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Cas:1441-87-8
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
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Min.Order:1 Kilogram
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Min.Order:1 Kilogram
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Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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Benzoyl chloride,2-hydroxy- cas 1441-87-8Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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Conditions | Yield |
---|---|
With thionyl chloride; N,N-dimethyl-formamide In toluene at 50℃; for 2.5h; | 100% |
With thionyl chloride In 1,2-dichloro-ethane for 2h; Heating; | 100% |
With thionyl chloride; N,N-dimethyl-formamide at 90℃; for 48h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With toluene |
Conditions | Yield |
---|---|
With thionyl chloride | |
With thionyl chloride | |
With phosphorus pentachloride In benzene |
Conditions | Yield |
---|---|
at 20℃; |
Conditions | Yield |
---|---|
With benzene | |
In benzene |
tetrachloromethane
phenol
A
(trichloromethoxy)benzene
B
Phenyl 4-hydroxybenzoate
C
phenyl Salicylate
D
salicyloyl chloride
Conditions | Yield |
---|---|
for 5h; Irradiation; Yield given. Yields of byproduct given; |
Conditions | Yield |
---|---|
for 2h; Heating; |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: potassium carbonate / 4 h / Reflux 2.1: sodium dihydrogenphosphate; dihydrogen peroxide; sodium chlorite / water; acetonitrile / 1.5 h / 10 - 20 °C 2.2: 0.08 h 3.1: thionyl chloride / dichloromethane; N,N-dimethyl-formamide / 1 h / 20 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sodium dihydrogenphosphate; dihydrogen peroxide; sodium chlorite / water; acetonitrile / 1.5 h / 10 - 20 °C 1.2: 0.08 h 2.1: thionyl chloride / dichloromethane; N,N-dimethyl-formamide / 1 h / 20 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium hydroxide / ethanol; water / Reflux 2: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 20 °C View Scheme |
anthranilic acid
salicyloyl chloride
2-(2-hydroxybenzoyl)aminobenzoic acid
Conditions | Yield |
---|---|
With pyridine at 50℃; for 0.583333h; Sonication; | 99% |
With triethylamine In tetrahydrofuran at 20℃; | |
With benzene |
Conditions | Yield |
---|---|
Stage #1: salicyloyl chloride With hydrazine hydrate In 1,4-dioxane at 0 - 20℃; Stage #2: With boron trifluoride diethyl etherate In 1,4-dioxane at 130℃; for 2.5h; | 98% |
Conditions | Yield |
---|---|
In dichloromethane byproducts: HCl; N2-atmosphere; stirring (25 min); evapn. (vac.), recrystn. (toluene / hexane); elem. anal.; | 96% |
N-hydroxybenzenecarboximidamide
salicyloyl chloride
O-salicylbenzamidoxime
Conditions | Yield |
---|---|
With ammonium hydroxide In tetrahydrofuran for 0.333333h; | 95% |
salicyloyl chloride
Conditions | Yield |
---|---|
With 4-vinylpyridine In tetrahydrofuran at 20℃; Acylation; | 95% |
salicyloyl chloride
Conditions | Yield |
---|---|
With 4-vinylpyridine; silver benzoate In tetrahydrofuran at 20℃; Acylation; | 95% |
salicyloyl chloride
Conditions | Yield |
---|---|
With 4-vinylpyridine; silver benzoate In tetrahydrofuran at 20℃; Acylation; | 95% |
4-vinyloxyaniline
salicyloyl chloride
2-hydroxybenzoic acid p-vinyloxyanilide
Conditions | Yield |
---|---|
With triethylamine In acetone at -20 - -10℃; | 92% |
2-(biphenyl-4-yloxy)acetic acid hydrazide
salicyloyl chloride
Conditions | Yield |
---|---|
With 4-vinylpyridine In tetrahydrofuran at 20℃; Acylation; | 92% |
Conditions | Yield |
---|---|
With triethylamine In benzene at 0 - 24℃; for 48h; | 92% |
With triethylamine In diethyl ether for 2h; Acylation; |
7-amino-4-methylcoumarin.
salicyloyl chloride
2-hydroxy-N-(4-methyl-2-oxo-2H-chromen-7-yl)benzamide
Conditions | Yield |
---|---|
With pyridine In acetone at 20℃; | 92% |
salicyloyl chloride
2-hydroxybenzoyl azide
Conditions | Yield |
---|---|
With sodium azide at 20℃; Substitution; | 91% |
Conditions | Yield |
---|---|
With sodium hydroxide at 20℃; | 90% |
With sodium hydroxide; water Erwaermen des nach dem Ansaeuern erhaltenen Reaktionsprodukts mit wss. Natronlauge; |
3-(vinyloxy)aniline
salicyloyl chloride
2-Hydroxy-N-(3-vinyloxy-phenyl)-benzamide
Conditions | Yield |
---|---|
With triethylamine In acetone at -20 - -10℃; | 90% |
salicyloyl chloride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 30 - 60℃; Large scale; | 90% |
Conditions | Yield |
---|---|
In tetrahydrofuran; Petroleum ether for 0.5h; | 89% |
Conditions | Yield |
---|---|
With pyridine In 1,4-dioxane for 4h; Acylation; Heating; | 88% |
Heating; |
Conditions | Yield |
---|---|
With water; sodium hydroxide at 20℃; Bamberger Imidazole Cleavage; | 87% |
Conditions | Yield |
---|---|
With pyridine In chloroform at 20℃; for 1h; | 87% |
salicyloyl chloride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 30 - 60℃; | 87% |
1-(2-naphthyloxyacetyl)hydrazine
salicyloyl chloride
Conditions | Yield |
---|---|
With 4-vinylpyridine In tetrahydrofuran at 20℃; Acylation; | 86% |
diethyl malonate
salicyloyl chloride
ethyl 3-ethoxy-3-hydroxy-2-(2-hydroxybenzoyl)acrylate
Conditions | Yield |
---|---|
Stage #1: diethyl malonate With tetrachloromethane; ethanol; magnesium In toluene at 20℃; for 1.5h; Reflux; Stage #2: salicyloyl chloride In toluene at 0 - 20℃; Stage #3: With hydrogenchloride; water In toluene at 0 - 5℃; | 86% |
salicyloyl chloride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane for 15h; Reflux; | 85.6% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 0.0833333h; | 85% |
With triethylamine In dichloromethane at 0 - 20℃; for 12h; | 60% |
1H-imidazole
salicyloyl chloride
1-(1-(2-hydroxyphenyl)-2-methanone)-1H-imidazole
Conditions | Yield |
---|---|
In chloroform at 20℃; Solvent; Schotten-Baumann Reaction; | 85% |
6,7-Dimethoxy-2H-1,3-benzothiazine
salicyloyl chloride
2,3-Dimethoxy-12aH-12-oxa-5-thia-6a-aza-benzo[a]anthracen-7-one
Conditions | Yield |
---|---|
83% |
anthranilic acid amide
salicyloyl chloride
2-(2'-hydroxyphenyl)-4-(3H)-quinazolinone
Conditions | Yield |
---|---|
With antimony(III) chloride In neat (no solvent) at 300℃; for 0.0666667h; Microwave irradiation; Green chemistry; | 82% |
dexamfetamine
salicyloyl chloride
S-N-<(+)-α-benzylethyl>-o-hydroxybenzamide
Conditions | Yield |
---|---|
80% |
Conditions | Yield |
---|---|
With N,N-dimethyl-aniline In 1,2-dichloro-ethane at 40℃; for 6h; | 80% |
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