Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
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4-Tolyl ether CAS 1579-40-4 p-Tolyl Ether CAS no 1579-40-4 Di-p-tolyl ether 4-Tolyl ether Manufacturer High quality Best price In stock factory CAS 1579-40-4 4-Tolyl ether COA TDS price MSDS highly quality and immedaite delivery 4-Tol
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inquiry4-Tolyl ether Basic information Product Name: 4-Tolyl ether Synonyms: 1,1’-oxybis(4-methyl-benzen;1,1’-oxybis(4-methylbenzene);1,1’-oxybis[4-methy
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inquiry4-Tolyl ether CAS:1579-40-4 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediat
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
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inquiryChemical Names: p-Tolyl ether, 4,4'-Dimethyldiphenyl ether Chemical Structure: Molecular Formula: C14H14O CAS: 1579-40-4 Pr
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inquiryProduct Name: 4-Tolyl ether Synonyms: 1,1’-oxybis(4-methyl-benzen;1,1’-oxybis(4-methylbenzene);1,1’-oxybis[4-methyl-benzen;Benzene, 1,1'-oxybis*4-methyl-;Benzene, 1,1'-oxybis[4-methyl-;Bis(4-methylphenyl) ether;bis(4-m
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inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
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Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
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Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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Specifications CAS No.: 1579-40-4 Other Names: 4-Tolyl ether MF: C14H14O EINECS No.: 216-423-0 Place of Origin: Shandong, China (Mainland) Grade Standard: Agriculture Grade, Electron Grade, Food Grade, Industrial Grade, Medicine Grade, Re
Cas:1579-40-4
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inquirygood quality, competitive price, thoughtful after sale serviceAppearance:White to Off-White Solid Storage:Keep it in dry,shady and cool place Package:as your requirement Application:Pharma;Industry;Agricultural;chemical reaserch Transportation:by Sea
4-Tolyl ether cas 1579-40-4Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Conditions | Yield |
---|---|
With copper diacetate; water; triethylamine In dichloromethane; acetonitrile at 25℃; for 6h; | 97% |
Multi-step reaction with 2 steps 1: 85 percent / H2O2 / H2O / 20 °C 2: molecular sieves 4 Angstroem; Cu(OAc)2; Et3N / CH2Cl2 / 20 °C View Scheme |
Conditions | Yield |
---|---|
With aluminum oxide; potassium fluoride; copper(l) iodide In toluene at 100 - 110℃; for 22h; | 95% |
With caesium carbonate In N,N-dimethyl-formamide at 130℃; for 24h; Ullmann Condensation; | 90% |
With potassium phosphate; copper(l) iodide; tetrabutylammomium bromide In N,N-dimethyl-formamide for 22h; Ullmann coupling; Heating; | 87% |
p-cresol
2,4-dimethoxyphenyl(4-methylphenyl)iodonium tosylate
1,1'-oxybis(4-methyl-benzene)
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 50℃; for 6h; regioselective reaction; | 93% |
Conditions | Yield |
---|---|
With potassium phosphate In N,N-dimethyl-formamide at 80℃; for 4h; Ullmann Condensation; | 90% |
With potassium carbonate In water for 2.41667h; Ullmann Condensation; Reflux; Green chemistry; | 87% |
With potassium phosphate; 2-((o-toluidino)methyl)phenol; copper(l) chloride In acetonitrile at 81℃; for 24h; Catalytic behavior; Ullmann Condensation; Schlenk technique; Inert atmosphere; | 85% |
Conditions | Yield |
---|---|
With potassium phosphate; copper(l) iodide; 2,2,6,6-tetramethylheptane-3,5-dione; water In ethanol at 130℃; for 30h; Inert atmosphere; Sealed tube; chemoselective reaction; | 90% |
