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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

Dichlorosilane

Cas:4109-96-0

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Dichlorosilane

Cas:4109-96-0

Min.Order:1

Negotiable

Type:Other

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

Dichlorosilane

Cas:4109-96-0

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Dichlorosilane

Cas:4109-96-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality Dichlorosilane

Cas:4109-96-0

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung, LG, Merck, Thermo Fisher Scientific and so o

4109-96-0 Dichlorosilane

Cas:4109-96-0

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

Dichlorosilane

Cas:4109-96-0

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

Silane, dichloro-

Cas:4109-96-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard

Hot selling products CAS 4109-96-0 with fast delivery

Cas:4109-96-0

Min.Order:1 Kilogram

FOB Price: $112.0

Type:Trading Company

inquiry

Xiamen AmoyChem Co.,Ltd

Amoychem is committed to providing the top-quality chemical products and services Internationally. We offer our customers with friendly, professional service and reliable, high performance products that have been manufactured according to the accredi

Dichlorosilane

Cas:4109-96-0

Min.Order:0

Negotiable

Type:Other

inquiry

Hubei Langyou International Trading Co., Ltd

Dichlorosilicon Application:Dichlorosilicon

Dichlorosilicon

Cas:4109-96-0

Min.Order:0

Negotiable

Type:Other

inquiry

Hunan Longxianng Runhui Trading Co.,Ltd

DichlorosiliconAppearance:ask Storage:Keep in dry and cool condition Package:foil aluminium bag/vacuum packing Application:intermediates Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount. By air(airport to airport) or

Dichlorosilicon

Cas:4109-96-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zhengzhou Kingorgchem Chemical Technology Co., Ltd.

Zhengzhou Kingorgchem Chemical Technology Co., Ltd. was founded on the basis of Organophosphorus Chemistry Lab of Institute of Chemistry Henan Academy of Sciences in 2015. The laboratory covers 600 m2 and the pilot plant covers 2000 m2. Kingorgchem i

National Research Platform ISO 9001 4109-96-0

Cas:4109-96-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Xiamen BaiFuchem Co.,Ltd

BaiFuChem is a Professional chemical raw material supplier in China, our main products include Biochemical , Pharma Intermediate and Organic chemical etc. BaiFuChem have wealth of products,experience , expertise and state-of-the-art

High Purity Dichlorosilane

Cas:4109-96-0

Min.Order:1 Kilogram

Negotiable

Type:Other

inquiry

HuBei Ipure Biotech CO.,ltd

HuBei ipure is a diversified product production and operation enterprise, with API, pharma intermediates, and other fine chemicals as well as R&D and pigments development and sales as one of the large enterprises, with more than 1

High quality Dichlorosilane supplier in China

Cas:4109-96-0

Min.Order:1 Gram

FOB Price: $1.0

Type:Trading Company

inquiry

Henan Fine Chemicals Co., Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & CommercialHenan Fine Chemicals Co., LTD. is a diversified technology - oriented integrated company, which mainly concentrates on fine chemicals. Our company is committed to becom

Silane, dichloro-

Cas:4109-96-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Shanghai united Scientific Co.,Ltd.

United Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat

Silane, dichloro-

Cas:4109-96-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Wanda Organosilicon New Material Co., Ltd

DICHLOROSILANE

Dichlorosilane

Cas:4109-96-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

changchun tuocai technology co.,ltld

DichlorosiliconAppearance:ask Storage:Keep in dry and cool condition Package:foil aluminium bag/vacuum packing Application:intermediates Transportation:by air or by sea

Dichlorosilicon

Cas:4109-96-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Allicon Pharmaceuticals,Inc.

COA,H-NMR,HPLC availableWe have offices in Boston,MA,USAWe ship it in real nameMerck and Sigma are our customersPayment:Credit card/Net 30 daysWeb:www.alliconpharma.com Storage:Store in a cool, dry, well-ventilated area away from incompatible substan

Dichlorosilane

Cas:4109-96-0

Min.Order:0

Negotiable

Type:Other

inquiry

Nanjing Raymon Biotech Co., Ltd.

