Product Description
Cas:156-28-5
Min.Order:1 Kilogram
FOB Price: $5.0 / 30.0
Type:Lab/Research institutions
inquiryCAS No.: 156-28-5 Other Names: Beta-Phenethylamine Hydrochloride MF: C8H12ClN EINECS No.: 205-849-2 Place of Origin: Anhui, China (Mainland) Type: Central Nervous System Agents Grade Standard: Medicine Grade Brand Nam
Cas:156-28-5
Min.Order:1 Metric Ton
Negotiable
Type:Trading Company
inquiryXi’an Quanao Biotech Co., Ltd. with 18 years experience in plant extract filed. Product grade: Medicine, Health care product, Cosmetics, Food, Beverage, Feed. Hot selling market: Europe, North America, South America, Middle East, Asia Pacifi
Cas:156-28-5
Min.Order:1 Kilogram
FOB Price: $149.0 / 161.0
Type:Manufacturers
inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
Cas:156-28-5
Min.Order:1 Kilogram
Negotiable
Type:Manufacturers
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:156-28-5
Min.Order:1
Negotiable
Type:Other
inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:156-28-5
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiry
Cas:156-28-5
Min.Order:1 Metric Ton
FOB Price: $1.0
Type:Manufacturers
inquiryProduct Name: 2-Phenylethylamine hydrochloride Cas No.:156-28-5 MF:C8H12ClN MW:157.64 Purity:99%
Cas:156-28-5
Min.Order:1 Kilogram
FOB Price: $12.0 / 14.0
Type:Other
inquiryHigh purity CAS 156-28-5 2-Phenylethylamine hydrochloride in stock Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED intermedi
Cas:156-28-5
Min.Order:1 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryName: .beta.-Phenethylamine hydrochloride CAS:156-28-5 MF: C8H12ClN Appearance:White Powder Storage:Store in cool and dry place, away from sun light. Package:25KG Application:Cosmetic Raw Materials, Detergent Raw Materials, Hair Care Chemicals Tran
Cas:156-28-5
Min.Order:1 Kilogram
FOB Price: $1.0
Type:Other
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:156-28-5
Min.Order:10 Gram
FOB Price: $146.0 / 176.0
Type:Trading Company
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by email in time prod
Cas:156-28-5
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiry1. Product advantages High purity, all above 98.5%, no impurities after dissolution We will test each batch to ensure quality OEM and private brand services designed for free Various cap colors available We can also provide MT1 peptide powd
Cas:156-28-5
Min.Order:1 Kilogram
FOB Price: $110.0 / 112.0
Type:Trading Company
inquiry1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:white or off-white powder Storage:Store in sealed containers
Cas:156-28-5
Min.Order:100 Gram
Negotiable
Type:Other
inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
Cas:156-28-5
Min.Order:1 Kilogram
FOB Price: $1.0 / 10.0
Type:Trading Company
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:156-28-5
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryWe are the manufacturers and suppliers of API in China, and warehouse in Germany and USA of California, which can quickly and safely deliver to your address 1.High quality and competitive price. 2.Free sample for your evaluation. 3.Promptly delivery
Cas:156-28-5
Min.Order:10 Gram
FOB Price: $1.35
Type:Trading Company
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
Cas:156-28-5
Min.Order:1 Kilogram
FOB Price: $30.0 / 35.0
Type:Trading Company
inquiryBeluga chemical professional supply High quality 2-phenylethanaminium chloride CAS 156-28-5 1. Beluga Chemical has a professional RESEARCH and development team and strong technical force to ensure technical support and research capabilities. 2. M
Cas:156-28-5
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:156-28-5
Min.Order:10 Kilogram
Negotiable
Type:Trading Company
inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
Cas:156-28-5
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:156-28-5