Multi-step reaction with 2 steps 1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 h / 20 °C 2: sodium hydroxide / dichloromethane / 22 h / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 h / 20 °C 2: sodium hydroxide; piperidine / dichloromethane / 14 h / 40 °C View Scheme |
Conditions | Yield |
---|---|
With potassium tert-butylate In tetrahydrofuran at 40℃; | 88% |
para-bromotoluene
tert-Butyl(dimethyl)-(4-methylphenoxy)silane
1,1'-oxybis(4-methyl-benzene)
Conditions | Yield |
---|---|
With copper(l) iodide; caesium carbonate In N,N-dimethyl-formamide at 100℃; for 8h; | 81% |
Conditions | Yield |
---|---|
With potassium phosphate; tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium(0) In 1,4-dioxane at 100℃; for 20h; | 78% |
Conditions | Yield |
---|---|
With potassium phosphate; tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium(0) In 1,4-dioxane at 100℃; for 20h; | 72% |
piperazine
para-bromotoluene
A
p-cresol
B
1,4-bis(4-methylphenyl)piperazine
C
toluene
D
1,1'-oxybis(4-methyl-benzene)
Conditions | Yield |
---|---|
With Adipic acid; N'-phenyloxalyl bishydrazide; copper diacetate; sodium acetate; cetyltrimethylammonim bromide; 2,5-hexanedione; potassium hydroxide In water at 100℃; for 3h; Inert atmosphere; | A 21 %Chromat. B 68% C 13 %Chromat. D 11 %Chromat. |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 100℃; for 24h; | 65% |
Conditions | Yield |
---|---|
Stage #1: para-chlorotoluene With potassium phosphate; N,N'-bis(2,5-dimethylpyrrol-1-yl)oxalamide; copper(I) bromide In dimethyl sulfoxide at 20℃; Inert atmosphere; Sealed tube; Glovebox; Stage #2: p-cresol In dimethyl sulfoxide at 120℃; for 24h; Sealed tube; Inert atmosphere; Glovebox; | 62% |
para-bromotoluene
diethylamine
A
p-cresol
B
N,N-diethyl-p-toluidine
C
toluene
D
1,1'-oxybis(4-methyl-benzene)
Conditions | Yield |
---|---|
With Adipic acid; N'-phenyloxalyl bishydrazide; copper diacetate; sodium acetate; cetyltrimethylammonim bromide; 2,5-hexanedione; potassium hydroxide In water at 100℃; for 3h; Inert atmosphere; | A 18 %Chromat. B 28% C 5 %Chromat. D 26 %Chromat. |
1,1'-oxybis(4-methyl-benzene)
Conditions | Yield |
---|---|
With piperidine; sodium hydroxide In dichloromethane at 40℃; for 14h; | 11% |
furan
A
1,4-dihydro-1,4-epoxy-6-methylnaphthalene
B
1,1'-oxybis(4-methyl-benzene)
Conditions | Yield |
---|---|
With sodium hydroxide In dichloromethane at 20℃; for 22h; Diels-Alder Cycloaddition; | A 11% B 11% |
p-cresol
carvacrol
A
(5-isopropyl-2-methyl-phenyl)-p-tolyl ether
B
1,1'-oxybis(4-methyl-benzene)
Conditions | Yield |
---|---|
at 440 - 450℃; |
Conditions | Yield |
---|---|
at 400℃; durch Ueberleiten ueber ThO2; | |
at 400℃; beim Ueberleiten ueber ThO2; | |
With copper diacetate; 4 A molecular sieve; triethylamine In dichloromethane at 20℃; |
Conditions | Yield |
---|---|
With p-cresol; copper at 200 - 240℃; |
2-(5-methyl-2-p-tolyloxy-benzoyl)-benzoic acid
A
benzene-1,2-dicarboxylic acid
B
1,1'-oxybis(4-methyl-benzene)
Conditions | Yield |
---|---|
in der Kalischmelze; |
aluminium tris(p-methylphenoxide)
A
p-cresol
B
2,7-dimethyl-xanthene
C
1,1'-oxybis(4-methyl-benzene)
Conditions | Yield |
---|---|
bei der trocknen Destillation; |
p-cresol
p-toluidine
A
4-Methyl-2-p-tolyl-phenol
B
1,1'-oxybis(4-methyl-benzene)
Conditions | Yield |
---|---|
With sulfuric acid at 95℃; Diazotization; |
tris(4-methylphenyl)sulfonium bromide
A
di-(p-tolyl)sulfane
B
toluene
C
1,1'-oxybis(4-methyl-benzene)
Conditions | Yield |
---|---|
With sodium isopropylate In isopropyl alcohol at 72℃; for 23h; Product distribution; Mechanism; var. of solvent, reagent, temp., time; D-incorporation into toluene; | A 100 % Chromat. B 33 % Chromat. C 35 % Chromat. |
Conditions | Yield |
---|---|
With copper(II) sulfate; acetic acid; zinc |
potassium p-cresolate
bis(4-methylphenyl)iodonium bromide
1,1'-oxybis(4-methyl-benzene)
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide |
Conditions | Yield |
---|---|
With potassium hydroxide at 150 - 160℃; |
