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inquiryhigh quality Appearance:Colorless liquid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
1,6-Dichlorohexane Appearance: Colorless liquid Melting point: -13℃ Boiling point: 204°C at 760 mmHg Flash point: 73.9°C Our Server 1. Compe
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inquiryProduct Description Product website: http://www.finerchem.com Product Name 1,6-Dichlorohexane CAS No. 2163-00-0
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inquiryCAS 2163-00-0 Name 1,6-Dichlorohexane Appearance Colorless Liquid Application Pharmaceutical intermediates Appearance: Colorless Liquid Storage:RT. Pa
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inquiry1,6-dichloro-n-hexane CAS:2163-00-0 Specification mp -13 °c bp 87-90 °c15 mm hg(lit.) density 1.068 g/ml at 25 °c(lit.) refractive index n20/d 1.457(lit.) fp 165 °f
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A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiry1,6-Dichlorohexane/high quality/best priceAppearance:clear colorless liquid Storage:Store in dry, dark and ventilated place Package:according to customers' requirements Application:Fine Intermediate Transportation:By air(EMS or EUB or FedEx or TNT ec
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inquirySuperior quality, moderate price & quick delivery. Appearance:colourless liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical Intermediat
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inquiryProduct name: 1,6-Dichlorohexane CAS No.: 2163-00-0 Molecule Formula:C6H12Cl2 Molecule Weight:155.07 Purity: 99.0% Package: 200kg/drum Description:Colorless transparent liquid Manufacture Standards:Enterprise Standard TESTING ITE
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inquiry1,6-Dichlorohexane Basic information Product Name: 1,6-Dichlorohexane Synonyms: HEXAMETHYLENE CHLORIDE;HEXAMETHYLENE DICHLORIDE;1,6-Dichlorohexane,97%;1,6-DICHLOROHEXANE 98+%;1,6-Dichlorohexane, 98% 100GR;1,6-dichloro-n-hexane;Hexamethylene Ch
Conditions | Yield |
---|---|
Stage #1: 1,6-hexanediol With N,N-dimethylthiourea In dichloromethane at 20℃; Stage #2: With N-chloro-succinimide In dichloromethane at 20℃; for 1h; Irradiation; | 98% |
With hydrogenchloride; ammonium chloride In water at 50 - 110℃; for 3h; Reagent/catalyst; | 96% |
With thionyl chloride; Triphenylphosphine oxide at 20 - 80℃; for 3h; | 87% |
Conditions | Yield |
---|---|
With hexabutylguanidinium chloride at 120℃; for 4h; | 93% |
3-(phenylsulfonyl)propyl chloride
A
1-Chloropropane
B
(cyclopropylsulfonyl)benzene
C
1,6-dichlorohexane
Conditions | Yield |
---|---|
With sodium amalgam In benzene for 6h; Heating; | A 17% B 53% C 13% |
Conditions | Yield |
---|---|
With tetrachloromethane; triphenylphosphine In acetonitrile Product distribution; Mechanism; | A 48% B 39% |
With hydrogenchloride at 92 - 96℃; | |
With hydrogenchloride |
Conditions | Yield |
---|---|
With nitrosylchloride |
Conditions | Yield |
---|---|
With phosphorus pentachloride Destillieren der erhaeltlichen Verbindung; |
1-Chlorohexane
A
1,5-dichloro-hexane
B
1,3-dichlorohexane
C
1,4-dichlorohexane
D
1,6-dichlorohexane
Conditions | Yield |
---|---|
With chlorine Further byproducts given; | |
With sulfuryl dichloride; dibenzoyl peroxide at 90℃; Further byproducts given; | |
With sulfuryl dichloride; dibenzoyl peroxide Further byproducts given; |
1-Chlorohexane
A
1,5-dichloro-hexane
B
1,2-dichlorohexane
C
1,3-dichlorohexane
D
1,4-dichlorohexane
E
1,1-dichloro-n-hexane
F
1,6-dichlorohexane
Conditions | Yield |
---|---|
With N-chloropiperidine; 2,2'-azobis(isobutyronitrile) In trifluoroacetic acid at 30℃; Product distribution; Rate constant; Irradiation; relative rate constants, position selectivity, substrate selectivity; | |
With chlorine In benzene at -10.1℃; Product distribution; dependence of the selectivity of chlorination on the conc. of benzene; | |
