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Conditions | Yield |
---|---|
With hydrogenchloride; tin(ll) chloride In dichloromethane; water for 16h; Reagent/catalyst; Reflux; | 81% |
With hydrogenchloride; tin | |
With hydrogen sulfide in ammoniakalischer Loesung; | |
With hydrogenchloride; tin(ll) chloride In dichloromethane; water for 24h; Reflux; |
Conditions | Yield |
---|---|
With sodium hydroxide; 4-sulfo-benzenediazonium-(1)-salt anschliessend Erwaermen der Reaktionsloesung mit Natriumdithionit; | |
Multi-step reaction with 3 steps 1: KOH / ethanol 2: HNO3, AcOH 3: H2 / Pd-C / ethanol View Scheme | |
Multi-step reaction with 2 steps 1: sodium nitrite; hydrogenchloride / ethanol; water / 1 h / 0 °C 2: hydrogenchloride; tin(ll) chloride / water; dichloromethane / 16 h / Reflux View Scheme |
Conditions | Yield |
---|---|
With sulfuric acid Electrolysis.Reduktion; | |
With sulfuric acid In ethanol at 90℃; (electrochemical reduction); |
Conditions | Yield |
---|---|
With sulfuric acid In water at 25℃; Rate constant; Thermodynamic data; ΔH(excit.), ΔS(excit.); | |
With sulfuric acid in Kohlendioxyd-Atmosphaere; |
Conditions | Yield |
---|---|
With sulfuric acid bei der elektrolytischen Oxydation an Platin-Anoden; |
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In ethanol |
2,5-Dimethyl-4-nitro-phenyl-benzylether
2,5-dimethyl-4-amino phenol
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In ethanol |
N-(2,5-dimethylphenyl)hydroxylamine
A
4-chloro-2,5-dimethylaniline
B
2,5-dimethyl-4-amino phenol
Conditions | Yield |
---|---|
With perchloric acid; sodium perchlorate; sodium chloride In water; acetonitrile at 25℃; Rate constant; |
Conditions | Yield |
---|---|
bei der elektrolytischen Oxydation an Platin-Anoden.Electrolysis; |
ethanol
2,5-dimethylphenyl azide
sulfuric acid
A
2,5-dimethylhydroquinone
B
2,5-dimethyl-4-amino phenol
2,5-dimethyl-4-amino phenol
Conditions | Yield |
---|---|
With titanium(III) chloride; water |
2,5-dimethyl-4-amino phenol
Conditions | Yield |
---|---|
With sulfuric acid | |
With sulfuric acid | |
With sulfuric acid |
2,5-dimethyl-4-amino phenol
Conditions | Yield |
---|---|
With hydrogenchloride |
hydrogenchloride
2,5-dimethyl-p-benzoquinone 4-oxime
2,5-dimethyl-4-amino phenol
sulfuric acid
N-(2,5-dimethylphenyl)hydroxylamine
A
2,5-dimethylhydroquinone
B
2,5-dimethyl-4-amino phenol
N-(2,4-dimethylphenyl)hydroxylamine
2,5-dimethyl-4-amino phenol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: alcohol; hydroxylamine hydrochloride 2: tin; hydrochloric acid View Scheme | |
Multi-step reaction with 2 steps 1: hydroxylamine hydrochloride; sodium acetate / ethanol / 1.5 h / Reflux 2: hydrogenchloride; tin(ll) chloride / water; dichloromethane / 16 h / Reflux View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: HNO3, AcOH 2: H2 / Pd-C / ethanol View Scheme |
2,5-dimethyl-4-amino phenol
acetic anhydride
1-Acetoxy-4-acetylamino-2,5-dimethylbenzene
Conditions | Yield |
---|---|