para-bromotoluene
sodium 4-methylphenoxide
1,1'-oxybis(4-methyl-benzene)
Conditions | Yield |
---|---|
With copper(I) oxide In N,N-dimethyl acetamide at 166℃; |
Conditions | Yield |
---|---|
With copper diacetate; sodium hydride In dichloromethane 1.) r.t., 10 min, 2.) 50 deg C, 16 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; |
Conditions | Yield |
---|---|
With 3-Methylindole; copper diacetate; sodium hydride In dichloromethane 1.) r.t., 10 min, 2.) 50 deg C, 16 h; Yield given. Yields of byproduct given; |
methanol
A
4-Methylanisole
B
1-methoxy-3-methyl-benzene
C
1,1'-oxybis(4-methyl-benzene)
Conditions | Yield |
---|---|
With sodium hydroxide In water for 10h; Heating; Yield given. Title compound not separated from byproducts; |
1,1'-oxybis(4-methyl-benzene)
2,8-Dimethyl-5-hydroxy-5-oxo-Pv-dibenzo<1,4>oxaphosphorin
Conditions | Yield |
---|---|
Stage #1: 1,1'-oxybis(4-methyl-benzene) With aluminium trichloride; phosphorus trichloride Heating; Stage #2: With sodium hydroxide; dihydrogen peroxide In water for 0.25h; | 97.2% |
Multi-step reaction with 3 steps 1: phosphorus trichloride; aluminium trichloride / 22 h / 80 °C 2: 10.2 g / H2O / 0 °C 3: 92 percent / O2; KOH / H2O View Scheme | |
Multi-step reaction with 2 steps 1: PCl3, AlCl3 2: aq. Br2 View Scheme |
phenylphosphinic acid
1,1'-oxybis(4-methyl-benzene)
2,8-dimethyl-10-phenylphenoxaphosphinine 10-oxide
Conditions | Yield |
---|---|
With dmap; trifluoromethylsulfonic anhydride In cis-1,2-Dichloroethylene at 120℃; for 16h; Schlenk technique; Inert atmosphere; | 94% |
1,1'-oxybis(4-methyl-benzene)
methyl cyclohexane
Conditions | Yield |
---|---|
With platinum on activated charcoal; N-methyldiethanolamine trifluoromethanesulfonate; hydrogen at 150℃; under 7500.75 Torr; for 6h; Autoclave; | 93.2% |
With carbon nanotubes-supported ruthenium; hydrogen In dodecane; water at 220℃; under 37503.8 Torr; for 3h; Autoclave; | 89 %Chromat. |
With hydrogen at 130℃; under 15001.5 Torr; for 6h; Ionic liquid; Autoclave; Schlenk technique; | 94.3 %Chromat. |
With hydrogen In decalin at 200℃; under 75007.5 Torr; for 3h; |
Conditions | Yield |
---|---|
With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) In tetrachloromethane at 80 - 90℃; for 6.5h; Inert atmosphere; | 93% |
With bromine; ethylene dibromide; dibenzoyl peroxide Irradiation.Sonnenlicht; | |
With N-Bromosuccinimide; dibenzoyl peroxide | |
With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) In tetrachloromethane at 80℃; | |
With hydrogen bromide; dihydrogen peroxide In 1,2-dichloro-ethane for 12h; Cooling with ice; Irradiation; |
Conditions | Yield |
---|---|
With dihydrogen peroxide; sodium carbonate at 100℃; under 7500.75 Torr; for 18h; Reagent/catalyst; Pressure; | 93% |
With pyridine; cobalt(III) acetylacetonate; dihydrogen peroxide; sodium carbonate In acetic acid at 100℃; under 15001.5 Torr; for 6h; Reagent/catalyst; Temperature; Solvent; Pressure; | 92% |
With 2-chloroanthracene-9,10-dione; water; oxygen; trifluoroacetic acid In ethyl acetate for 72h; Irradiation; | 70% |
1,1'-oxybis(4-methyl-benzene)
2,8-dimethyl-10,10-dichlorophenoxatellurine
Conditions | Yield |
---|---|
With tellurium tetrachloride at 200℃; for 4h; | 93% |
sodium methylate
1,1'-oxybis(4-methyl-benzene)
4,4'-Bis-methoxymethyl diphenyl ether
Conditions | Yield |
---|---|
Stage #1: 1,1'-oxybis(4-methyl-benzene) With 2,2'-azobis(isobutyronitrile); bromine In benzene at 80℃; for 3h; Reflux; Stage #2: sodium methylate In methanol at 45℃; for 2h; Temperature; Reflux; | 92.8% |
Conditions | Yield |
---|---|
Stage #1: 1,1'-oxybis(4-methyl-benzene) With 2,2'-azobis(isobutyronitrile); bromine In tetrachloromethane at 80℃; for 4.1h; Reflux; Stage #2: sodium isopropylate In isopropyl alcohol at 50℃; for 3h; Reflux; | 92.8% |
benzoic acid
1,1'-oxybis(4-methyl-benzene)
2, 7-dimethyl-9-phenyl xanthen-9-ol
