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inquiry1-phenylpropane-1,2-diol CAS:1855-09-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic i
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
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inquiry1,we produce and sell good chemicals around the world.2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%.3,our staff consists of highly qualified in
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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inquiryWe product this chemical more than 10 years . We are very experience to export it to many countries, Our superior & stable quality , competitive price gain warm reception from our customers. Application:intermediate
1-phenylpropane-1,2-diol Application:1-phenylpropane-1,2-diol
1,2-Dihydroxy-1-phenylpropaneAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:pharmaceutical intermediate Transportation:by air, by sea, by express
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
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inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highl
Conditions | Yield |
---|---|
With osmium(VIII) oxide; cinchona alkaloid on mesoporous SBA-15 silica support at 0℃; for 24h; | 100% |
With 4-methylmorpholine N-oxide; Mg(1-x)Al(x)(OH)2(Cl)2*zH2O-OsO4 In water; acetone; acetonitrile at 20℃; | 96% |
With 4-methylmorpholine N-oxide In water; acetone at 20℃; for 2h; Inert atmosphere; | 96% |
Conditions | Yield |
---|---|
With sodium tetrahydroborate In ethanol at 0℃; for 1h; Inert atmosphere; | 95% |
With hydrogen; cinchonidine; acetic acid In water at 20℃; under 5171.62 Torr; Autoclave; | |
With rabbit 3-hydroxyhexobarbital dehydrogenase (AKR1C29); NADPH In aq. phosphate buffer; ethyl acetate at 37℃; for 0.5h; pH=7.4; Catalytic behavior; Kinetics; Enzymatic reaction; | |
With sodium tetrahydroborate In tetrahydrofuran; water at 20℃; |
Conditions | Yield |
---|---|
With oxygen; 4-methylmorpholine N-oxide In water; acetone at 25℃; for 2h; | 94% |
With osmium(VIII) oxide; 4-methylmorpholine N-oxide In water; acetone at 20℃; for 3h; | 81% |
With seleno-L-cystine; water; dihydrogen peroxide at 20℃; for 168h; Optical yield = 32 %de; stereoselective reaction; | 45% |
With Hydroquinone 1,4-phthalazinediyl diether; methanesulfonamide; potassium carbonate; potassium hexacyanoferrate(III); OsO4 immobilized on Amberlite XAD-4 In water; tert-butyl alcohol at 20℃; for 1.5h; | |
With dihydrogen peroxide; nitric acid; potassium iodide In water; acetonitrile at 24.84℃; under 760.051 Torr; for 4h; pH=Ca. 4; |
1-<<(1,1-dimethylethyl)dimethylsilyl>oxy>-1-phenyl-2-propanone
1-phenyl-1,2-propandiol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran for 1h; Heating; | 90% |
1-Phenylpropane-1,2-dione
A
3-phenyl-2-propanol
B
1-Phenyl-1-propanol
C
1-phenyl-1,2-propandiol
D
1-phenyl-propan-1-one
Conditions | Yield |
---|---|
With samarium diiodide; water In tetrahydrofuran at 20℃; for 0.166667h; Further byproducts given; | A 6% B 79% C 3% D 7% |
(E)-1-Bromo-2-butene
benzaldehyde
A
1-phenyl-1,2-propandiol
B
2-methyl-1-phenyl-3-butene-1-ol
Conditions | Yield |
---|---|
bis(cyclopentadienyl)titanium (III) chloride In tetrahydrofuran at 20℃; for 1.5h; | A 17% B 77% |
cis-1-phenyl-1-propylene
A
1-phenyl-1,2-propandiol
D
1-phenylpropylene oxide
Conditions | Yield |
---|---|
With [Fe(CF3SO3)2((S,S)-N,N’-bis(2-pyridylmethyl)-2,2’-bipyrrolidine)]; dihydrogen peroxide; 18O-labeled water In acetonitrile at 0℃; for 3h; Catalytic behavior; | A 32% B 15% C 68% D n/a |
acetone
1-phenylpropylene oxide
A
1-phenyl-1,2-propandiol
B
2,2,5-trimethyl-4-phenyl-1,3-dioxolane
Conditions | Yield |
---|---|
With Amberlyst 15 at 20℃; for 12h; | A 34% B 66% |
Conditions | Yield |
---|---|