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:156-28-5
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:156-28-5
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:156-28-5
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:156-28-5
Min.Order:100 Gram
FOB Price: $100.0 / 2000.0
Type:Lab/Research institutions
inquiryEstablished in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
Cas:156-28-5
Min.Order:10 Gram
Negotiable
Type:Lab/Research institutions
inquiry1. A strong scientific research team . 2. Stable quality (with a complete scientific research center and testing center to ensure the quality stability of each batch of products). 3. Rich export experience (with practical experience in exporting to m
Cas:156-28-5
Min.Order:1 Kilogram
FOB Price: $8.2 / 8.8
Type:Trading Company
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:156-28-5
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryOur Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
Cas:156-28-5
Min.Order:0
Negotiable
Type:Trading Company
inquiryConditions | Yield |
---|---|
With hydrogenchloride; hydrogen In propan-1-ol; water at 60℃; under 375.038 Torr; for 18h; Flow reactor; | 100% |
Stage #1: phenylacetonitrile With water; palladium diacetate; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane In dichloromethane at 25℃; for 12h; Sealed tube; Inert atmosphere; Stage #2: With hydrogenchloride In water chemoselective reaction; | 99% |
Stage #1: phenylacetonitrile With ammonium hydroxide; hydrogen; cobalt(II) diacetate tetrahydrate; zinc trifluoromethanesulfonate; zinc In methanol at 120℃; under 30003 Torr; for 15h; Sealed tube; Autoclave; Stage #2: With hydrogenchloride In diethyl ether | 96% |
Conditions | Yield |
---|---|
Stage #1: phenethyl azide With triphenylphosphine at 110℃; for 20h; Staudinger Azide Reduction; Green chemistry; Stage #2: With hydrogenchloride In 1,4-dioxane; diethyl ether Green chemistry; | 97% |
Stage #1: phenethyl azide With 1,3-diphenyl-disiloxane; triphenylphosphine at 20℃; for 24h; Staudinger Azide Reduction; Stage #2: With water Stage #3: With hydrogenchloride In 1,4-dioxane chemoselective reaction; | 90% |
Multi-step reaction with 2 steps 1: benzene / Ambient temperature 2: HCl / benzene / 2 h / Ambient temperature View Scheme |
Conditions | Yield |
---|---|
With hydrogenchloride In methanol | 90% |
With hydrogenchloride In water | |
With hydrogenchloride In methanol; diethyl ether at 20℃; Inert atmosphere; | |
With hydrogenchloride In water at 20℃; | 68.6 mg |
Conditions | Yield |
---|---|
Stage #1: 2-Phenylnitroethane With C36H56Cl3CrN2O; magnesium; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane In tetrahydrofuran at 60℃; for 24h; Inert atmosphere; Schlenk technique; Stage #2: With hydrogenchloride In tetrahydrofuran; water; ethyl acetate at 20℃; | 83% |
Conditions | Yield |
---|---|
Stage #1: 3-phenylpropionamide With tetrafluoroboric acid; iodobenzene; 3-chloro-benzenecarboperoxoic acid In dichloromethane; water at 25℃; for 48h; Hofmann rearrangement; Inert atmosphere; Stage #2: With hydrogenchloride In dichloromethane; water Inert atmosphere; | 82% |
With hydrogenchloride; formic acid; iodosylbenzene 1.) CH3CN, H2O, 15 h, room temp.; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
Stage #1: 1-phenethyl-3,4-diphenyl-1H-pyrrole-2,5-dione With potassium hydroxide In ethanol; water at 102℃; for 0.133333h; Microwave irradiation; Green chemistry; Stage #2: With hydrogenchloride In ethanol; water pH=4; Temperature; Green chemistry; | A n/a B 82% |
Conditions | Yield |
---|---|
Stage #1: L-phenylalanine With (R)-Carvone In propan-1-ol at 190℃; under 11251.1 Torr; for 0.0833333h; Sealed tube; Stage #2: With hydrogenchloride In propan-1-ol; water at 190℃; for 0.0833333h; | 78% |
Multi-step reaction with 2 steps 1: propan-1-ol / 20 - 190 °C / Green chemistry 2: hydrogenchloride / propan-1-ol / 0.08 h / 190 °C / Green chemistry View Scheme |
