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Cas:43121-43-3
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Name: Triadimefon CAS no. : 43121-43-3 Molecular formula: C14H16ClN3O2 Molecular weight:293.7487 Product Quality 12 years of chemical raw materials Mature operation of the industry System stability Data storage Security without vulnerabi
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inquiryProduct name: Triadimefon CAS: 43121-43-3 Molecular structure: C14H16ClN3O2 Molecular weight: 293.7487 Appearance: white powder Storage:Store in cool and dry place, away from sun light. Package: 25kg per bag or 25kg per drum Ap
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inquiryTriadimefon CAS: 43121-43-3 Specification Item Standard Structural data confirmation 1.H-NMR: The data of structure are identical with reference standard 2.HPLC-MS: Ensure the mol
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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4-Amino-1-[1-(4-chloro-phenoxy)-3,3-dimethyl-2-oxo-butyl]-4H-[1,2,4]triazol-1-ium; chloride
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
Conditions | Yield |
---|---|
With hydrogenchloride; sodium nitrite at 0 - 20℃; | 81% |
1,2,4-Triazole
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
Conditions | Yield |
---|---|
With hydrogenchloride; sodium hydroxide; potassium carbonate In water; acetone; toluene | |
With hydrogenchloride; sodium hydroxide; potassium carbonate In water; acetone; toluene | |
With hydrogenchloride; sodium hydroxide; potassium carbonate In water; acetone; toluene |
(R)-1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
Conditions | Yield |
---|---|
In water pH=6.0; Kinetics; Activation energy; pH-value; |
(S)-1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
Conditions | Yield |
---|---|
In water pH=6.0; Kinetics; Activation energy; pH-value; |
1,2,3-triazole
1-chloro-3,3-dimethyl-butan-2-one
4-chloro-phenol
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
Conditions | Yield |
---|---|
Stage #1: 1,2,3-triazole; 1-chloro-3,3-dimethyl-butan-2-one; 4-chloro-phenol With potassium carbonate In dichloromethane at 100℃; for 4h; Stage #2: With sulfuryl dichloride In dichloromethane at 50℃; for 3h; Temperature; Solvent; |
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
Conditions | Yield |
---|---|
With aluminum isopropoxide In isopropyl alcohol at 150℃; for 8h; Temperature; Inert atmosphere; | 99.6% |
4-fluoroboronic acid
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
1-(4'-fluorobiphenyl-4-yloxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
Conditions | Yield |
---|---|
With palladium on activated charcoal; potassium carbonate; CyJohnPhos In N,N-dimethyl acetamide; water at 80℃; for 48h; Suzuki Coupling; Schlenk technique; Inert atmosphere; | 98% |
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
phenylboronic acid
1-(biphenyl-4-yloxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
Conditions | Yield |
---|---|
With palladium on activated charcoal; potassium carbonate; CyJohnPhos In N,N-dimethyl acetamide; water at 105℃; for 2h; Temperature; Suzuki Coupling; Schlenk technique; Inert atmosphere; Microwave irradiation; | 97% |
With palladium on activated charcoal; potassium carbonate; CyJohnPhos In N,N-dimethyl acetamide; water at 80℃; for 48h; Temperature; Time; Concentration; Reagent/catalyst; Suzuki Coupling; Schlenk technique; Inert atmosphere; | 85% |
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
Conditions | Yield |
---|---|
With potassium carbonate In methanol at 25℃; for 1h; Reflux; | 90% |
ethanol
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
Conditions | Yield |
---|---|
for 6h; Reflux; | 85% |
trimethyltin(IV)chloride
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)-1-(4-(trimethylstannyl)phenoxy)butan-2-one
Conditions | Yield |
---|---|
Stage #1: trimethyltin(IV)chloride With ammonia; sodium Stage #2: 1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one for 1.5h; Concentration; Time; Reagent/catalyst; UV-irradiation; | 77% |
water
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
Conditions | Yield |
---|---|
In methanol at 20℃; for 6h; | 73% |
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1,2,4-triazol-4-yl)butanol-2
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1,2,4-triazol-4-yl)butanol-2
Conditions | Yield |
---|---|
With titanium tetrachloride; tetrabutylammonium borohydride In dichloromethane Product distribution; 1) 30 min, room temp.; 2) 1 h, room temp.; also other Lewis acid, other solv.; | |
With tetrabutylammonium borohydride; zinc(II) chloride 1) CH2Cl2, ether, 30 min, room temp.; 2) CH2Cl2, 1 h, room temp.; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; | |
With titanium tetrachloride; tetrabutylammonium borohydride 1) CH2Cl2, 30 min, room temp.; 2) CH2Cl2, 1 h, room temp.; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; | |
With soil at 15℃; Kinetics; Further Variations:; Reagents; Decomposition; |
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-ol
Conditions | Yield |
---|---|
With sodium tetrahydroborate In tetrahydrofuran for 1h; Ambient temperature; | |
With formic acid; triethylamine In cyclohexane | |
With concentrated aqueous hydrochloric acid; sodium borohydrid; sodium hydrogencarbonate In methanol; water |
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
A
1-[(4-chlorophenoxy)methyl]-1,2,4-triazole
B
3,3-dimethyl-1-(1,2,4-triazol-1-yl)-2-butanone
Conditions | Yield |
---|---|
