydrate

perchloropropene
1888-71-7

perchloropropene

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

Conditions
ConditionsYield
Inert atmosphere; Reflux;100%
aluminium trichloride
7446-70-0

aluminium trichloride

uranium dioxide

uranium dioxide

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

Conditions
ConditionsYield
Stage #1: aluminium trichloride; uranium dioxide at 250℃; for 5h; Sealed tube;
Stage #2: at 350℃; for 72h; Sealed tube;
99%
perchloropropene
1888-71-7

perchloropropene

uranium(VI) trioxide

uranium(VI) trioxide

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

Conditions
ConditionsYield
at 190℃; for 18h; Schlenk technique; Inert atmosphere;98%
In neat (no solvent) refluxing; sublimation (vac.);
In neat (no solvent) absence of air and moisture; refluxing;
uranium(IV) oxide dihydrate

uranium(IV) oxide dihydrate

uranium(VI) oxide dihydrate

uranium(VI) oxide dihydrate

perchloropropene
1888-71-7

perchloropropene

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

Conditions
ConditionsYield
In further solvent(s) (N2); standard Schlenk technique; UO2*2H2O was added to hexachloropropene at 190°C; heated at 190°C; UO3*2H2O was carefully added;mixt. was heated at 190°C overnight; cooled to room temp.; filtered; washed (CH2Cl2); dried (vac.);98%
hydrogenchloride
7647-01-0

hydrogenchloride

uranium

uranium

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

Conditions
ConditionsYield
In water refluxing (2 h); filtn.;93%
U dissolved in HCl;
In hydrogenchloride prepn. by dissolving U metal chips in 6 M HCl according to N. Dacheux etal., New J. Chem. 19 (1995) 1029; not isolated;
uranium oxide

uranium oxide

perchloropropene
1888-71-7

perchloropropene

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

Conditions
ConditionsYield
Inert atmosphere;55%
uranium(III) hydride

uranium(III) hydride

ammonium chloride

ammonium chloride

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

Conditions
ConditionsYield
In neat (no solvent, solid phase) byproducts: NH3, H2; excess of NH4Cl; heated to 300°C for 30 h; decompn. of NH4-salt in vac. (1E-3 Torr) at 350°C; powder XRD;
uranyl oxalate

uranyl oxalate

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

Conditions
ConditionsYield
With tetrachloromethane
uranyl chloride

uranyl chloride

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

Conditions
ConditionsYield
In perchloric acid aq. HClO4; Electrolysis; electrolytic reduction;
In hydrogenchloride Electrolysis; electrolytic reduction;
uranyl chloride

uranyl chloride

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

Conditions
ConditionsYield
In diethyl ether photochemical redn.;;
In diethyl ether photochemical redn.;;
uranyl chloride

uranyl chloride

A

uranium dioxide

uranium dioxide

B

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

Conditions
ConditionsYield
In hydrogenchloride Electrolysis; dark green soln. of UCl4 and black UO2 sol formed;; not isolated, only in soln.; sol flocculates within 24 h;;
In hydrogenchloride Electrolysis; electrolytical redn. of UO2Cl2 (50g) in 2n HCl (100ml); forming of UCl4 in soln. and a black ppte.;;
uranyl chloride

uranyl chloride

hydrazine
302-01-2

hydrazine

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

Conditions
ConditionsYield
With HCl In water byproducts: N2;
hydrogenchloride
7647-01-0

hydrogenchloride

uranyl chloride

uranyl chloride

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

Conditions
ConditionsYield
In hydrogenchloride Electrolysis; platinum electrodes, diaphragme, 8V;; not isolated;;
In hydrogenchloride Electrolysis; electrolytic reduction on Hg cathode under Ar in cell with cathod and anod septd. by cation-exchange diaphragm; detd. spectrophotometrically and by complexometric titration;
In hydrogenchloride Electrolysis; platinum electrodes, diaphragme, 8V;; not isolated;;
Conditions
ConditionsYield
In neat (no solvent) react. only proceeds at red heat completely; formed UCl4 is sublimating off quantitatively; using sufficient amt. of S2Cl2 inhibits simultaneous formation of UO2Cl2;;>99
chlorinating of U3O8;;
In neat (no solvent) react. only proceeds at red heat completely; formed UCl4 is sublimating off quantitatively; using sufficient amt. of S2Cl2 inhibits simultaneous formation of UO2Cl2;;>99
chlorinating of U3O8;;
Conditions
ConditionsYield
With pyrographite In neat (no solvent) mixture of U3O8 and coal (4:1), passing over of a stream of Cl, forming of UCl4;; proportions (see above) are used to inhibit forming of compd., which contain C;;
With coal In neat (no solvent) mixture of U3O8 and coal (4:1), passing over of a stream of Cl, forming of UCl4;; proportions (see above) are used to inhibit forming of compd., which contain C;;
uranium