2-phenylethylamine hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In propan-1-ol at 190℃; for 0.0833333h; Temperature; Green chemistry; | 78% |
N-phenethylbenzamide
ethylmagnesium bromide
A
2-phenylethylamine hydrochloride
B
1-phenyl-propan-1-one
Conditions | Yield |
---|---|
Stage #1: N-phenethylbenzamide With 2-fluoropyridine; trifluoromethylsulfonic anhydride In dichloromethane at 0℃; for 0.5h; Stage #2: ethylmagnesium bromide With cerium(III) chloride In tetrahydrofuran; dichloromethane at -78℃; for 2h; Stage #3: With hydrogenchloride In ethyl acetate | A 76% B n/a |
Conditions | Yield |
---|---|
Stage #1: Benzeneacetamide With [(aNHC)KN(SiMe3)2]2; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane In toluene at 40℃; for 12h; Inert atmosphere; Glovebox; Schlenk technique; Stage #2: With water; sodium hydroxide In diethyl ether; toluene at 40℃; for 1h; Inert atmosphere; Glovebox; Schlenk technique; Stage #3: With hydrogenchloride In diethyl ether; water Inert atmosphere; Glovebox; Schlenk technique; | 75% |
Stage #1: Benzeneacetamide With triethyl borane; phenylsilane; potassium acetate In tetrahydrofuran; tert-butyl methyl ether at 120℃; Inert atmosphere; Schlenk technique; Sealed tube; Stage #2: With hydrogenchloride In ethyl acetate at 20℃; for 8h; Inert atmosphere; chemoselective reaction; | 54% |
Stage #1: Benzeneacetamide With triethyl borane; phenylsilane; potassium acetate In tert-butyl methyl ether at 120℃; Inert atmosphere; Glovebox; Schlenk technique; Sealed tube; Stage #2: With hydrogenchloride In ethyl acetate at 20℃; for 8h; Inert atmosphere; Schlenk technique; Glovebox; Sealed tube; | 54% |
Multi-step reaction with 2 steps 1: lithium 2,6-di-tert-butylphenolate / neat (no solvent) / 18 h / 60 °C / Inert atmosphere; Glovebox; Schlenk technique 2: sodium hydroxide / water; diethyl ether / 1 h View Scheme |
ethyl 3-(4-oxo-1-(2-phenylethyl)-3-piperidinyl)propionate hydrochloride
aniline
A
2,4'-diaminodiphenylmethane
B
2-phenylethylamine hydrochloride
Conditions | Yield |
---|---|
In toluene for 4h; | A n/a B 69% |
1-<<(Triphenylphosphoranylidene)amino>methyl>benzotriazole
benzylmagnesium chloride
2-phenylethylamine hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride 1.) THF/diethyl ether, 20 min, rt.; 2.) diethyl ether, 1h; | 67% |
Conditions | Yield |
---|---|
With hydrogenchloride; palladium 10% on activated carbon; hydrogen In ethanol at 0℃; for 6h; Inert atmosphere; | 51% |
Conditions | Yield |
---|---|
With hydrogenchloride; palladium 10% on activated carbon; hydrogen In ethanol at 0℃; for 3.5h; | 51% |
Conditions | Yield |
---|---|
Stage #1: methyl-N-(benzyl-methyl)-formamide With pyridine; oxalyl dichloride In tetrahydrofuran at 0℃; for 0.5h; Inert atmosphere; Stage #2: With propylene glycol In tetrahydrofuran at 0 - 25℃; Inert atmosphere; | 49% |
2-phenylethylamine hydrochloride
Conditions | Yield |
---|---|
Stage #1: 2-oxo-2-phenylethyl phenethylcarbamate With potassium phosphate; tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate; ascorbic acid In water; acetonitrile at 20℃; for 3h; Sealed tube; Irradiation; Inert atmosphere; Stage #2: With hydrogenchloride In diethyl ether Inert atmosphere; | 49% |
methanol
Nα-diphenylphosphinyl-2-phenylethylamine
A
2-phenylethylamine hydrochloride
B
methyl diphenylphosphinate
Conditions | Yield |
---|---|
With hydrogenchloride Rate constant; Kinetics; Thermodynamic data; E, ΔS, ΔG presented; |
methanol
N-(2-phenylethyl)-P,P-dimethylphosphinamide
A
dimethyl-phosphinic acid methyl ester
B
2-phenylethylamine hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride Rate constant; Kinetics; Thermodynamic data; E, ΔS, ΔG presented; |
methanol
N-(2-phenylethyl)-P,P-diethylphosphinamide
A
methyl diethylphosphinate
B