Silane, dichloro- Storage:keep in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/pharma intermediate Transportation:By Sea,by Air,By courier like DHL or Fedx. Port:Shanghai/Shenzhen

Silane, dichloro-

Cas:4109-96-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hebei Minshang Biotechnology Co., Ltd

High Cost-Effective Application:intermediates

4109-96-0

Cas:4109-96-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Synova( Tianjin ) Chemical Technology Co,.Ltd

The company have effective management team, professional technical R & D personnel, the service spirit of customer oriented. We have long-term cooperation with famous domestic manufacturer, and excellent customer resources overseas. We are skilled in

DICHLOROSILANE

Cas:4109-96-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Fenjun Chemical Co Ltd.

Dichlorosilicon Application:Dichlorosilicon

Dichlorosilicon

Cas:4109-96-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hebei Ruishun Trade Co.,Ltd

Supply top quality products with a reasonable price Application:api

4109-96-0

Cas:4109-96-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Changzhou Foreign Trade Corp

CFTC?PharmaChem?is?a?service?based?company?in?China,?a?pharmachem?division?of?Changzhou?Foreign?Trade?Corp.,supplying?raw?materials,?intermediates,?APIs?and?fine?chemicals?for?the?pharmaceutical?and?specialty?chemical?industries?worldwide. Applicatio

dichlorosilane

Cas:4109-96-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Chemical Co.Ltd

Silane, dichloro-Appearance:Off white to slight yellow solid Storage:Stored in shaded, cool and dry places Package:1L 5L 10L 25L bottle Application:pharma intermediate Transportation:Handle with cares to avoid damaging the packages. Protect them from

Silane, dichloro-

Cas:4109-96-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

NovaChemistry

High purity Application:Pharmaceutical intermediates, Material synthesis and analyzing the expectant ingredients

dichlorosilane, 25% in heptane

Cas:4109-96-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Synthetic route

hydrogenchloride
7647-01-0

hydrogenchloride

monosilane
7440-21-3

monosilane

Dichlorosilane
4109-96-0

Dichlorosilane

Conditions
ConditionsYield
In neat (no solvent) reaction at 100 °C for a longer period of time;;79%
In neat (no solvent) reaction at 100 °C for a longer period of time;;79%
(4-methylphenyl)silane
931-70-4

(4-methylphenyl)silane

A

HSiCl2-p-CH3C6H4
13272-80-5

HSiCl2-p-CH3C6H4

B

Dichlorosilane
4109-96-0

Dichlorosilane

C

monochloro(p-tolyl)silane

monochloro(p-tolyl)silane

Conditions
ConditionsYield
With hydrogenchloride In diethyl ether at 60℃; for 19h; Temperature;A 5%
B 17%
C 76%
With hydrogenchloride; diethyl ether In benzene-d6 at 80℃; Reagent/catalyst; Schlenk technique; Inert atmosphere;A 16 %Spectr.
B 36 %Spectr.
C 40 %Spectr.
hydrogenchloride
7647-01-0

hydrogenchloride

monosilane
7440-21-3

monosilane

A

chlorosilane
13966-57-9

chlorosilane

B

Dichlorosilane
4109-96-0

Dichlorosilane

Conditions
ConditionsYield
In diethyl ether at 60℃; for 20h;A 73%
B 27%
In diethyl ether at 80℃; for 42h;A 34%
B 66%
(2,4,6-trimethylphenyl)silane
120578-34-9

(2,4,6-trimethylphenyl)silane

A

chlorosilane
13966-57-9

chlorosilane

B

Dichlorosilane
4109-96-0

Dichlorosilane

Conditions
ConditionsYield
With hydrogenchloride In diethyl ether at 80℃; for 15h; Solvent; Temperature;A 64%
B 36%
With hydrogenchloride; diethyl ether In benzene-d6 at 80℃; for 15h; Reagent/catalyst; Schlenk technique; Inert atmosphere;A 64 %Spectr.
B 36 %Spectr.
allylsilane
18191-59-8

allylsilane

A

chlorosilane
13966-57-9

chlorosilane

B

Dichlorosilane
4109-96-0

Dichlorosilane

Conditions
ConditionsYield
With hydrogenchloride In diethyl ether at 60℃; for 20h;A 42%
B 13%
With hydrogenchloride In diethyl ether at 80℃; for 42h;A 20%
B 33%
With hydrogenchloride; diethyl ether In benzene-d6 at 60℃; for 20h; Reagent/catalyst; Schlenk technique; Inert atmosphere;A 42 %Spectr.
B 13 %Spectr.
With hydrogenchloride; diethyl ether In benzene-d6 at 80℃; Reagent/catalyst; Schlenk technique; Inert atmosphere;A 20 %Spectr.
B 33 %Spectr.
trichlorosilane
10025-78-2