With N-chloropiperidine; 2,2'-azobis(isobutyronitrile) In trifluoroacetic acid at 30℃; for 3h; Product distribution; Rate constant; Irradiation; other objects - relative reactivities and relative rate constants for the various positions of chlorination; |
Conditions | Yield |
---|---|
With aluminium trichloride at 154℃; for 1h; Product distribution; Mechanism; var. temp.; | A 29 % Chromat. B 4 % Chromat. |
N-benzoyl-1H-hexahydroazepine
phosphorus pentachloride
1,6-dichlorohexane
Conditions | Yield |
---|---|
folgend Destillieren; |
1,6-dichlorohexane
Conditions | Yield |
---|---|
With hydrogenchloride at 165 - 175℃; |
1,6-dichlorohexane
Conditions | Yield |
---|---|
With phosphorus pentachloride |
1,6-Hexanediamine
diethyl ether
A
1,5-dichloro-hexane
B
1,6-dichlorohexane
hydrogenchloride
1,6-hexanediol
A
6-chloro-1-hexanol
B
1,6-dichlorohexane
Conditions | Yield |
---|---|
unter kontinuierlicher Extraktion mit Toluol; |
hydrogenchloride
1,6-hexanediol
A
6-chloro-1-hexanol
B
1,13-dichloro-7-oxatridecane
C
13-chloro-7-oxatridecane-1-ol
D
1,6-dichlorohexane
Conditions | Yield |
---|---|
at 92 - 96℃; weitere Produkte: 6.6'-Dihydroxy-dihexylaether und Hexamethylenglykol-bis-<6-hydroxy-hexyl>-aether; |
Conditions | Yield |
---|---|
at 165 - 175℃; im geschlossenen Rohr; |
Conditions | Yield |
---|---|
With HBGF at 120℃; for 1.5h; Title compound not separated from byproducts; | A n/a B 57 % Spectr. C n/a |
Conditions | Yield |
---|---|
With lead(IV) acetate; ammonium chloride at 20℃; for 4h; mechanical activation; | 0.92 mmol |
With lead(IV) acetate; ammonium chloride at 20℃; for 6h; mechanical activation; | 0.94 mmol |
Conditions | Yield |
---|---|
With lead(IV) acetate; ammonium chloride at 20℃; for 48h; | A 0.13 mmol B 0.60 mmol |
With lead(IV) acetate; ammonium chloride at 20℃; for 96h; | A 0.11 mmol B 0.44 mmol |
Conditions | Yield |
---|---|
With hydrogenchloride; 1-methylimidazolium chloride at 80 - 135℃; Conversion of starting material; |
1-methylimidazolium chloride
1,6-dichlorohexane
Conditions | Yield |
---|---|
With hydrogenchloride |
Conditions | Yield |
---|---|
In tetrahydrofuran; diethyl ether drop by drop addn. of 1,6-dichlorohexane in THF over 30 min to a (c-C6H11)2SbLi soln. in ether at -45°C; mixt. treated with aq. NH4Cl, evapn. of the ether; | 98.9% |
In tetrahydrofuran; diethyl ether drop by drop addn. of 1,6-dichlorohexane in THF over 30 min to a (c-C6H11)2SbLi soln. in ether at -45°C; mixt. treated with aq. NH4Cl, evapn. of the ether; | 98.9% |
1-(4-vinylbenzyl)-1H-imidazole
1,6-dichlorohexane
Conditions | Yield |
---|---|
In acetonitrile at 80℃; for 12h; Inert atmosphere; Schlenk technique; | 98% |
Conditions | Yield |
---|---|
With calcium chloride In acetonitrile for 48h; Reflux; | 97% |
In acetonitrile at 20℃; for 24h; Reflux; | 87% |
at 70 - 100℃; for 0.025h; Microwave irradiation; | 82% |
Conditions | Yield |
---|---|
tetrabutylammomium bromide at 115℃; for 1.5h; | 96% |
3-Mercaptopropyltriethoxysilane
1,6-dichlorohexane
Conditions | Yield |
---|---|
Stage #1: 3-Mercaptopropyltriethoxysilane With sodium ethanolate In ethanol at 20℃; for 3h; Reflux; Stage #2: 1,6-dichlorohexane In ethanol at 80℃; for 3.5h; Reflux; | A 95% B 5% |
Conditions | Yield |
---|---|
With tetrabutylammomium bromide; sodium hydroxide for 6h; Reflux; | 93.4% |
1,6-dichlorohexane
Conditions | Yield |
---|---|
With sodium hydroxide; sodium thiosulfate In water for 9h; pH=7.1 - 7.3; Product distribution / selectivity; Heating / reflux; | 93.3% |
With sodium hydroxide; sodium thiosulfate In water for 9h; pH=7.2 - 10.0; Product distribution / selectivity; Heating / reflux; | 93.3% |
With sodium hydroxide; sodium thiosulfate In water for 9h; pH=4.9 - 5.1; Product distribution / selectivity; Heating / reflux; | 91.4% |
1-(2,6-diisopropylphenyl)-1H-imidazole
1,6-dichlorohexane
Conditions | Yield |
---|---|
at 140℃; for 24h; | 93% |
at 140℃; for 6h; neat (no solvent); | 72% |
1,6-dichlorohexane