uranium

chlorine
7782-50-5

chlorine

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

Conditions
ConditionsYield
In acetonitrile Electrolysis; N2/Cl2-atmosphere, U-anode (pptn.);
uranium

uranium

chlorine
7782-50-5

chlorine

A

UCl2

UCl2

B

UCl

UCl

C

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

Conditions
ConditionsYield
In gaseous matrix co-condensation of U atoms (generated by Nd:YAG laser pulse of 20-50 mJ/10 ns) with Cl2/Ar (1:200 to 1:800) on CsI window at 12 K (6 h, 2-3 mmol*h**-1), stepwise annealing to 20-40 K; not isolated, detd. by IR spectroscopy; product ratio depending on laser pulse intensity and temp. of annealing;
thionyl chloride
7719-09-7

thionyl chloride

uranium oxide

uranium oxide

A

sulfuryl dichloride
7791-25-5

sulfuryl dichloride

B

uranium pentachloride
13470-21-8

uranium pentachloride

C

sulfur dioxide
7446-09-5

sulfur dioxide

D

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

Conditions
ConditionsYield
In neat (no solvent)
In neat (no solvent)
thionyl chloride
7719-09-7

thionyl chloride

uranium dioxide

uranium dioxide

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

Conditions
ConditionsYield
In neat (no solvent) some days, 200°C;;>99
In thionyl chloride UO2 refluxed with SOCl2;
In neat (no solvent) some days, 200°C;;>99
tetrachloromethane
56-23-5

tetrachloromethane

uranium(IV) oxalate

uranium(IV) oxalate

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

Conditions
ConditionsYield
about 500°C; vapor recrystallization;
phosgene
75-44-5

phosgene

uranium oxide

uranium oxide

A

uranyl chloride

uranyl chloride

B

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

Conditions
ConditionsYield
In neat (no solvent) react. at 500 °C;;
phosgene
75-44-5

phosgene

uranium oxide

uranium oxide

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

Conditions
ConditionsYield
In neat (no solvent) byproducts: UO2Cl2; on heating U3O8 (porcelain little ship) in a stream of COCl2 at about 500 °C, small amt. of UO2Cl2 are sublimating off, pptn. of half-molten compd. UCl4;;
In neat (no solvent) byproducts: UO2Cl2; on heating U3O8 (porcelain little ship) in a stream of COCl2 at about 500 °C, small amt. of UO2Cl2 are sublimating off, pptn. of half-molten compd. UCl4;;
phosgene
75-44-5

phosgene

autunite

autunite

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

Conditions
ConditionsYield
In neat (no solvent) byproducts: POCl3, CO2, CaCl2; decompn. at 800 °C;; easy separation of UCl4 from CaCl2;;
In neat (no solvent) byproducts: POCl3, CO2, CaCl2; decompn. at 800 °C;; easy separation of UCl4 from CaCl2;;
phosgene
75-44-5

phosgene

uranium dioxide

uranium dioxide

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

Conditions
ConditionsYield
react. proceeds at about 450 °C;;
In neat (no solvent) react. of a slowly stream of COCl2 with heated UO2, react. temp. about 450 °C;;
react. proceeds at about 450 °C;;
In neat (no solvent) react. of a slowly stream of COCl2 with heated UO2, react. temp. about 450 °C;;
tetrachloromethane
56-23-5

tetrachloromethane

uranium(V) oxide

uranium(V) oxide

A

uranium pentachloride
13470-21-8

uranium pentachloride

B

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

Conditions
ConditionsYield
In neat (no solvent) passing steam of CCl4 over U3O8 at 360 °C;;
disulfur dichloride
10025-67-9

disulfur dichloride

uranium(VI) trioxide

uranium(VI) trioxide

chlorine
7782-50-5

chlorine

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

Conditions
ConditionsYield
In neat (no solvent) byproducts: UCl5, UO2Cl2, S; on heating UO3 in with S2Cl2 satd. chlorine vapor for several hours;; removing of by-products on heating, pptn. of mixture of UCl4 and sulfides, separation of this mixture by sublimation;;
In neat (no solvent) byproducts: UCl5, UO2Cl2, S; on heating UO3 in with S2Cl2 satd. chlorine vapor for several hours;; removing of by-products on heating, pptn. of mixture of UCl4 and sulfides, separation of this mixture by sublimation;;
disulfur dichloride
10025-67-9