trichlorosilane

hydrogen
1333-74-0

hydrogen

A

chlorosilane
13966-57-9

chlorosilane

B

Dichlorosilane
4109-96-0

Dichlorosilane

Conditions
ConditionsYield
With aluminium In neat (no solvent) passing a mixture of SiHCl3 and H2 (1:2) over Al at 350 °C;; separation by fractionated distillation;;A 1-2
B 15%
With Al In neat (no solvent) passing a mixture of SiHCl3 and H2 (1:2) over Al at 350 °C;; separation by fractionated distillation;;A 1-2
B 15%
trichlorosilane
10025-78-2

trichlorosilane

A

chlorosilane
13966-57-9

chlorosilane

B

Dichlorosilane
4109-96-0

Dichlorosilane

diphenylsilyl dichloride
80-10-4

diphenylsilyl dichloride

A

Dichlorosilane
4109-96-0

Dichlorosilane

B

Phenyltrichlorosilane
98-13-5

Phenyltrichlorosilane

Conditions
ConditionsYield
With hydrogenchloride; trichlorosilane; aluminium chloride
With trichlorosilane; aluminium chloride
With trichlorosilane; aluminium chloride
dibromochlorosilane
82146-27-8

dibromochlorosilane

trimethylstannane
1631-73-8

trimethylstannane

A

dibromosilane
13768-94-0

dibromosilane

B

chlorosilane
13966-57-9

chlorosilane

C

Dichlorosilane
4109-96-0

Dichlorosilane

Conditions
ConditionsYield
In neat (no solvent) condensing of equimolar amts. of tinhydride and SiClHBr2 (trace of SiCl2HBr present) into cold finger, reaction at room temp. (30 min); further products; not isolated; IR spectroscopy;A 0%
B n/a
C 0%
trichlorosilane
10025-78-2

trichlorosilane

trimethylstannane
1631-73-8

trimethylstannane

A

trimethyltin(IV)chloride
1066-45-1

trimethyltin(IV)chloride

B

monosilane
7440-21-3

monosilane

C

Dichlorosilane
4109-96-0

Dichlorosilane

Conditions
ConditionsYield
In neat (no solvent) inert atmosphere (N2, Ar or high vac.), room temperature, equimolar amts. of halosilane/tinhydride, reactn. time 12 h; not isolated; IR spectroscopy (identified 41% SiCl2H2 and 15% SiH4 in product mixt.);
tetrachlorosilane
10026-04-7, 53609-55-5

tetrachlorosilane

trimethylstannane
1631-73-8

trimethylstannane

A

trichlorosilane
10025-78-2

trichlorosilane

B

trimethyltin(IV)chloride
1066-45-1

trimethyltin(IV)chloride

C

monosilane
7440-21-3

monosilane

D

Dichlorosilane
4109-96-0

Dichlorosilane

Conditions
ConditionsYield
In neat (no solvent) inert atmosphere (N2, Ar or high vac.), room temperature, equimolar amts. of halosilane/tinhydride, reactn. time 36 h; not isolated; IR spectroscopy (identified 25-30% SiCl3H, 15% SiCl2H2 and 10% SiH4 in product mixt.);
calcium hydride
7789-78-8

calcium hydride

tetrachlorosilane
10026-04-7, 53609-55-5

tetrachlorosilane

A

trichlorosilane
10025-78-2

trichlorosilane

B

chlorosilane
13966-57-9

chlorosilane

C

Dichlorosilane
4109-96-0

Dichlorosilane

Conditions
ConditionsYield
In neat (no solvent) byproducts: H2, HCl; passing SiCl4 vapor over CaH2 below red heat;;A n/a
B 0%
C 0%
In neat (no solvent) byproducts: H2, HCl; passing SiCl4 vapor over CaH2 below red heat;;A n/a
B 0%
C 0%
tetrachlorosilane
10026-04-7, 53609-55-5

