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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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Conditions | Yield |
---|---|
With potassium phosphate In tetrahydrofuran at 115℃; for 18h; | 100% |
With CF3-DPPF; bis(dibenzylideneacetone)-palladium(0) In tetrahydrofuran; toluene at 120℃; for 20h; | 79.6% |
With CF3-DPPF ligand; bis(dibenzylideneacetone)-palladium(0) In tetrahydrofuran; toluene at 120℃; for 30h; Product distribution; various DPPF ligands for the Pd-catalyzed formation of diaryl ethers; |
Conditions | Yield |
---|---|
With N,N-dimethylglycine hydrochoride; caesium carbonate; copper(l) iodide In 1,4-dioxane at 90℃; for 88h; | 100% |
With caesium carbonate; copper(l) iodide; N,N-dimethylglycine hydrochoride In 1,4-dioxane at 90℃; for 88h; Inert atmosphere; | 100% |
With copper(l) iodide; N,N-dimethylglycine hydrochoride; caesium carbonate In 1,4-dioxane at 90℃; for 88h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With di-tert-butyl{2′-isopropoxy-[1,1′-binaphthalen]-2-yl}phosphane; potassium phosphate; bis(dibenzylideneacetone)-palladium(0) In toluene at 110℃; for 18h; Catalytic behavior; Reagent/catalyst; Solvent; Inert atmosphere; | 99% |
With potassium carbonate In N,N-dimethyl-formamide at 110℃; for 12h; | 95% |
With copper(l) iodide; potassium carbonate; dimethylbiguanide In acetonitrile at 20 - 60℃; for 10.1667h; Ullmann Condensation; | 92% |
Conditions | Yield |
---|---|
With 1,1,1,5,5,5-hexafluoroacetylacetone; copper(II) ferrite; caesium carbonate In 1-methyl-pyrrolidin-2-one at 135℃; for 24h; Ullmann Condensation; Inert atmosphere; Schlenk technique; | 98% |
With potassium phosphate; 2-((di-adamantan-1-yl)phosphaneyl)-1-(2,6-diisopropylphenyl)-1H-imidazole; palladium diacetate In toluene at 100℃; for 10h; Inert atmosphere; | 97% |
With potassium fluoride; copper(II) ion; silica gel In dimethyl sulfoxide at 130℃; for 16h; Ullmann diaryl etherification; | 95% |
Conditions | Yield |
---|---|
With [Pd((η5-C5H5)Fe[(η5-C5H3)C(Me)=N(C6H4-4-Me)])(μ-Cl)]2; caesium carbonate In N,N-dimethyl-formamide at 100℃; for 2h; | 97% |
With caesium carbonate In N,N-dimethyl-formamide at 100℃; for 5h; Inert atmosphere; Schlenk technique; Green chemistry; | 93% |
With copper(II) acetate monohydrate; caesium carbonate In N,N-dimethyl-formamide at 100℃; for 4h; Inert atmosphere; Schlenk technique; | 90% |
Conditions | Yield |
---|---|
With potassium carbonate In dimethyl sulfoxide for 0.0833333h; Heating; microwave irradiation; | 96% |
With sodium carbonate In N,N-dimethyl-formamide for 24h; Reflux; | 94% |
With cesium fluoride/clinoptilolite In dimethyl sulfoxide at 110℃; for 0.5h; Ullmann Condensation; | 92% |
4-cyanophenol
triphenylsulfonium trifluoromethanesulfonate
4-phenoxybenzonitrile
Conditions | Yield |
---|---|
With cesium hydroxide In 1,4-dioxane at 50℃; for 24h; Inert atmosphere; Glovebox; | 94% |
Conditions | Yield |
---|---|
With potassium fluoride; 4,4'-dimethyl-2,2'-bipyridines; trifluoroacetic acid; sodium iodide; nickel dichloride; zinc In N,N-dimethyl acetamide at 60℃; for 36h; | 94% |
Conditions | Yield |
---|---|
With dichloro[bis{1-(dicyclohexylphosphanyl)piperidine}]palladium; sodium carbonate In 1-methyl-pyrrolidin-2-one at 140℃; for 6h; Inert atmosphere; | 93% |
4-phenoxybenzaldehyde oxime
4-phenoxybenzonitrile
Conditions | Yield |
---|---|
With 4-nitro-1-((trifluoromethyl)sulfonyl)-1H-imidazole; triethylamine In acetonitrile at 20℃; for 0.166667h; Inert atmosphere; Sealed tube; | 92% |
triphenyl bismuth (2+); dichloride
4-cyanophenol
4-phenoxybenzonitrile
Conditions | Yield |
---|---|
With N,N,N′,N′-tetramethyl-N″-tert-butylguanidine In toluene for 3h; Heating; | 91% |
4-phenoxybenzonitrile
Conditions | Yield |