disulfur dichloride

uranium oxide

uranium oxide

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

Conditions
ConditionsYield
In neat (no solvent) byproducts: UCl3, S; on using CO2 instead of Cl to pass over S2Cl2, forming of a mixture of UCl4 with some amt. of UCl3 and pptn. of large amt. of S;;
on heating at 230 up to 250 °C;;
In neat (no solvent) below 500°C;;
disulfur dichloride
10025-67-9

disulfur dichloride

uranium dioxide

uranium dioxide

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

Conditions
ConditionsYield
In neat (no solvent) on heating UO2 in Cl-free S2Cl2, react. starts at 230 up to 250 °C; react. proceeds even below sublimation temp. quantitatively;; UCl4 remains free of oxide (nearly); cooling down in dry Cl;;>99
react. of UO2 with S2Cl2 at 230 up to 250 °C, forming of UCl4;;
In neat (no solvent) below 500°C;;
methyl methylphenylphosphinate
6389-79-3

methyl methylphenylphosphinate

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

poly(uranium methylphenylphosphinate)

poly(uranium methylphenylphosphinate)

Conditions
ConditionsYield
In further solvent(s) byproducts: MeCl; slow heating in neat Ph(Me)P(O)OMe until complete pptn.; particle size and polymerization degree depending on heating rate;100%
uranium(IV) chloride
10026-10-5

uranium(IV) chloride

Triphenylphosphine oxide
791-28-6

Triphenylphosphine oxide

[UCl4(triphenylphosphine oxide)2]
58001-79-9, 85281-21-6, 16923-61-8

[UCl4(triphenylphosphine oxide)2]

Conditions
ConditionsYield
In tetrahydrofuran Glovebox;100%
In tetrahydrofuran inert atmosphere; stirring UCl4 for 24 h, Ph3PO addn. (pptn.); collection (filtration), washing (PhMe, hexane);94%
In tetrahydrofuran for 0.166667h;
uranium(IV) chloride
10026-10-5

uranium(IV) chloride

UCl3

UCl3

Conditions
ConditionsYield
With silicon at 450℃; for 480h; Glovebox; Inert atmosphere;100%
uranium(IV) chloride
10026-10-5

uranium(IV) chloride

molybdenum(VI) oxide

molybdenum(VI) oxide

A

molybdenum(VI) oxychloride

molybdenum(VI) oxychloride

B

uranium oxide chloride

uranium oxide chloride

Conditions
ConditionsYield
heating one end of vac. sealed ampoule with equimolar mixt. at 350°C, Mo-compd. crystn. in cold ampoule part, after 3-4 h at 400°CMo-compd. formation ceased, residue crytn. on furnace temp. raising to 450°C; compounds sepn.; elem. anal.;A n/a
B 99%
tetrahydrofuran
109-99-9

tetrahydrofuran

[U(N,N'-bis(3-methoxysalicylidene)-(2,2-dimethyl-1,3-propanediamine)(-2H))2]

[U(N,N'-bis(3-methoxysalicylidene)-(2,2-dimethyl-1,3-propanediamine)(-2H))2]

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

[U(N,N'-bis(3-methoxysalicylidene)-(2,2-dimethyl-1,3-propanediamine)(-2H))Cl2(THF)]
831194-98-0

[U(N,N'-bis(3-methoxysalicylidene)-(2,2-dimethyl-1,3-propanediamine)(-2H))Cl2(THF)]

Conditions
ConditionsYield
In tetrahydrofuran-d8 (Ar); std. Schlenk technique; mixt. of U complex and UCl4 in THF-d8 was heated at 50°C for 12 h;99%
tetrahydrofuran
109-99-9

tetrahydrofuran

lithium bis(diphenylthiophosphinoyl)methanediide

lithium bis(diphenylthiophosphinoyl)methanediide

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

[UCl4(C(PSPh2)2)(Li(THF)2)2]
1223591-44-3

[UCl4(C(PSPh2)2)(Li(THF)2)2]

Conditions
ConditionsYield
In tetrahydrofuran; toluene (Ar); addn. of 1 equiv. of phosphine sulfide deriv. in toluene to THF soln. of 1 equiv. of uranium compd., stirring at 20°C for 5 min; evapn., NMR;98%
tetrahydrofuran
109-99-9

tetrahydrofuran

[U((Ph2P(=S))2C)2(THF)2]