tetrachlorosilane

monosilane
7440-21-3

monosilane

A

trichlorosilane
10025-78-2

trichlorosilane

B

chlorosilane
13966-57-9

chlorosilane

C

Dichlorosilane
4109-96-0

Dichlorosilane

Conditions
ConditionsYield
In gas reactor temp.: 250 - 500°C; detn. by gas chromy.;
tetrachlorosilane
10026-04-7, 53609-55-5

tetrachlorosilane

hydrogen
1333-74-0

hydrogen

A

aluminium trichloride
7446-70-0

aluminium trichloride

B

trichlorosilane
10025-78-2

trichlorosilane

C

Dichlorosilane
4109-96-0

Dichlorosilane

Conditions
ConditionsYield
With aluminium In neat (no solvent) byproducts: SiCl4; reaction by passing SiCl4 vapor with H2 (1:1) over Al at 400 °C;; distn.;;
With Al In neat (no solvent) byproducts: SiCl4; reaction by passing SiCl4 vapor with H2 (1:1) over Al at 400 °C;; distn.;;
tetrachlorosilane
10026-04-7, 53609-55-5

tetrachlorosilane

hydrogen
1333-74-0

hydrogen

A

trichlorosilane
10025-78-2

trichlorosilane

B

Dichlorosilane
4109-96-0

Dichlorosilane

Conditions
ConditionsYield
With co-catalyst: pyrimidine or P(OPh)3; tri-n-butyl-tin hydride In toluene absence of air; H2-stream; further alternate co-catalysts: PCy3 or PBu3 or N-methylimidazole or pyridine or chinoline; gas chromy.;
tri-n-butyl-tin hydride In acetonitrile absence of air; H2-stream; gas chromy.;
With Al or Mg or Zn In neat (no solvent, gas phase) passing SiCl4 vapor and H2 over granulated Al, Mg or Zn at 350-450 °C;; condensation of the gaseous reaction product by dry ice, separation of the mixture by fractionation;;
With Al or Mg or Zn In gas passing SiCl4 vapor and H2 over granulated Al, Mg or Zn at 350-450 °C;; condensation of the gaseous reaction product by dry ice, separation of the mixture by fractionation;;
tetrachlorosilane
10026-04-7, 53609-55-5

tetrachlorosilane

hydrogen
1333-74-0

hydrogen

A

trichlorosilane
10025-78-2

trichlorosilane

B

monosilane
7440-21-3

monosilane

C

Dichlorosilane
4109-96-0

Dichlorosilane

Conditions
ConditionsYield
With co-catalyst: P(O(i)Pr)3 or PMe2Ph or PPh3; tri-n-butyl-tin hydride In toluene absence of air; H2-stream; further alternate co-catalysts: PCy3 or PBu3 or N-methylimidazole or pyridine or chinoline; gas chromy.;
tetrachlorosilane
10026-04-7, 53609-55-5

tetrachlorosilane

hydrogen
1333-74-0

hydrogen

A

trichlorosilane
10025-78-2

trichlorosilane

B

chlorosilane
13966-57-9

chlorosilane

C

Dichlorosilane
4109-96-0

Dichlorosilane

Conditions
ConditionsYield
With co-catalyst: P(OMe)3; tri-n-butyl-tin hydride In toluene absence of air; H2-stream; further alternate co-catalysts: PCy3 or PBu3 or N-methylimidazole or pyridine or chinoline; gas chromy.;
tin(IV) chloride
7646-78-8

tin(IV) chloride

monosilane
7440-21-3

monosilane

A

chlorosilane
13966-57-9

chlorosilane

B

Dichlorosilane
4109-96-0

Dichlorosilane

Conditions
ConditionsYield
In not given chlorination with SnCl4 leads to SiH3Cl at room temp.; no SnH2Cl2 formed;;A n/a
B 0%
hydrogenchloride
7647-01-0

hydrogenchloride

monosilane
7440-21-3

monosilane

A

disilane

disilane

B

trichlorosilane
10025-78-2

trichlorosilane

C

chlorosilane
13966-57-9

chlorosilane

D

hydrogen
1333-74-0

hydrogen

E

Dichlorosilane
4109-96-0

Dichlorosilane

Conditions
ConditionsYield
In gas Kinetics; Irradiation (UV/VIS); infrared laser irrdn. of SiH4-HCl mixt. in pressure range of 28-60 torrand in temp. range of 295-414 K; analyzed by mass spectrometry;
Dichloromethylsilane
75-54-7