Conditions | Yield |
---|---|
With trichlorophosphate; zinc(II) chloride at 95℃; for 2h; Product distribution / selectivity; Friedel Crafts Reaction; | 91.8% |
With zinc(II) chloride; trichlorophosphate at 95℃; for 4h; | 66% |
With zinc(II) chloride; trichlorophosphate at 80 - 95℃; | |
With zinc(II) chloride; trichlorophosphate at 95℃; for 4h; |
sodium ethanolate
1,1'-oxybis(4-methyl-benzene)
4,4'-diethoxymethyldiphenyl ether
Conditions | Yield |
---|---|
Stage #1: 1,1'-oxybis(4-methyl-benzene) With 2,2'-azobis(isobutyronitrile); bromine In tetrachloromethane at 80℃; for 3.2h; Reflux; Stage #2: sodium ethanolate In ethanol at 46℃; for 2h; Reflux; | 91.2% |
oxalyl dichloride
1,1'-oxybis(4-methyl-benzene)
2,7-dimethylxanthen-9-one
Conditions | Yield |
---|---|
With aluminium trichloride In carbon disulfide at 0 - 20℃; for 18h; | 90% |
With aluminum (III) chloride In dichloromethane at 0℃; Friedel Crafts reaction; Inert atmosphere; Reflux; | 77% |
With carbon disulfide; aluminium trichloride |
benzoyl chloride
1,1'-oxybis(4-methyl-benzene)
2-<(p-methylphenyl)oxy>-5-methylbenzophenone
Conditions | Yield |
---|---|
With aluminium trichloride In carbon disulfide at 0℃; for 3h; | 90% |
Conditions | Yield |
---|---|
With hydrogenchloride; oxygen; 9-(2-mesityl)-10-methylacridinium perchlorate at 20℃; under 760.051 Torr; for 30h; Schlenk technique; Irradiation; Green chemistry; | 90% |
With 2,3-dicarboxyanthraquinone; oxygen for 48h; Irradiation; | 80% |
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride; iron(III)-acetylacetonate; sodium t-butanolate In toluene at 140℃; for 24h; Inert atmosphere; | 88% |
Conditions | Yield |
---|---|
With sodium persulfate; copper diacetate; iron(II) sulfate; dimethyl sulfoxide In water; acetonitrile at 75℃; for 0.75h; | 87% |
With sodium persulfate; dimethylsulfide; copper diacetate; iron(II) sulfate In water; acetonitrile at 75℃; for 1.08333h; | 84% |
With sodium persulfate; racemic methyl phenyl sulfoxide; copper diacetate; iron(II) sulfate In water; acetonitrile at 75℃; for 0.75h; | 84% |
Multi-step reaction with 2 steps 1: 1,2-dibromo-ethane; dibenzoyl peroxide; bromine / Irradiation.Sonnenlicht 2: CHCl3 / Erhitzen des Reaktionsprodukts mit wss. Essigsaeure und anschliessend mit wss. HCl View Scheme |
1,1'-oxybis(4-methyl-benzene)
4-nitro-benzoic acid
2,7-dimethyl-9-(4-nitrophenyl)-xanthen-9-ol
Conditions | Yield |
---|---|
With zinc(II) chloride; trichlorophosphate at 95℃; for 4h; | 86% |
Conditions | Yield |
---|---|
With zinc(II) chloride; trichlorophosphate In neat (no solvent) at 100℃; for 24h; Inert atmosphere; | 85% |
1,1'-oxybis(4-methyl-benzene)
4-(4'-methylphenoxy)benzonitrile
Conditions | Yield |
---|---|
With sodium azide; copper(ll) sulfate pentahydrate; [bis(acetoxy)iodo]benzene In acetonitrile at -40 - 25℃; Inert atmosphere; | 83% |
Conditions | Yield |
---|---|
With oxygen; palladium diacetate at 55℃; | 82% |
With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; copper dichloride 1.) Et2O, cyclohexane, RT, 16 h, 2.) Et2O, cyclohexane, 5 deg C, 3 h; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
With sodium tetrahydroborate; 10 wt% Pd(OH)2 on carbon; ammonia In water; m-xylene at 150℃; for 24h; Inert atmosphere; Sealed tube; | A 82% B n/a C 88 %Chromat. |
4-(1,1-dimethylethyl)benzoic acid
1,1'-oxybis(4-methyl-benzene)
2,7-dimethyl-9-(4-t-butyl)phenylxanthene-9-ol
Conditions | Yield |
---|---|
With trichlorophosphate; zinc(II) chloride for 2h; Friedel Crafts Reaction; | 81% |
With zinc(II) chloride; trichlorophosphate at 95℃; for 4h; | 70% |
ammonium formate
1,1'-oxybis(4-methyl-benzene)
2,7-dimethylxanthen-9-one
Conditions | Yield |
---|---|
With dipotassium peroxodisulfate; sulfuric acid; palladium diacetate; trifluoroacetic acid at 45℃; | 80% |
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