In acetone at 25 - 30℃; for 4h; Decomposition; UV-irradiation; Further byproducts given; |
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
A
1-[(4-chlorophenoxy)methyl]-1,2,4-triazole
B
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-ol
Conditions | Yield |
---|---|
With alluvial soil for 48h; Kinetics; Further Variations:; Reagents; time; Decomposition; UV-irradiation; |
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
Toluene-4-sulfonic acid (S)-1-[(S)-(4-chloro-phenoxy)-[1,2,4]triazol-1-yl-methyl]-2,2-dimethyl-propyl ester
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: NaBH4 / tetrahydrofuran / 1 h / Ambient temperature 2: 1.) NaH / 1.) THF, room temp., 30 min.; 2.) THF,0 deg C to room temp., 1 h. View Scheme |
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
Toluene-4-sulfonic acid (S)-1-[(R)-(4-chloro-phenoxy)-[1,2,4]triazol-1-yl-methyl]-2,2-dimethyl-propyl ester
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: NaBH4 / tetrahydrofuran / 1 h / Ambient temperature 2: 1.) NaH / 1.) THF, room temp., 30 min.; 2.) THF,0 deg C to room temp., 1 h. View Scheme |
hydrogen sulfide
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
Conditions | Yield |
---|---|
With 1-methyl-pyrrolidin-2-one In dichloromethane | |
With 1-methyl-pyrrolidin-2-one In dichloromethane | |
With 1-methyl-pyrrolidin-2-one In dichloromethane | |
With 1-methyl-pyrrolidin-2-one In dichloromethane | |
With 1-methyl-pyrrolidin-2-one In dichloromethane |
phosgene
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
Conditions | Yield |
---|---|
With pyridine In tetrahydrofuran; n-Butyl chloride |
mercury (II) chloride
propargyl bromide
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
aluminium
Conditions | Yield |
---|---|
With ammonium chloride In tetrahydrofuran |
sulfuric acid
aluminum isopropoxide
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-ol
Conditions | Yield |
---|---|
In water; isopropyl alcohol |
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
methyl iodide
1-(4-chloro-phenoxy)-2,3,3-trimethyl-1-[1,2,4]triazol-1-yl-butan-2-ol
Conditions | Yield |
---|---|
With ammonium chloride; magnesium In water; ethyl acetate |
Pentachlorophenol
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
copper(II) 2,3,4,5,6-pentachlorophenolate (3,3-dimethyl-1-(1-H-1,2,4-triazolyl-1)-1-(4-chlorophenoxy)butan-2-one)
Conditions | Yield |
---|---|
With sodium hydroxide In methanol addn. of CuCl2 and L1 to soln. of NaOH and PCP, stirred, 30 min., pptn; filtered off, washed with methanol, dried in air, elem. anal.; |
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
copper(II) chloride (3,3-dimethyl-1-(1-H-1,2,4-triazolyl-1)-1-(4-chlorophenoxy)butan-2-one)
Conditions | Yield |
---|---|
In methanol vigorous stirring, 24 h, pale-blue ppt.; filtered off, washed with methanol and absolute ether, dried in vac., elem. anal.; |
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
A
(R)-1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
B
(S)-1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
Conditions | Yield |
---|---|
With ChiralpakADH column In methanol; carbon dioxide at 25℃; Resolution of racemate; Supercritical conditions; optical yield given as %ee; | |
Resolution of racemate; |
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
Conditions | Yield |
---|---|
With chiralpak IC column In hexane; isopropyl alcohol at 20℃; Thermodynamic data; Solvent; Temperature; Resolution of racemate; enantioselective reaction; |
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
A
1-phenoxy-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)-2-butanone
B
1-(biphenyl-4-yloxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sodium; ammonia 1.2: 1.5 h / UV-irradiation 2.1: bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; cesium fluoride; copper(l) iodide / toluene / 48 h / 100 °C / Schlenk technique; Inert atmosphere View Scheme |
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
1-(4'-fluorobiphenyl-4-yloxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sodium; ammonia 1.2: 1.5 h / UV-irradiation 2.1: bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; cesium fluoride; copper(l) iodide / toluene / 48 h / 100 °C / Schlenk technique; Inert atmosphere View Scheme |
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
A
3,3-dimethyl-1-(4-(naphthalen-1-yl)phenoxy)-1-(1H-1,2,4-triazol-1-yl)butan-2-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sodium; ammonia 1.2: 1.5 h / UV-irradiation 2.1: bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; cesium fluoride; copper(l) iodide / toluene / 48 h / 100 °C / Schlenk technique; Inert atmosphere View Scheme |
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
1-phenoxy-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)-2-butanone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sodium; ammonia 1.2: 1.5 h / UV-irradiation 2.1: bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; cesium fluoride; copper(l) iodide / toluene / 48 h / 100 °C / Schlenk technique; Inert atmosphere View Scheme |
1-Naphthylboronic acid
1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)butan-2-one
3,3-dimethyl-1-(4-(naphthalen-1-yl)phenoxy)-1-(1H-1,2,4-triazol-1-yl)butan-2-one
Conditions | Yield |
---|---|
With palladium on activated charcoal; potassium carbonate; CyJohnPhos In N,N-dimethyl acetamide; water at 80℃; for 48h; Suzuki Coupling; Schlenk technique; Inert atmosphere; | 5 %Chromat. |
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