As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:101-17-7
Min.Order:1 Kilogram
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Type:Lab/Research institutions
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Min.Order:5 Kiloliter
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Type:Manufacturers
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Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
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Cas:101-17-7
Min.Order:1 Gram
FOB Price: $12.0 / 15.0
Type:Trading Company
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Min.Order:1 Kilogram
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Type:Trading Company
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Min.Order:1 Metric Ton
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inquiryAppearance:Pale Yellow to Yellow oil Storage:room temperature Package:200kg/drum Application:3-Chlorodiphenylamine (cas# 101-17-7) is a compound useful in organic synthesis Transportation:Express/Sea/Air Port:Shanghai
Cas:101-17-7
Min.Order:1 Kilogram
FOB Price: $1.0
Type:Lab/Research institutions
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Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
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Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
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Cas:101-17-7
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
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Cas:101-17-7
Min.Order:10 Gram
Negotiable
Type:Trading Company
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Min.Order:0 Metric Ton
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Cas:101-17-7
Min.Order:0
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Cas:101-17-7
Min.Order:10 Gram
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Min.Order:1 Kilogram
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Cas:101-17-7
Min.Order:1 Metric Ton
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Type:Trading Company
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Conditions | Yield |
---|---|
With tris(dibenzylideneacetone)dipalladium (0); 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate In toluene at 90 - 110℃; for 11h; Buchwald-Hartwig reaction; | 100% |
With pectin-stabilized copper nanoparticles In dimethyl sulfoxide at 110℃; for 2h; | 82% |
Conditions | Yield |
---|---|
With dicyclohexyl-(2′,4′,6′-triisopropyl-3,6-dimethoxy-[1,1′-biphenyl]-2-yl)phosphine; chloro[2-(dicyclohexylphosphino)-3,6-dimethoxy-2',4',6'-triisopropyl-1,1'-biphenyl][2-(2-aminoethyl)phenyl]palladium(ll); sodium t-butanolate In toluene at 80℃; Inert atmosphere; | 96% |
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In ethanol at 75℃; for 1h; Inert atmosphere; | 95% |
With toluene-4-sulfonic acid In ethanol at 75℃; | 40% |
Conditions | Yield |
---|---|
With η5‐cyclopentadienyl‐η3‐1‐phenylallylpalladium; potassium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In 1,4-dioxane at 80℃; for 12h; Reagent/catalyst; Temperature; Solvent; | 95% |
Conditions | Yield |
---|---|
With copper immobilized at polyimide covalent organic framework In methanol; water at 20℃; for 8h; Chan-Lam Coupling; | 87% |
With pyridine; copper(II) acetate monohydrate In dichloromethane at 39.84℃; for 24h; | 83% |
With potassium tert-butylate; tetra(n-butyl)ammonium hydroxide; copper diacetate In water at 20℃; for 22h; | 72% |
Conditions | Yield |
---|---|
Stage #1: nitrobenzene With [2,2]bipyridinyl; [MoO2Cl2(dmf)2] In toluene for 0.0333333h; Stage #2: 3-chlorophenylboronic acid With triphenylphosphine In toluene at 100℃; for 20h; | 87% |
2-(trimethylsilyl)phenyl trifluoromethanesulfonate
3-chloro-aniline
3-chlorodiphenylamine
Conditions | Yield |
---|---|
With cis,trans-2,5-dimethoxytetrahydrofuran; acetonedicarboxylic acid; cesium fluoride In acetonitrile at 20℃; | 85.7% |
Conditions | Yield |
---|---|
With copper phthalocyanine; copper(II) sulfate In methanol at 15℃; | 85% |