With pyridine In ethyl acetate for 1h; Heating / reflux; | 95% |
With potassium acetate In chloroform at 20℃; Heating / reflux; |
Conditions | Yield |
---|---|
In toluene | 91% |
di-tert-butyl dicarbonate
2,5-dimethyl-4-amino phenol
4-hydroxy-2,5-dimethylphenylcarbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 20℃; | 90% |
With triethylamine In methanol at 20℃; for 13h; | 80% |
In tetrahydrofuran for 4h; Heating; | |
In tetrahydrofuran Reflux; |
N-methyl-N-ethylformamide
2,5-dimethyl-4-amino phenol
N-ethyl-N'-(4-hydroxy-2,5-dimethylphenyl)-N-methylimidoformamide hydrochloride
Conditions | Yield |
---|---|
With trichlorophosphate In acetonitrile at 60℃; for 1h; | 85% |
2,5-dimethyl-4-amino phenol
trimethyl orthoformate
methyl N-(4-hydroxy-2,5-dimethylphenyl)formimidate
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid for 2h; Reflux; | 83.8% |
With toluene-4-sulfonic acid for 1h; Reflux; |
5-chloro-3-(4-chlorobenzyl)-1,2,4-thiadiazole
2,5-dimethyl-4-amino phenol
4-{[3-(4-chlorobenzyl)-1,2,4-thiadiazol-5-yl]oxy}-2,5-dimethylaniline
Conditions | Yield |
---|---|
Stage #1: 2,5-dimethyl-4-amino phenol With sodium hydroxide In N,N-dimethyl acetamide at 40℃; for 0.5h; Inert atmosphere; Stage #2: 5-chloro-3-(4-chlorobenzyl)-1,2,4-thiadiazole In N,N-dimethyl acetamide at 20℃; for 2h; Inert atmosphere; | 83.8% |
2,5-dimethyl-4-amino phenol
5-chloro-3-phenyl-isothiazole
2,5-dimethyl-4-[(3-phenylisothiazol-5-yl)oxy]aniline
Conditions | Yield |
---|---|
Stage #1: 2,5-dimethyl-4-amino phenol With sodium hydride In N,N-dimethyl-formamide; mineral oil at 20℃; for 2h; Stage #2: 5-chloro-3-phenyl-isothiazole In N,N-dimethyl-formamide; mineral oil at 100℃; for 3h; | 80% |
Conditions | Yield |
---|---|
In acetone at 40℃; for 1h; | 80% |
Conditions | Yield |
---|---|
With pyridine at 0 - 20℃; for 5h; Inert atmosphere; | 80% |
With pyridine at 0 - 20℃; for 24h; Inert atmosphere; | |
With pyridine at 0 - 25℃; for 12h; Inert atmosphere; |
3-tert-butyl-5-chloroisothiazole-4-carbonitrile
2,5-dimethyl-4-amino phenol
5-(4-amino-2,5-dimethylphenoxy)-3-tert-butylisothiazole-4-carbonitrile
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide for 6h; Reflux; | 79% |
3-[1-(4-chloro-phenyl)cyclopropyl]-5-[(4-methylphenyl)sulphonyl]-1,2,4-thiadiazole
2,5-dimethyl-4-amino phenol
4-({3-[1-(4-chlorophenyl)cyclopropyl]-1,2,4-thiadiazol-5-yl}oxy)-2,5-dimethylaniline
Conditions | Yield |
---|---|
Stage #1: 2,5-dimethyl-4-amino phenol With potassium carbonate In acetonitrile at 20℃; for 0.5h; Stage #2: 3-[1-(4-chloro-phenyl)cyclopropyl]-5-[(4-methylphenyl)sulphonyl]-1,2,4-thiadiazole In acetonitrile at 50℃; for 12h; | 76.9% |
4,5-dichloro-3-phenylisothiazole
2,5-dimethyl-4-amino phenol
4-[(4-chloro-3-phenylisothiazol-5-yl)oxy]-2,5-dimethylaniline
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide at 150℃; for 4h; | 72% |
2,5-dimethyl-4-amino phenol
4-methylphenylacetyl chloride
N-(4-hydroxy-2,5-dimethylphenyl)-2-(4-methylphenyl)acetamide
Conditions | Yield |
---|---|