[U((Ph2P(=S))2C)2(THF)2]

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

[U((Ph2P(=S))2C)Cl2(THF)2]
1223591-45-4

[U((Ph2P(=S))2C)Cl2(THF)2]

Conditions
ConditionsYield
In tetrahydrofuran (Ar); mixing uranium compds. in 1:1 molar ratio in THF, keeping at 20°C for 3 h; evapn., elem. anal.;98%
tetrahydrofuran
109-99-9

tetrahydrofuran

bis(diphenylthiophosphoryl)methane
14633-92-2

bis(diphenylthiophosphoryl)methane

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

[U((Ph2P(=S))2C)2(THF)2]

[U((Ph2P(=S))2C)2(THF)2]

Conditions
ConditionsYield
With LiCH2SiMe3 In tetrahydrofuran byproducts: LiCl; (Ar); std. Schlenk technique; Li compd. (4 equiv.) was added to mixt. ofUCl4 (1 equiv.) and H2C(Ph2PS)2 (2 equiv.) in THF; stirred at 20.degree .C for 3 h; evapd.; extd. (toluene); evapd.;98%
tetrahydrofuran
109-99-9

tetrahydrofuran

lithium bis(diphenylthiophosphinoyl)methanediide

lithium bis(diphenylthiophosphinoyl)methanediide

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

[Li2(THF)4U((Ph2P(=S))2C)Cl4]

[Li2(THF)4U((Ph2P(=S))2C)Cl4]

Conditions
ConditionsYield
In tetrahydrofuran; toluene (Ar); std. Schlenk technique; soln. of Li salt in toluene was poured with stirring into soln. of UCl4 in THF; stirred at 20°C for 5 min; evapd.; elem. anal.;98%
[U((Ph2P(=S))2C)2(THF)2]

[U((Ph2P(=S))2C)2(THF)2]

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

[U((Ph2P(=S))2C)Cl2(THF)2]
1223591-45-4

[U((Ph2P(=S))2C)Cl2(THF)2]

Conditions
ConditionsYield
In tetrahydrofuran (Ar); std. Schlenk technique; mixt. of U compd. (1 equiv.) and UCl4 (1 equiv.) in THF was reacted at 20°C for 3 h; evapd.; elem. anal.;98%
pyridine
110-86-1

pyridine

[Cu(N,N'-bis(3-hydroxysalicylidene)-1,2-phenylenediamine(-2H))]
149693-03-8

[Cu(N,N'-bis(3-hydroxysalicylidene)-1,2-phenylenediamine(-2H))]

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

[Cu(N,N'-bis(3-hydroxysalicylidene)-1,2-phenylenediamine-4H)(pyridine)UCl2(pyridine)2]

[Cu(N,N'-bis(3-hydroxysalicylidene)-1,2-phenylenediamine-4H)(pyridine)UCl2(pyridine)2]

Conditions
ConditionsYield
In pyridine all manipulations under Ar atm.; mixt. of Cu compd. and UCl4 heated in py at 80°C for 12 h; filtered, washed with py, dried in vac.; elem. anal.;97%
uranium(IV) chloride
10026-10-5

uranium(IV) chloride

2K(1+)*C8H7CHCH2(2-)=K2C8H7CHCH2

2K(1+)*C8H7CHCH2(2-)=K2C8H7CHCH2

U(C8H7CHCH2)2
37274-09-2

U(C8H7CHCH2)2

Conditions
ConditionsYield
In tetrahydrofuran extraction with cyclohexane;97%
In tetrahydrofuran extraction with cyclohexane;97%
tetrahydrofuran
109-99-9

tetrahydrofuran

[(Li(diethyl ether))2U(C(PSPh2)2)3]

[(Li(diethyl ether))2U(C(PSPh2)2)3]

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

[U((Ph2P(=S))2C)2(THF)2]

[U((Ph2P(=S))2C)2(THF)2]

Conditions
ConditionsYield
In tetrahydrofuran byproducts: LiCl; (Ar); mixing 1 equiv. of uranium tetachloride and 1 equiv. of uranium carbene deriv. in THF, keeping at 20°C for 4 h; evapn., extn. (toluene), evapn., drying in vac., elem. anal.;97%
1,2-dimethoxyethane
110-71-4