Stage #1: allylbenzene With sodium hydrogencarbonate; 9-(2-mesityl)-10-methylacridinium perchlorate In acetonitrile at 20℃; for 6h; Irradiation; Stage #2: With triphenylphosphine In acetonitrile at 20℃; for 3h; | 66% |
1-propenylbenzene
A
1-phenyl-1,2-propandiol
B
benzaldehyde
C
1-phenyl-propan-1-one
D
benzoic acid
E
1-phenyl-acetone
1-phenylpropylene oxide
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); oxygen In chlorobenzene at 120℃; under 759.8 Torr; Product distribution; Mechanism; | A 3.4% B 26.9% C 3.2% D 2.9% E 0.8% F 55.1% |
cis-1-phenyl-1-propylene
A
1-phenyl-1,2-propandiol
C
1-phenylpropylene oxide
Conditions | Yield |
---|---|
With [Fe(CF3SO3)2((S,S)-N,N’-bis(2-pyridylmethyl)-2,2’-bipyrrolidine)]; 18O-labeled water; 3-chloro-benzenecarboperoxoic acid In acetonitrile at 0℃; for 3h; Catalytic behavior; | A 53% B 47% C n/a |
1-propenylbenzene
A
1-phenyl-1,2-propandiol
B
benzaldehyde
C
1-phenyl-propan-1-one
D
benzoic acid
1-phenylpropylene oxide
cis-1-phenylpropene oxide
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); oxygen In chlorobenzene at 100℃; under 759.8 Torr; Product distribution; Mechanism; | A 2.7% B 26.4% C 2.9% D 3.2% E 52.1% F 0.4% |
ethanol
benzaldehyde
A
1-phenyl-1,2-propandiol
B
1,2-diphenyl-1,2-ethanediol
Conditions | Yield |
---|---|
at 20℃; for 3h; pinacol coupling; | A 51% B 49% |
acetic acid 1-methyl-2-oxo-2-phenyl-ethyl ester
A
1-phenyl-1,2-propandiol
B
(R)-2-hydroxy-1-phenylpropan-1-one
C
(R)-1-oxo-1-phenylpropan-2-yl acetate
Conditions | Yield |
---|---|
With ammonium sulfate; D-glucose; Rhizopus oryzae NRRL 395; magnesium sulfate; zinc(II) sulfate In phosphate buffer; dimethyl sulfoxide at 30℃; for 60h; pH=6.0 - 6.5; | A n/a B 42% C n/a |
cis-1-phenyl-1-propylene
A
1-phenyl-1,2-propandiol
B
benzaldehyde
C
benzoic acid
D
1-phenyl-acetone
1-phenylpropylene oxide
cis-1-phenylpropene oxide
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); oxygen; chlorobenzene at 80℃; under 759.8 Torr; Product distribution; Mechanism; other temperature; | A 2.1% B 38.7% C 6.3% D 3.5% E 33.1% F 1.8% |
cis-1-phenyl-1-propylene
A
1-phenyl-1,2-propandiol
B
benzaldehyde
C
1-phenyl-propan-1-one
D
benzoic acid
E
1-phenyl-acetone
1-phenylpropylene oxide
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); oxygen In chlorobenzene at 120℃; under 759.8 Torr; Product distribution; Mechanism; | A 2.2% B 24.5% C 1.8% D 4% E 7.4% F 32.4% |
(1-bromoethyl)benzyl bromide
potassium acetate
acetic acid
A
1-phenylpropene
B
1-phenyl-1,2-propandiol
Conditions | Yield |
---|---|
Verseifen des Reaktionsgemisches mit alkoh. Kalilauge; |
methyl magnesium iodide
1-phenyl-2-hydroxyethanone
A
1-phenyl-1,2-propandiol
B
2,5-dimethyl-2,5-diphenyl-[1,4]dioxane
Conditions | Yield |
---|---|
With diethyl ether Zersetzung des Reaktionsprodukts mit Wasser und Essigsaeure; | |
Reagiert analog mit Aethylmagnesiumjodid; |
3-monochloro-1,2-propanediol
A
3-phenylpropane-1,2-diol
B
1-phenyl-1,2-propandiol
2,2-dichloro-1-phenylpropan-1-one
1-phenyl-1,2-propandiol
Conditions | Yield |
---|---|
With sodium hydroxide; nickel |
Conditions | Yield |
---|---|
With sodium tetrahydroborate |
Conditions | Yield |
---|---|
With dihydrogen peroxide; sodium hydrogencarbonate; dihydrogen hexachloroplatinate Yield given. Multistep reaction. Yields of byproduct given; |
Conditions | Yield |
---|---|
With water Product distribution; enantioselectivity and regioselectivity by cytosolic and microsomal epoxide hydrolase; |
(+)-(R,R)-β-methylstyrene oxide
1-phenyl-1,2-propandiol
Conditions | Yield |
---|---|
With water Product distribution; enantioselectivity and regioselectivity by cytosolic and microsomal epoxide hydrolase; |
1-Phenylpropane-1,2-dione
A
1-phenyl-1,2-propandiol
B
(S)-2-hydroxypropiophenone
Conditions | Yield |
---|---|
Product distribution; bioreduction with baker's yeast; pH effect; |
1-Phenylpropane-1,2-dione
A
1-Phenyl-1-propanol
B
(RS)-2-phenyl-1-propanol
C
1-phenyl-1,2-propandiol
D