2-phenylethylamine hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride Rate constant; Kinetics; Thermodynamic data; E, ΔS, ΔG presented; |
methanol
N-(2-phenylethyl)-P,P-di-n-butylphosphinamide
A
methyl dibutylphosphinate
B
2-phenylethylamine hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride Rate constant; Kinetics; Thermodynamic data; E, ΔS, ΔG presented; |
methanol
5-dibenzophosphole-5-oxide
A
5-methoxydibenzophosphole 5-oxide
B
2-phenylethylamine hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride Rate constant; Kinetics; Thermodynamic data; E, ΔS, ΔG presented; |
methanol
N-(2-phenylethyl)-P,P-dibenzylphosphinamide
A
methyl dibenzylphosphinate
B
2-phenylethylamine hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride Rate constant; Kinetics; Thermodynamic data; E, ΔS, ΔG presented; |
1--2-phenyl-ethan
A
Hexamethyldisiloxane
B
2-phenylethylamine hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride; water In diethyl ether Yield given; |
Nα-diphenylphosphinyl-2-phenylethylamine
2-phenylethylamine hydrochloride
Conditions | Yield |
---|---|
With trifluoroacetic acid for 0.166667h; |
Conditions | Yield |
---|---|
With ammonium formate; palladium on activated charcoal In methanol at 65℃; for 2h; Yield given; |
Phenethyl-phosphorimidic acid triethyl ester
2-phenylethylamine hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In benzene for 2h; Ambient temperature; Yield given; |
3-<(E)-(2-phenylethenyl)>-4,5-diphenyl-2(3H)oxazolone
2-phenylethylamine hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride; hydrogen; palladium on activated charcoal 1) EtOH, H2O, HOAc, 50 deg C, 50 psi, 4h, 2) EtOH; Yield given. Multistep reaction; |
2-phenylethylamine hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride; hydrogen; palladium on activated charcoal 1) EtOH, H2O, HOAc, 50 deg C, 50 psi, 4h, 2) EtOH; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
With hydrogenchloride; sodium azide 2) ether; Multistep reaction; |
2-phenylethylamine hydrochloride
N,N-dimethyl-formamide dimethyl acetal
N,N-dimethyl-N'-phenethyl-formamidine
Conditions | Yield |
---|---|
for 2h; Reflux; | 100% |
2-phenylethylamine hydrochloride
Conditions | Yield |
---|---|
With hydrogen; water-d2; palladium on activated charcoal at 20℃; for 72h; | 99% |
With hydrogen; water-d2; palladium on activated charcoal at 110℃; under 760.051 Torr; for 24h; | 94% |
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol for 8h; Mannich reaction; Heating; | 98% |
2-phenylethylamine hydrochloride
phenylacetylene
N-phenethyl-2-phenylacetamide
Conditions | Yield |
---|---|
With potassium hexafluorophosphate; 4-methylpyridine-1-oxide; chloro(cyclopentadienyl)bis(triphenylphosphine)ruthenium (II); potassium carbonate In 1,2-dichloro-ethane at 100℃; for 24h; Catalytic behavior; Reagent/catalyst; Inert atmosphere; Sealed tube; | 98% |
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol for 8h; Mannich reaction; Heating; | 97% |
With hydrogenchloride In ethanol; water Mannich reaction; Reflux; | 24% |
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol for 14h; Mannich reaction; Heating; | 97% |
2-phenylethylamine hydrochloride
Conditions | Yield |
---|---|
With sodium 2-ethylhexanoic acid In tetrahydrofuran at 20℃; for 144h; | 96% |
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol for 16h; Mannich reaction; Heating; | 96% |
In isopropyl alcohol Mannich reaction; Heating; Acidic conditions; | 35% |
Conditions | Yield |
---|---|
Stage #1: benzoic acid With 1,1'-carbonyldiimidazole In neat (no solvent) for 0.0833333h; Milling; Stage #2: 2-phenylethylamine hydrochloride In neat (no solvent) for 0.166667h; Milling; | 96% |
Stage #1: benzoic acid With 1,1'-carbonyldiimidazole for 0.0833333h; Milling; Green chemistry; Stage #2: 2-phenylethylamine hydrochloride for 0.166667h; Milling; Green chemistry; | 96% |