Dichloromethylsilane

A

trichlorosilane
10025-78-2

trichlorosilane

B

chlorosilane
13966-57-9

chlorosilane

C

monosilane
7440-21-3

monosilane

D

Dichlorosilane
4109-96-0

Dichlorosilane

E

dimethylsilicon dichloride
75-78-5

dimethylsilicon dichloride

Conditions
ConditionsYield
With AlCl3 In neat (no solvent) (CH3)SiHCl2 and AlCl3 at 325°C under pressure; further products;;
With AlCl3 In neat (no solvent) (CH3)SiHCl2 and AlCl3 at 325°C under pressure; further products;;
hydrogenchloride
7647-01-0

hydrogenchloride

silicon
7440-21-3

silicon

A

chlorosilane
13966-57-9

chlorosilane

B

Dichlorosilane
4109-96-0

Dichlorosilane

Conditions
ConditionsYield
In neat (no solvent) reaction at rather low temperature;;
In neat (no solvent) heating of amorphous Si with HCl;;
In neat (no solvent) reaction at rather low temperature;;
In neat (no solvent) heating of amorphous Si with HCl;;
Dimethyl ether
115-10-6

Dimethyl ether

silicon
7440-21-3

silicon

A

Methyltrichlorosilane
75-79-6

Methyltrichlorosilane

B

tetrachlorosilane
10026-04-7, 53609-55-5

tetrachlorosilane

C

trichlorosilane
10025-78-2

trichlorosilane

D

Dichlorosilane
4109-96-0

Dichlorosilane

Conditions
ConditionsYield
With hydrogenchloride; copper In neat (no solvent) Si-Cu (9:1) and a mixt. of CH3OCH3 and HCl (2:1) at 325°C;;
calcium hydride
7789-78-8

calcium hydride

tetrachlorosilane
10026-04-7, 53609-55-5

tetrachlorosilane

A

chlorosilane
13966-57-9

chlorosilane

B

Dichlorosilane
4109-96-0

Dichlorosilane

Conditions
ConditionsYield
In neat (no solvent) passing SiCl4 vapor over heated CaH2;;A 0%
B 0%
In neat (no solvent) passing SiCl4 vapor over heated CaH2;;A 0%
B 0%
trichlorosilane
10025-78-2

trichlorosilane

Dichlorosilane
4109-96-0

Dichlorosilane

Conditions
ConditionsYield
With catalyst: anion exchange resin In gas Kinetics; byproducts: SiCl4; mixt. of Ar and SiHCl3 is passed over the catalyst (anion exchange resins AV17-12P with active group -N(+)Me3, AV27-10P with active group -N(+)Me2C2H5O, AN18-12P with active group -N(+)HMe2) at 388 K; react. is monitored by chromy.;
trichlorosilane
10025-78-2

trichlorosilane

A

chlorosilane
13966-57-9

chlorosilane

B

monosilane
7440-21-3

monosilane

C

Dichlorosilane
4109-96-0

Dichlorosilane

Conditions
ConditionsYield
With hydrogen; aluminium In neat (no solvent) byproducts: AlCl3; passing a mixture of SiHCl3 and H2 (1:2) over Al at 350 °C;;
trichlorosilane
10025-78-2

trichlorosilane

hydrogen
1333-74-0

hydrogen

A

chlorosilane
13966-57-9

chlorosilane

B

monosilane
7440-21-3

monosilane

C

Dichlorosilane
4109-96-0

Dichlorosilane

Conditions
ConditionsYield
In neat (no solvent, gas phase)
In gas
tetrachlorosilane
10026-04-7, 53609-55-5

tetrachlorosilane

magnesium hydride

magnesium hydride

A

trichlorosilane
10025-78-2

trichlorosilane

B

chlorosilane
13966-57-9

chlorosilane

C

monosilane
7440-21-3

monosilane

D

Dichlorosilane
4109-96-0

Dichlorosilane

Conditions
ConditionsYield
In tetrahydrofuran-d8 MgH2 and clorosilane (1.10:0.66 molar ratio) sealed under Ar; stored for 3 d at room temp., NMR;
tetrachlorosilane
10026-04-7, 53609-55-5