benzyl alcohol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride; oxygen at 110℃; under 759.8 Torr; Product distribution; 1.) oxidation, 2.) reductiv reactions of different α-diketones to different products; |
1-phenylpropene
A
2-hydroxypropiophenone
B
1-phenyl-1,2-propandiol
C
benzaldehyde
Conditions | Yield |
---|---|
With laccase from Trametes versicolor; oxygen; benzotriazol-1-ol In water at 45℃; pH=4.5; |
Conditions | Yield |
---|---|
at 20℃; |
Conditions | Yield |
---|---|
With N-iodo-succinimide; 1,10-Phenanthroline; oxygen; potassium carbonate; copper dichloride In dimethyl sulfoxide at 140℃; under 3750.38 Torr; for 12h; Molecular sieve; | 98% |
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate In dichloromethane at 20℃; for 2h; Inert atmosphere; regioselective reaction; | 97% |
With sulfuric acid at -19℃; | |
With sulfuric acid at 50 - 55℃; |
1-phenyl-1,2-propandiol
Conditions | Yield |
---|---|
With thionyl chloride In tetrachloromethane for 1h; Heating; | 92% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; potassium tert-butylate In water at 80℃; for 8h; | 92% |
With 2-chloroanthracene-9,10-dione; oxygen In ethyl acetate for 30h; Irradiation; | 81% |
Conditions | Yield |
---|---|
Stage #1: 1-phenyl-1,2-propandiol In dichloromethane at 20℃; for 0.5h; Stage #2: 2-Chloro-2-oxo-1,3,2-dioxaphospholane In dichloromethane at 0 - 20℃; for 12h; | 92% |
Conditions | Yield |
---|---|
In dichloromethane at 0 - 20℃; for 12h; | 92% |
Conditions | Yield |
---|---|
With sodium nitrate; water; oxygen In dimethyl sulfoxide at 130℃; for 24h; | A n/a B 90% |
1-phenyl-1,2-propandiol
A
2-hydroxypropiophenone
B
(RS)-1-hydroxy-1-phenylpropan-2-one
Conditions | Yield |
---|---|
With 3,3-dimethyldioxirane In acetone Ambient temperature; | A 85% B n/a |
With 3,3-dimethyldioxirane In acetone Ambient temperature; | |
With NADH‐dependent oxidase from Streptococcus mutans; NAD In aq. phosphate buffer at 40℃; for 24h; pH=6.5; Reagent/catalyst; pH-value; Temperature; Enzymatic reaction; |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; Rh2(Msip)4; sodium hydrogencarbonate In dichloromethane; water at 40℃; for 24h; Sealed tube; chemoselective reaction; | 85% |
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran at 20℃; for 16h; | 77% |
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; dodecacarbonyl-triangulo-triruthenium; 1-Adamantanecarboxylic acid In m-xylene at 130℃; for 20h; Inert atmosphere; Sealed tube; regioselective reaction; | 74% |
Conditions | Yield |
---|---|
With oxygen; cetyltrimethylammonim bromide In water at 20℃; under 760.051 Torr; for 5h; Irradiation; Green chemistry; | 72% |
In water; acetonitrile at 40℃; | |
With sodium periodate; sodium hydrogencarbonate In water; acetonitrile at 20℃; for 1.5h; | |
With Na0274MnO2*6H2O; oxygen In butan-1-ol at 100℃; under 760.051 Torr; for 6h; Green chemistry; | 94 %Chromat. |
Conditions | Yield |
---|---|
With oxone; 2-iodo-3,4,5,6-tetramethylbenzoic acid In water; acetonitrile at 20℃; for 3h; | A 30% B 62% |
Conditions | Yield |
---|---|
With [Ru(CO)2(4,5-bis(diphenylphosphino)-9,9-dimethyl-9H-xanthene)]2; [Ru(CO)2(4,5-bis(diphenylphosphino)-9,9-dimethyl-9H-xanthene)]2; toluene-4-sulfonic acid In tert-Amyl alcohol at 120℃; regioselective reaction; | 61% |
1-phenyl-1,2-propandiol
toluene
A
Benzyl acetate
B
benzoic acid benzyl ester
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide In water; acetonitrile at 80℃; for 24h; Sealed tube; | A 54% B 51% |
1-phenyl-1,2-propandiol
A
(1R,2R)-1-phenylpropane-1,2-diol
B
(1S,2R)-1-phenylpropane-1,2-diol
C
(S)-2-hydroxypropiophenone
Conditions | Yield |
---|---|
With sodium alginate and calcium chloride immobilized Candida parapsilosis ATCC 7330 cell In 2,2,4-trimethylpentane; water; acetone at 25℃; for 72h; stereoselective reaction; | A n/a B 41.59% C 42.34% |
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