---|---|
With potassium tert-butylate In N,N-dimethyl acetamide at 140℃; for 16h; | 90% |
4-Bromodiphenyl ether
formamide
4-phenoxybenzonitrile
Conditions | Yield |
---|---|
With 1,3,5-trichloro-2,4,6-triazine; palladium on activated charcoal; potassium carbonate; triphenylphosphine at 25 - 130℃; for 12.1667h; | 90% |
4-cyanobenzoic acid methyl ester
methyl (4-phenyloxy)phenyl sulfide
4-phenoxybenzonitrile
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)nickel (0); 1,2-bis-(dicyclohexylphosphino)ethane In o-xylene at 140℃; for 24h; Glovebox; Inert atmosphere; | 88% |
1-naphthalenecarboxylic acid
4-bromobenzenecarbonitrile
phenol
4-phenoxybenzonitrile
Conditions | Yield |
---|---|
With caesium carbonate; silica gel In dichloromethane; ethyl acetate; toluene | 86% |
4-(4-(hydroxymethyl)phenoxy)benzonitrile
4-phenoxybenzonitrile
Conditions | Yield |
---|---|
With oxygen; palladium diacetate; sodium carbonate In cyclohexane at 130℃; for 48h; Molecular sieve; Schlenk technique; | 86% |
2,2-dimethylmalononitrile
4-phenoxyphenylboronic acid
4-phenoxybenzonitrile
Conditions | Yield |
---|---|
With chloro(1,5-cyclooctadiene)rhodium(I) dimer; caesium carbonate In 1,4-dioxane at 100℃; for 6h; Inert atmosphere; | 86% |
Conditions | Yield |
---|---|
With tris-(3,6-dioxaheptyl)amine In 1,2-dichloro-benzene for 8h; Heating; | 85% |
4-fluorobenzonitrile
phenol
A
4-(4'-cyanophenoxy)benzonitrile
B
4-phenoxybenzonitrile
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)diiridium(I) dichloride; water; caesium carbonate; 1,2-bis-(diphenylphosphino)ethane; bis(pinacol)diborane In N,N-dimethyl-formamide at 140℃; for 24h; Schlenk technique; chemoselective reaction; | A 82% B 11% |
Conditions | Yield |
---|---|
With caesium carbonate; Cu nanoparticles In acetonitrile at 50 - 55℃; under 760.051 Torr; for 4h; Ullmann coupling; | 81% |
With copper(II) oxide In dimethyl sulfoxide at 120℃; for 26h; Ullmann Condensation; | 78% |
With potassium carbonate In toluene at 80℃; for 12.1h; Catalytic behavior; Inert atmosphere; | 70% |
With copper(l) iodide; potassium carbonate; dimethylbiguanide In acetonitrile at 20 - 60℃; for 24.1667h; Ullmann Condensation; | 20% |
With tetrabutylammomium bromide; caesium carbonate In dimethyl sulfoxide at 120℃; for 20h; | 7% |
Conditions | Yield |
---|---|
With oxygen; copper diacetate; triethylamine In dichloromethane at 50℃; for 16h; Reagent/catalyst; Time; Solvent; Sealed tube; | 81% |
tert-butyl isocyanide
4-phenoxyphenylmagnesium bromide
4-phenoxybenzonitrile
Conditions | Yield |
---|---|
Stage #1: tert-butyl isocyanide; 4-phenoxyphenylmagnesium bromide In diethyl ether at 60℃; for 48h; Cooling with ice; Sealed tube; Stage #2: With methanol; oxygen; copper(ll) bromide In diethyl ether; N,N-dimethyl-formamide at 0 - 80℃; under 760.051 Torr; for 24h; | 81% |
Conditions | Yield |
---|---|
80% | |
With oxygen; copper(ll) bromide; potassium hexacyanoferrate(III) In N,N-dimethyl-formamide at 150℃; for 12h; Sealed tube; | 72% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 40℃; for 20h; | 80% |
Conditions | Yield |
---|---|
With copper(l) iodide; cesium hydroxide; 2,2,6,6-tetramethylheptane-3,5-dione; caesium carbonate In dimethyl sulfoxide at 130℃; for 30h; Inert atmosphere; Sealed tube; chemoselective reaction; | 78% |
Conditions | Yield |
---|---|
Stage #1: 4-fluorobenzonitrile With cesium fluoride In N,N-dimethyl-formamide for 0.166667h; Inert atmosphere; Stage #2: phenyltrimethylsilyl ether In N,N-dimethyl-formamide at 20℃; for 42h; | 78% |
Glutaronitrile
4-Phenoxybenzoic acid
A
piperidine-2,6-dione
B
4-phenoxybenzonitrile
Conditions | Yield |
---|---|
With aluminum (III) chloride at 200℃; for 5h; Sealed tube; | A n/a B 78% |
Conditions | Yield |
---|---|