2-chloropyridine
trifluoromethylsulfonic anhydride
4-trifluoromethylbenzoic acid
2-phenylethylamine hydrochloride
1-(4-(trifluoromethyl)phenyl)-1,2,3,4-tetrahydroisoquinoline
Conditions | Yield |
---|---|
Stage #1: 4-trifluoromethylbenzoic acid; 2-phenylethylamine hydrochloride With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane for 17h; Stage #2: 2-chloropyridine; trifluoromethylsulfonic anhydride at -78 - 20℃; for 37h; Stage #3: With sodium tetrahydroborate In methanol at 20℃; for 13h; | 96% |
2-oxo-4-phenylbutyric acid
2-phenylethylamine hydrochloride
N-phenethyl-3-phenylpropanamide
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide In water; acetonitrile at 20℃; for 1h; Reagent/catalyst; Sealed tube; Darkness; chemoselective reaction; | 96% |
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol for 7h; Mannich reaction; Heating; | 95% |
With hydrogenchloride In ethanol; water Mannich reaction; Reflux; | 18% |
2-phenylethylamine hydrochloride
Conditions | Yield |
---|---|
In chloroform at 25℃; for 24h; | 95% |
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol for 13h; Mannich reaction; Heating; | 94% |
Stage #1: 2-phenylethylamine hydrochloride; 1-(4-methoxyphenyl)ethanone In ethanol Mannich reaction; Heating; Stage #2: formaldehyd In ethanol; water for 9h; Mannich reaction; Heating; Stage #3: With hydrogenchloride In diethyl ether |
potassium cyanide
2-phenylethylamine hydrochloride
3,7-dimethyl-3,7-diazabicyclo[3.3.1]nonan-9-one
3,7-dimethyl-9-phenethylamino-3,7-diazabicyclo<3.3.1>nonane-9-carbonitrile
Conditions | Yield |
---|---|
In methanol; water for 72h; Ambient temperature; | 93% |
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol for 19h; Mannich reaction; Heating; | 93% |
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol for 7h; Mannich reaction; Heating; | 93% |
formaldehyd
2-phenylethylamine hydrochloride
1-(2,4-dichlorophenyl)ethan-1-one
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol for 26h; Mannich reaction; Heating; | 91% |
2-phenylethylamine hydrochloride
acetyl chloride
methyl-N-(benzyl-methyl)-formamide
Conditions | Yield |
---|---|
Stage #1: 2-phenylethylamine hydrochloride With triethylamine In dichloromethane for 0.5h; Stage #2: acetyl chloride In dichloromethane at 0 - 20℃; for 18.5h; | 90% |
With sodium hydroxide In dichloromethane for 3h; | 65% |
2-phenylethylamine hydrochloride
2,5-di-O-acetyl-3-azido-1-(6-chloropurin-9-yl)-β-D-1,3-dideoxyribofuranose
Conditions | Yield |
---|---|
With triethylamine In ethanol at 50℃; | 90% |
Conditions | Yield |
---|---|
In hydrogenchloride; water 80°C; cooling (room temp.), pptn., filtn., washing (aq. HCl), recrystn. (aq. HCl); elem. anal.; | 89% |
Conditions | Yield |
---|---|
With copper(l) iodide; calcium carbonate In water; acetonitrile at 40℃; for 6h; | 88% |
Stage #1: benzaldehyde With 1-hydroxy-pyrrolidine-2,5-dione; oxygen; cobalt(II) diacetate tetrahydrate; sodium hydrogencarbonate In acetonitrile at 20℃; under 760.051 Torr; for 1h; Molecular sieve; Stage #2: 2-phenylethylamine hydrochloride In acetonitrile at 20℃; Molecular sieve; | 80% |
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol for 12h; Mannich reaction; Heating; | 87% |
6-chloro-9-((3aR,3bR,4aS,5R,5aS)-hexahydro-2,2dimethylbicyclo[3.1.0]hex-1(5)-eno[3,2-d] [1,3]dioxol-5-yl)-2-iodo-9H-purine
2-phenylethylamine hydrochloride
(1R,2R,3S,4R,5S)-4-(2-iodo-6-(2-phenylethylamino)-9H-purin-9-yl)-2',3'-O-(isopropylidene)bicyclo[3.1.0]hexane
Conditions | Yield |
---|---|
With triethylamine In methanol at 20℃; Inert atmosphere; | 84% |
Conditions | Yield |
---|---|
Stage #1: N-Cbz-L-Phe With chloroformic acid ethyl ester; triethylamine In tetrahydrofuran at 0℃; for 0.5h; Stage #2: 2-phenylethylamine hydrochloride In tetrahydrofuran; water at 0℃; for 0.5h; | 84% |
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