tetrachlorosilane

hydrogen
1333-74-0

hydrogen

Dichlorosilane
4109-96-0

Dichlorosilane

Conditions
ConditionsYield
With aluminium In neat (no solvent) passing a mixture of SiCl4 and H2 over Al at 400 °C;;3-5
With Al In neat (no solvent) passing a mixture of SiCl4 and H2 over Al at 400 °C;;3-5
chlorine
7782-50-5

chlorine

silacarbene
7440-21-3

silacarbene

Dichlorosilane
4109-96-0

Dichlorosilane

Conditions
ConditionsYield
In gas Kinetics; helium buffer gas (total pressure 5 Torr), ambient temp.; high-resolution transient absorption spectroscopy (SiH2);
Dichlorosilane
4109-96-0

Dichlorosilane

silicon
7440-21-3

silicon

Conditions
ConditionsYield
Prepd. by laser chemical vapor pptn. at atmospheric pressure.;100%
In neat (no solvent) chemical vapor deposition with a mixt. of SiH2Cl2 and H2;
With hydrogen chemical vapor deposition (hot-wall reactor, basic pressure 10 or 76 Torr, 1223 K);
ammonia
7664-41-7

ammonia

Dichlorosilane
4109-96-0

Dichlorosilane

silicon nitride

silicon nitride

Conditions
ConditionsYield
Prepd. by laser chemical vapor pptn. at atmospheric pressure.;100%
In neat (no solvent) Kinetics; under Ar, in a low-pressure flow reactor at various condns.;
low pressure chemical vapor deposition at 820 °C;
chloroplatinic acid

chloroplatinic acid

Dichlorosilane
4109-96-0

Dichlorosilane

1,7-Octadiene
3710-30-3

1,7-Octadiene

A

bis(octenyl)dichlorosilane

bis(octenyl)dichlorosilane

B

bis(8-trimethylsilyloctyl)dimethylsilane

bis(8-trimethylsilyloctyl)dimethylsilane

Conditions
ConditionsYield
In isopropyl alcoholA 90%
B n/a
Dichlorosilane
4109-96-0

Dichlorosilane

tris(trimethylsilyl)silyl potassium

tris(trimethylsilyl)silyl potassium

C9H29ClSi5
134648-78-5

C9H29ClSi5

Conditions
ConditionsYield
In toluene at -78℃; for 23h; Inert atmosphere;90%
n-propylmagnesium bromide
927-77-5

n-propylmagnesium bromide

Dichlorosilane
4109-96-0

Dichlorosilane

dipropylsilane
871-77-2

dipropylsilane

Conditions
ConditionsYield
In diethyl ether H2SiCl2 and n-C3H7MgBr in ether; acidic hydrolysis;;88%
In diethyl ether H2SiCl2 and n-C3H7MgBr in ether; acidic hydrolysis;;88%
Cp(PMe3)2RuH
90413-24-4

Cp(PMe3)2RuH

Dichlorosilane
4109-96-0

Dichlorosilane

A

RuCp(PMe3)SiH2Cl
222175-87-3

RuCp(PMe3)SiH2Cl

B

[Cp(PMe3)2RuH2]Cl
160158-78-1

[Cp(PMe3)2RuH2]Cl

Conditions
ConditionsYield
In diethyl ether Ar-atmosphere; -78°C; filtering, evapn.; elem. anal.;A 81%
B n/a
antimony(III) fluoride
7783-56-4

antimony(III) fluoride

Dichlorosilane
4109-96-0

Dichlorosilane

A

difluorosilane
13824-36-7

difluorosilane

B

trifluorosilane
13465-71-9

trifluorosilane

C

silicon tetrafluoride
7783-61-1

silicon tetrafluoride

Conditions
ConditionsYield
In neat (no solvent) byproducts: H2; reaction in presence of SbCl5 at room temperature;;A 80%
B n/a
C 10%
antimony(III) fluoride
7783-56-4

antimony(III) fluoride

Dichlorosilane
4109-96-0

Dichlorosilane

A

difluorosilane
13824-36-7

difluorosilane

B

hydrogen
1333-74-0

hydrogen

C

trifluorosilane
13465-71-9

trifluorosilane

D

silicon tetrafluoride
7783-61-1

silicon tetrafluoride

Conditions
ConditionsYield
In neat (no solvent) fluorination of SiH2Cl2 with SbF3 at room temp. for a longer period of time;;A 80%
B n/a
C n/a
D n/a
Dichlorosilane
4109-96-0