1,2-dimethoxyethane

dichlorobis(η-tetramethylphospholyl)uranium(IV)
146687-48-1

dichlorobis(η-tetramethylphospholyl)uranium(IV)

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

{(dimethoxyethane)(η5-tetramethylphospholyl)uranium trichloride}
155706-45-9

{(dimethoxyethane)(η5-tetramethylphospholyl)uranium trichloride}

Conditions
ConditionsYield
In 1,2-dimethoxyethane (under Ar) a flask is charged with UCl4, the U-Complex and DME is condensed into it under vac. at -78°C, mixt. is stirred for 2 h at 20°C; soln. is evapd. to dryness;96%
tetrahydrofuran
109-99-9

tetrahydrofuran

lithium bis(diphenylthiophosphinoyl)methanediide

lithium bis(diphenylthiophosphinoyl)methanediide

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

[U((Ph2P(=S))2C)2(THF)2]

[U((Ph2P(=S))2C)2(THF)2]

Conditions
ConditionsYield
In tetrahydrofuran; toluene (Ar); std. Schlenk technique; soln. of Li salt (2 equiv.) in toluene waspoured with stirring into soln. of UCl4 in THF; stirred at 20°C for 5 min; evapd.; extd. (toluene); evapd. (vac.); elem. anal.;96%
In tetrahydrofuran; toluene (Ar); addn. of 2 equiv. of phosphine sulfide deriv. in toluene to THF soln. of 1 equiv. of uranium compd., stirring at 20°C for 5 min; evapn., extn. (toluene), evapn., drying in vac., elem. anal.;95%
C60H57Li3N4Si3

C60H57Li3N4Si3

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

C60H57ClN4Si3U

C60H57ClN4Si3U

Conditions
ConditionsYield
In tetrahydrofuran at -78 - 20℃; for 16.0833h; Reflux;96%
lithium diethylamide
816-43-3

lithium diethylamide

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

dipotassium cyclooctatetraenide
34480-05-2

dipotassium cyclooctatetraenide

[(η(8)-C8H8)U(NEt2)3]
152249-43-9

[(η(8)-C8H8)U(NEt2)3]

Conditions
ConditionsYield
With TlBPh4 In tetrahydrofuran (argon); condensing THF at -78°C under vac. to UCl4 and LiNEt2, stirring (20°C, 5 h), addn. of K2C8H8, after 90 min addn. of TlBPh4, reacting further 90 min; evapn., extn. (pentane), evapn.; elem. anal.;95%
3-picoline-N-oxide
1003-73-2

3-picoline-N-oxide

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

{(3-picoline-N-oxide)2(ethanol)2uranium(IV) tetrachloride}

{(3-picoline-N-oxide)2(ethanol)2uranium(IV) tetrachloride}

Conditions
ConditionsYield
With C2H5OH In ethanol addn. of the ligand in ice-cold abs. EtOH to the U compd. in abs. EtOH under a flow of dry and oxygen-free N2 (Schlenk technique); addn. of dry EtO2, filtn. under anhydrous condition, washing with abs. EtOH-THF and ether and drying in vac.; elem. anal.;95%
tetrahydrofuran
109-99-9

tetrahydrofuran

N,N′-bis(3-methoxysalicylidene)-2,2-dimethyl-1,3-propanediamine
188482-90-8

N,N′-bis(3-methoxysalicylidene)-2,2-dimethyl-1,3-propanediamine

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

[U(N,N'-bis(3-methoxysalicylidene)-(2,2-dimethyl-1,3-propanediamine)(-2H))Cl2(THF)]
831194-98-0

[U(N,N'-bis(3-methoxysalicylidene)-(2,2-dimethyl-1,3-propanediamine)(-2H))Cl2(THF)]

Conditions
ConditionsYield
In tetrahydrofuran-d8 byproducts: HCl; (Ar); std. Schlenk technique; mixt. of ligand (1 equiv.) and UCl4 in THF-d8 in NMR tube was heated at 50°C for 24 h; elem. anal.;95%
[K(diethyl ether)][SPS(Me)]

[K(diethyl ether)][SPS(Me)]

uranium(IV) chloride
10026-10-5

uranium(IV) chloride

[UCl2(SPS(Me))2]

[UCl2(SPS(Me))2]

Conditions
ConditionsYield
In tetrahydrofuran byproducts: KCl; (Ar); stirred for 4 h at 20°C; filtered, evapd., extd (THF), filtered, concd., Et2O added, crystd. for 24 h, filtered off, dried (vac.); elem. anal.;95%

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