Stage #1: phenol With potassium tert-butylate In tetrahydrofuran; N,N-dimethyl-formamide at 25℃; for 0.166667h; Inert atmosphere; Schlenk technique; Stage #2: 4-cyano-N,N,N-trimethylanilinium trifluoromethansulfonate In tetrahydrofuran; N,N-dimethyl-formamide at 25℃; for 3h; Inert atmosphere; Schlenk technique; | 78% |
Conditions | Yield |
---|---|
Stage #1: potassium phenyltrifluoborate With dmap; copper diacetate; 4 A molecular sieve In dichloromethane at 20℃; for 0.0833333h; Stage #2: 4-cyanophenol With oxygen In dichloromethane at 20℃; for 24h; | 77% |
Conditions | Yield |
---|---|
With Oxone; caesium carbonate; copper dichloride In dimethyl sulfoxide at 100℃; for 24h; | 77% |
4-phenoxybenzonitrile
(Z)-N′-hydroxy-4-phenoxybenzamidine
Conditions | Yield |
---|---|
With hydroxylamine In ethanol for 3h; Heating / reflux; | 100% |
With hydroxylamine In ethanol for 3h; Reflux; | 100% |
With hydroxylamine In ethanol for 3h; Reflux; | 100% |
Conditions | Yield |
---|---|
With dihydrogen peroxide; potassium hydroxide In methanol; ethanol for 4.5h; Reflux; | 96% |
With potassium phosphate buffer at 30℃; for 72h; Rhodococcus sp. AJ270 cells; | 59.3% |
With potassium hydroxide |
4-phenoxybenzonitrile
4-phenoxybenzamidoxime
Conditions | Yield |
---|---|
With hydroxylamine In ethanol; water Reflux; | 96% |
With hydroxylamine In ethanol | |
With hydroxylamine In ethanol Heating; | |
With hydroxylamine hydrochloride; triethylamine In methanol at 60℃; for 6h; |
Conditions | Yield |
---|---|
Stage #1: 4-phenoxybenzonitrile; phenyllithium With water In dibutyl ether at 20℃; for 0.0166667h; Inert atmosphere; Schlenk technique; Stage #2: allylmagnesium bromide With water In dibutyl ether at 20℃; for 0.0833333h; Inert atmosphere; Schlenk technique; chemoselective reaction; | 92% |
4-phenoxybenzonitrile
4-penoxybenzothioamide
Conditions | Yield |
---|---|
With sodium hydrogen sulfide; magnesium chloride In N,N-dimethyl-formamide at 40℃; | 89% |
With pyridine; hydrogen sulfide; triethylamine at 20℃; for 72h; |
Conditions | Yield |
---|---|
With tetra-n-butylammoniumfluoride hydrate at 120℃; for 9h; | 89% |
4-phenoxybenzonitrile
4-phenoxybenzylamine
Conditions | Yield |
---|---|
With 5%-palladium/activated carbon; hydrogen In methanol for 3h; Inert atmosphere; | 88% |
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 20℃; for 6h; | 45% |
4-phenoxybenzonitrile
5-(4-phenoxy)phenyltetrazole
Conditions | Yield |
---|---|
With trimethylsilylazide; di(n-butyl)tin oxide In toluene at 20℃; for 5h; Inert atmosphere; Reflux; | 87% |
Conditions | Yield |
---|---|
With silver hexafluoroantimonate; sodium hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; water; acetic acid; silver(l) oxide In 1,2-dichloro-ethane at 120℃; for 12h; Inert atmosphere; | 87% |
Dibenzothiophene sulfoxide
trifluoromethylsulfonic anhydride
4-phenoxybenzonitrile
Conditions | Yield |
---|---|
In dichloromethane at -40 - 20℃; for 2h; Inert atmosphere; | 87% |
thianthrene-5-oxide
trifluorormethanesulfonic acid
4-phenoxybenzonitrile
sodium triflate
Conditions | Yield |
---|---|
Stage #1: thianthrene-5-oxide; trifluorormethanesulfonic acid; 4-phenoxybenzonitrile With trifluoroacetic anhydride In acetonitrile at -40 - 20℃; for 1h; Inert atmosphere; Stage #2: sodium triflate In water Inert atmosphere; | 85% |
4-phenoxybenzonitrile
acetonitrile
3-amino-3-(4-phenoxyphenyl)acrylonitrile
Conditions | Yield |
---|---|
Stage #1: 4-phenoxybenzonitrile; acetonitrile With n-butyllithium; N-ethyl-N,N-diisopropylamine In tetrahydrofuran at -78℃; for 2h; Stage #2: With hydrogenchloride; ammonium chloride In tetrahydrofuran; water | 82% |
With n-butyllithium; diisopropylamine In tetrahydrofuran; hexane at -78 - 0℃; |
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