8-hydroxy-1,1,7,7-tetramethyl-2,3,6,7-tetrahydro-1H,5H-pyrido[3,2,1-ij]quinoline-9-carbaldehyde
Conditions | Yield |
---|---|
With tetrabutylammomium bromide; sodium hydroxide for 6h; Reflux; | 93% |
With 18-crown-6 ether; potassium carbonate In N,N-dimethyl-formamide Reflux; | 90% |
With potassium carbonate In N,N-dimethyl-formamide for 12h; Reflux; Inert atmosphere; | 83% |
Conditions | Yield |
---|---|
In cyclohexane for 8h; Reflux; Inert atmosphere; | 93% |
Conditions | Yield |
---|---|
Stage #1: indole With sodium hydroxide In dimethyl sulfoxide Stage #2: 1,6-dichlorohexane In dimethyl sulfoxide at 20℃; for 3h; Further stages.; | 92% |
Conditions | Yield |
---|---|
In toluene for 24h; Reflux; | 92% |
sodium dibenzyldithiocarbamate
1,6-dichlorohexane
Conditions | Yield |
---|---|
With potassium iodide for 4h; Reagent/catalyst; Reflux; | 91.8% |
sodium dibenzyldithiocarbamate
1,6-dichlorohexane
Conditions | Yield |
---|---|
Stage #1: 1,6-dichlorohexane With sodium hydroxide; sodium thiosulfate In water for 9h; pH=7.1 - 7.3; Heating / reflux; Stage #2: sodium dibenzyldithiocarbamate With formaldehyd; sodium hydrogencarbonate In water; toluene at 22 - 23℃; for 23h; Product distribution / selectivity; | 91% |
sodium dibenzyldithiocarbamate
1,6-dichlorohexane
Conditions | Yield |
---|---|
Stage #1: sodium thiosulfate; 1,6-dichlorohexane With sodium hydroxide In water for 9h; pH=7.2; Heating / reflux; Stage #2: sodium dibenzyldithiocarbamate With formaldehyd; sodium hydrogencarbonate In water; toluene at 20 - 23℃; for 23h; pH=~ 8.3 - ~ 10.7; Product distribution / selectivity; | 91% |
sodium diphenylphosphide
1,6-dichlorohexane
(6-chlorohexyl)diphenylphosphane
Conditions | Yield |
---|---|
In tetrahydrofuran; toluene at -40℃; 5 hour's addition; | 90.6% |
Conditions | Yield |
---|---|
With sodium hydroxide Heating; | 90% |
Conditions | Yield |
---|---|
With sodium hydroxide Heating; | 90% |
3-Mercaptopropyltriethoxysilane
1,6-dichlorohexane
Conditions | Yield |
---|---|
Stage #1: 3-Mercaptopropyltriethoxysilane With sodium ethanolate In ethanol at 20℃; for 3h; Reflux; Stage #2: 1,6-dichlorohexane In ethanol at 80℃; for 3.5h; Reflux; | 89% |
Stage #1: 3-Mercaptopropyltriethoxysilane With sodium ethanolate In ethanol at 20℃; for 3h; Reflux; Stage #2: 1,6-dichlorohexane In ethanol at 80℃; for 3.5h; Reflux; | 89% |
Stage #1: 3-Mercaptopropyltriethoxysilane With sodium ethanolate In ethanol at 80℃; for 3h; Stage #2: 1,6-dichlorohexane In ethanol at 80℃; for 5h; |
3-Mercaptopropyltriethoxysilane
1,6-dichlorohexane
Conditions | Yield |
---|---|
Stage #1: 3-Mercaptopropyltriethoxysilane With sodium ethanolate In ethanol at 35℃; for 2h; Reflux; Stage #2: 1,6-dichlorohexane In ethanol at 80℃; for 4.5h; Reflux; | 88% |
Stage #1: 3-Mercaptopropyltriethoxysilane With ethanol; sodium ethanolate for 2h; Reflux; Stage #2: 1,6-dichlorohexane at 80℃; for 4.5h; Reflux; | 88% |
S,S-dimethyl dithiocarbonate
1,6-dichlorohexane
6-chloro-1-methylsulfanylhexane
Conditions | Yield |
---|---|
With tetrabutylammomium bromide; potassium hydroxide In water for 0.5h; Reflux; | 87% |
Conditions | Yield |
---|---|
In isopropyl alcohol for 16h; Reflux; | 87% |
3,5-dimethyl-1H-pyrazole
1,6-dichlorohexane
1,1'-(hexane-1,6-diyl)-bis(3,5-dimethyl-1H-pyrazole)
Conditions | Yield |
---|---|
Stage #1: 3,5-dimethyl-1H-pyrazole With potassium hydroxide In dimethyl sulfoxide at 20 - 22℃; for 0.333333h; Stage #2: 1,6-dichlorohexane In dimethyl sulfoxide at 20 - 30℃; | 84% |
Conditions | Yield |
---|---|
With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate for 16h; Heating; | 82% |
Conditions | Yield |
---|---|
In acetonitrile at 20℃; for 24h; | 82% |
1,6-dichlorohexane
Conditions | Yield |
---|---|
With nickel; triethylamine at 100℃; for 12h; Autoclave; Inert atmosphere; | 82% |
Conditions | Yield |
---|---|
In isopropyl alcohol for 16h; Reflux; | 81% |
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