Dichlorosilane

cyclohexylmagnesium bromide
931-50-0

cyclohexylmagnesium bromide

dicyclohexylsilane
15493-30-8

dicyclohexylsilane

Conditions
ConditionsYield
In not given79%
In not given79%
Dichlorosilane
4109-96-0

Dichlorosilane

diphenylsilane
775-12-2

diphenylsilane

Conditions
ConditionsYield
With C6H5MgBr In not given77%
With C6H5MgBr In not given77%
Dichlorosilane
4109-96-0

Dichlorosilane

lithium iodide

lithium iodide

diiodosilane
13760-02-6

diiodosilane

Conditions
ConditionsYield
In pentane at -70 - 35℃; for 16h; Temperature; Solvent; Inert atmosphere; Large scale;77%
at 40℃; under 1277.21 - 2311.54 Torr; for 0.08h; Temperature;45.3 g
Dichlorosilane
4109-96-0

Dichlorosilane

N,N,N',N'-tetramethylguanidine
80-70-6

N,N,N',N'-tetramethylguanidine

C12H30N6Si

C12H30N6Si

Conditions
ConditionsYield
In hexane at -78 - 20℃; Inert atmosphere;76%
1-hexene
592-41-6

1-hexene

Dichlorosilane
4109-96-0

Dichlorosilane

1,1-dichloro-1-silaheptane
871-64-7

1,1-dichloro-1-silaheptane

Conditions
ConditionsYield
chloroplatinic acid72%
Dichlorosilane
4109-96-0

Dichlorosilane

silicon nitride

silicon nitride

Conditions
ConditionsYield
With ammonia In dichloromethane byproducts: NH4Cl, H2; the silazane product formed in react. of SiH2Cl2 and gaseous NH3 in solvent, the product heated to 200°C for 1h under Ar then pyrolized at 1150°C for 12 under N2, Si formed only in traces;70%
ammonia
7664-41-7

ammonia

Dichlorosilane
4109-96-0

Dichlorosilane

silicon nitride

silicon nitride

Conditions
ConditionsYield
In diethyl ether byproducts: NH4Cl, H2; the silazane product formed in react. of SiH2Cl2 and gaseous NH3 in solvent, the product heated to 200°C for 1h under Ar then pyrolized at 1150°C for 12 under N2, Si formed only in traces;70%
Na2[nido-dodecahydrodecaborate(2-)]

Na2[nido-dodecahydrodecaborate(2-)]

Dichlorosilane
4109-96-0

Dichlorosilane

Na(7-H-7-SiB10H12)

Na(7-H-7-SiB10H12)

Conditions
ConditionsYield
In diethyl ether byproducts: NaCl, B10H14; condensation of Et2O into borane at -196°C, then condensation of excess of Si-compd. at -196°C, stirring and warming to room temp.overnight; solvent removal (vac.), washing (i-Pr2O), extn. into THF, filtration, evapn. (vac.);70%
Dichlorosilane
4109-96-0

Dichlorosilane

2.6-dimethylpiperidine
504-03-0

2.6-dimethylpiperidine

2,6-dimethylpiperidinochlorosilane
1427523-48-5

2,6-dimethylpiperidinochlorosilane

Conditions
ConditionsYield
With triethylamine In hexane at -20℃;66%
1,4-di-tert-butyl-1,4-diazabutadiene
28227-42-1, 30834-74-3

1,4-di-tert-butyl-1,4-diazabutadiene

Dichlorosilane
4109-96-0

Dichlorosilane

1,3-Di-tert-butyl-2,3-dihydro-1H-[1,3,2]diazasilole

1,3-Di-tert-butyl-2,3-dihydro-1H-[1,3,2]diazasilole

Conditions
ConditionsYield
Stage #1: 1,4-di-tert-butyl-1,4-diazabutadiene With lithium In tetrahydrofuran at 0 - 20℃; for 4h;
Stage #2: Dichlorosilane In tetrahydrofuran; toluene at -20 - 20℃; for 6h;
65%
1-dodecene
112-41-4