With sodium acetate; acetic acid In N,N-dimethyl-formamide at 20℃; | 72% |
2,5-dimethyl-4-amino phenol
methanesulfonyl chloride
N-(4-hydroxy-2,5-dimethylphenyl)methanesulfonamide
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water at 70℃; for 0.5h; | 70% |
4-formyl indole
2-Butynoic acid
tert-butylisonitrile
2,5-dimethyl-4-amino phenol
Conditions | Yield |
---|---|
In methanol at 50℃; Ugi Condensation; | 70% |
2,5-dimethyl-4-amino phenol
N-phenylsulfonylbenzimidoyl chloride
N-(4-hydroxy-2,5-dimethylphenyl)-N'-(phenylsulfonyl)benzimidamide
Conditions | Yield |
---|---|
With sodium acetate In acetic acid; N,N-dimethyl-formamide | 69% |
2,5-dimethyl-4-amino phenol
Cinnamoyl chloride
(2E)-N-(4-hydroxy-2,5-dimethylphenyl)-3-phenylprop-2-enamide
Conditions | Yield |
---|---|
With sodium acetate; acetic acid In N,N-dimethyl-formamide at 20℃; | 66% |
2,5-dimethyl-4-amino phenol
2,6-dichloro-4-(trifluoromethyl)pyridine
Conditions | Yield |
---|---|
With potassium carbonate In dimethyl sulfoxide at 120℃; for 6h; | 64% |
2,5-dimethyl-4-amino phenol
phenyl isocyanate
1-(4-hydroxy-2,5-dimethylphenyl)-3-phenylurea
Conditions | Yield |
---|---|
In 1,4-dioxane at 100℃; | 64% |
N-(tolylsulfonyl)benzimidoyl chloride
2,5-dimethyl-4-amino phenol
N-(4-hydroxy-2,5-dimethylphenyl)-N'-(4-methylphenylsulfonyl)benzimidamide
Conditions | Yield |
---|---|
With sodium acetate In acetic acid; N,N-dimethyl-formamide | 62% |
4-nitro-benzenesulfinyl chloride
2,5-dimethyl-4-amino phenol
N-4-nitrophenylthio-2,5-dimethyl-1,4-benzoquinone imine
Conditions | Yield |
---|---|
With triethylamine In diethyl ether | 60% |
2,5-dimethyl-4-amino phenol
3,4-dichloro-2-ethylpyridine
Conditions | Yield |
---|---|
With potassium carbonate In dimethyl sulfoxide at 120℃; for 6h; | 59% |
Conditions | Yield |
---|---|
Stage #1: 2,5-dimethyl-4-amino phenol; trimethyl orthoformate With toluene-4-sulfonic acid for 2h; Heating / reflux; Stage #2: N-Ethylmethylamine In toluene at 50℃; for 20h; | 55% |
2,5-dimethyl-4-amino phenol
N-p-chlorophenylsulfonylbenzimidoyl chloride
N'-(4-chlorophenylsulfonyl)-N-(4-hydroxy-2,5-dimethylphenyl)benzimidamide
Conditions | Yield |
---|---|
With sodium acetate In acetic acid; N,N-dimethyl-formamide | 54% |
4-nitro-benzenesulfinyl chloride
2,5-dimethyl-4-amino phenol
Conditions | Yield |
---|---|
Stage #1: 4-nitro-benzenesulfinyl chloride; 2,5-dimethyl-4-amino phenol With triethylamine In diethyl ether for 0.166667h; Stage #2: With silver(l) oxide In acetone for 0.5h; Further stages.; | 53% |
7-(benzyloxy)-4-chloro-6-methoxyquinoline
2,5-dimethyl-4-amino phenol
4-{[7-(Benzyloxy)-6-methoxy-4-quinolyl]oxy}-2,5-dimethylaniline
Conditions | Yield |
---|---|
With dimethyl sulfoxide In methanol; water | 52% |
4-chloro-2-(2-pyridinyl)-6-(trifluoromethyl)pyrimidine
2,5-dimethyl-4-amino phenol
Conditions | Yield |
---|---|
47% |
4-chloro-2-(2-pyrazinyl)-6-(trifluoromethyl)pyrimidine
2,5-dimethyl-4-amino phenol
Conditions | Yield |
---|---|
47% |
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