With tetrabenzoporphyrinatocobalt(II); copper diacetate In acetonitrile at 0℃; for 13h; chemoselective reaction; | 55% |
Conditions | Yield |
---|---|
With copper diacetate; triethylamine at 20℃; for 24h; | 84% |
Conditions | Yield |
---|---|
Stage #1: 3-Nitrochlorobenzene With [2,2]bipyridinyl; [MoO2Cl2(dmf)2] In toluene for 0.0333333h; Stage #2: phenylboronic acid With triphenylphosphine In toluene at 100℃; for 20h; | 84% |
Conditions | Yield |
---|---|
With palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate In toluene for 24h; Reflux; | 82% |
With palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate In toluene for 24h; Reflux; | 82% |
With palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate In toluene for 24h; Reflux; | 82% |
With potassium hydroxide In N,N-dimethyl-formamide at 130℃; for 0.483333h; Buchwald-Hartwig Coupling; | 68% |
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine; tetrabutylammonium perchlorate; copper diacetate; triethylamine In acetonitrile at 20℃; for 20h; Chan-Lam Coupling; Electrochemical reaction; chemoselective reaction; | 75% |
With N-(pyrid-2-yl)benzamide; nickel(II) acetate tetrahydrate; N,N,N',N'-tetramethylguanidine In toluene at 60℃; for 24h; Chan-Lam Coupling; | 74% |
With ammonium cerium (IV) nitrate; copper diacetate In toluene at 20℃; for 12h; Chan-Lam Coupling; | 73% |
With 2,6-dimethylpyridine; fac-tris(2-phenylpyridinato-N,C2')iridium(III); copper diacetate; n-tetradecanoic acid In toluene; acetonitrile at 35℃; for 20h; Reagent/catalyst; Chan-Lam Coupling; Irradiation; | 62% |
With C30H25N4O(1-)*3C2H3O2(1-)*2Cu(2+) In methanol at 20℃; for 24h; | 34 %Spectr. |
3-[(4-methylphenyl)sulfonyl]-1-phenyltriaz-1-ene
3-chlorophenylboronic acid
3-chlorodiphenylamine
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In toluene at 110℃; for 24h; Molecular sieve; Inert atmosphere; Schlenk technique; | 65% |
Conditions | Yield |
---|---|
With copper; potassium carbonate | 50% |
Conditions | Yield |
---|---|
With copper; potassium carbonate; potassium iodide Reagens 4: Nitrobenzol; und Erwaermen des Reaktionsprodukts mit wss.-aethanol. HCl; | |
With copper(l) iodide; potassium carbonate In nitrobenzene for 15h; Heating; |
N-(3-chlorophenyl)anthranilic acid
3-chlorodiphenylamine
Conditions | Yield |
---|---|
at 250 - 260℃; |
N-(3-chloro-phenyl)-N-phenyl-benzamide
A
3-chlorodiphenylamine
B
benzoic acid
Conditions | Yield |
---|---|
With barium dihydroxide; cetyltrimethylammonim bromide In water at 65.5℃; Rate constant; Mechanism; absence of ctab, other reagent, other solvent; |
chlorobenzene
Phenyl azide
A
3-chlorodiphenylamine
B
N-(4-chlorophenyl)aniline
C
N-phenyl-2-chloroaniline
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid at 65℃; for 2h; Yield given. Yields of byproduct given; |
3-chlorodiphenylamine
Conditions | Yield |
---|---|
With copper(l) chloride und nachfolgenden Hydrolyse; |
Conditions | Yield |
---|---|
for 0.25h; Microwave irradiation; |
C15H14ClNO2
3-chlorodiphenylamine
Conditions | Yield |
---|---|
With potassium hydroxide at 130℃; for 2h; | 138 mg |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sodium nitrite; hydrogenchloride; sodium acetate / water / 1 h / 0 °C 1.2: 0 - 20 °C 2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 24 h / 110 °C / Molecular sieve; Inert atmosphere; Schlenk technique View Scheme |
3-chlorodiphenylamine
chloroacetyl chloride
N-chloroacetyl-N-phenyl-m-chloroaniline
Conditions | Yield |
---|---|
In toluene Heating; | 95% |
In N,N-dimethyl-formamide at 20℃; for 4h; | 89.6% |
In benzene Heating; | |
In toluene |
3-chlorodiphenylamine
N,N-diethylcarbamyl chloride
N,N-diethyl-N'-(3-chlorophenyl)-N'-phenylurea
Conditions | Yield |
---|---|
With lithium diisopropyl amide In tetrahydrofuran at 0 - 20℃; | 89% |
Conditions | Yield |
---|---|
potassium hydroxide; copper In various solvent(s) at 160℃; for 27h; | 88% |
3-chlorodiphenylamine
sodium isocyanate
1-(m-chlorophenyl)-1-phenylurea
Conditions | Yield |
---|---|
With trifluoroacetic acid In benzene for 5h; Ambient temperature; | 84% |
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