1-dodecene

Dichlorosilane
4109-96-0

Dichlorosilane

di-n-dodecyldichlorosilane
18768-06-4

di-n-dodecyldichlorosilane

Conditions
ConditionsYield
Stage #1: 1-dodecene; Dichlorosilane at -78 - 0℃; Inert atmosphere;
Stage #2: dihydrogen hexachloroplatinate(IV) hexahydrate In isopropyl alcohol at 0 - 20℃; Inert atmosphere;
62.5%
isopropylmagnesium bromide
920-39-8

isopropylmagnesium bromide

Dichlorosilane
4109-96-0

Dichlorosilane

di-isopropylsilane
18209-66-0

di-isopropylsilane

Conditions
ConditionsYield
In diethyl ether H2SiCl2 and i-C3H7MgBr in ether; acidic hydrolysis;;60%
In diethyl ether H2SiCl2 and i-C3H7MgBr in ether; acidic hydrolysis;;60%
Na(1+)*{((CH3)3Si)(CH3)C2B4H5}(1-)=Na{((CH3)3Si)(CH3)C2B4H5}

Na(1+)*{((CH3)3Si)(CH3)C2B4H5}(1-)=Na{((CH3)3Si)(CH3)C2B4H5}

Dichlorosilane
4109-96-0

Dichlorosilane

A

{((CH3)3Si)(CH3)C2B4H4}Si
109065-43-2

{((CH3)3Si)(CH3)C2B4H4}Si

B

{((CH3)3Si)(CH3)C2H4B4}SiHCl
109122-66-9

{((CH3)3Si)(CH3)C2H4B4}SiHCl

Conditions
ConditionsYield
With n-butyllithium In tetrahydrofuran addn. of a THF-soln. of 10.08mmol carborane to a soln. of 10.50mmol n-BuLi in THF in vac., react. with SiCl2H2 at -23°C for 2h, removal of THF in vac. at 0°C;; distn. at 0°C; elem. anal.; detn. by MS, IR, (1)H-, (11)B-, (13)C-, (29)Si-NMR;;A n/a
B 58%
Dichlorosilane
4109-96-0

Dichlorosilane

zinc(II) carbonate
743369-26-8

zinc(II) carbonate

1,1,3,3,5,5,7,7,9,9,11,11-dodecahydro-cyclohexasiloxane
295-01-2

1,1,3,3,5,5,7,7,9,9,11,11-dodecahydro-cyclohexasiloxane

Conditions
ConditionsYield
In hexane Cooling;57.6%
fac-(CO)3(2,2'-bipyridine)W(NCEt)
135814-32-3, 158513-30-5

fac-(CO)3(2,2'-bipyridine)W(NCEt)

Dichlorosilane
4109-96-0

Dichlorosilane

fac-(CO)3(2,2'-bipyridine)W(H)(Cl)
135848-51-0

fac-(CO)3(2,2'-bipyridine)W(H)(Cl)

Conditions
ConditionsYield
In dichloromethane N2; 1 equivalent; 10 min;; concd.; filtered; washed with cold CH2Cl2; recrystd. from acetone; elem. anal.;;54%
Dichlorosilane
4109-96-0

Dichlorosilane

Cl2H32O15Si16

Cl2H32O15Si16

Conditions
ConditionsYield
In water at -40 - 20℃; for 1.5h; Inert atmosphere;51%
o-Xylylene dichloride
612-12-4

o-Xylylene dichloride

Dichlorosilane
4109-96-0

Dichlorosilane

1-chloromethyl-2-(trichlorosilylmethyl)benzene
36147-65-6

1-chloromethyl-2-(trichlorosilylmethyl)benzene

Conditions
ConditionsYield
triphenylphosphine In benzene50%
(chloromethyl)triisopropoxysilane
18162-82-8

(chloromethyl)triisopropoxysilane

Dichlorosilane
4109-96-0

Dichlorosilane

1,1,1,5,5,5-hexaisopropoxy-1,3,5-trisilapentane
1469432-28-7

1,1,1,5,5,5-hexaisopropoxy-1,3,5-trisilapentane

Conditions
ConditionsYield
Stage #1: (chloromethyl)triisopropoxysilane With magnesium; ethylene dibromide In tetrahydrofuran at 25 - 35℃; for 8.5h;
Stage #2: Dichlorosilane In tetrahydrofuran; n-heptane at 40 - 50℃; for 7h;
50%

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