DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
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Cas:4837-90-5
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inquiry4-Methoxyindole Basic information Product Name: 4-Methoxyindole Synonyms: Indole, 4-methoxy-;1H-INDOL-4-YL METHYL ETHER;4-METHOXY-1H-INDOLE;4-METHOXYLINDOLE;4-METHOXYINDOLE;AKOS JY208261
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inquiry1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W
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inquiryAppearance:White powder Storage:ln stock Package:25kg/Barrel Application:Chemicals Transportation:Express/Sea/Air Port:Any port in china
Cas:4837-90-5
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inquiry1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:Powder Storage:Store in sealed containers at cool & dry pla
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
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The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquirysuperior quality moderate price & quick delivery Appearance:light brown to grey crystalline powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Appli
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Product name: 4-Methoxyindole CAS No.:4837-90-5 Molecule Formula:C9H9NO Molecule Weight:147.17 Purity: 98.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS SPEC
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inquiry4-Methoxyindole Chemical Properties Melting point 69-70 °C (lit.) Boiling point 181-183 °C/24 mmHg (lit.) density 1.1135 (rough estimate) refractive index 1.5310 (estimate) Fp 181-183°C/24mm storage temp. Keep Cold
Cas:4837-90-5
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Cas:4837-90-5
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Wuhu Nuovo Chemical Technology Co., Ltd. was established in August 2014, mainly engaged in the development, production and sales of ionic liquids, ribose, nucleosides, nucleotides and related chemicals; Products are mainly used in new energy, new ma
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We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
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inquiry4-methoxy-1H-indole-2-carboxylic acid
4-methoxy-1H-indole
Conditions | Yield |
---|---|
In quinoline for 0.2h; microwave; | 97% |
With quinoline; copper for 2h; Heating; | 94% |
copper In quinoline for 2h; Heating / reflux; | 94% |
With quinoline; copper oxide-chromium oxide at 200 - 210℃; |
(6-methoxy-2-nitrophenyl)acetonitrile
4-methoxy-1H-indole
Conditions | Yield |
---|---|
With hydrogen; acetic acid; 10% palladium on active carbon In ethanol under 2280 Torr; for 2h; Ambient temperature; | 96% |
With palladium 10% on activated carbon; hydrogen; acetic acid at 20℃; for 12h; |
4-methoxy-1-<(4-methylphenyl)sulfonyl>indole
4-methoxy-1H-indole
Conditions | Yield |
---|---|
With sodium hydroxide In methanol for 12h; Heating; | 96% |
With sodium hydride In N,N-dimethyl acetamide at 60℃; for 3h; Inert atmosphere; | 74% |
Conditions | Yield |
---|---|
With potassium carbonate In methanol; butanone for 6h; Heating; | 95% |
Stage #1: 1H-indol-4-ol With sodium hydride In tetrahydrofuran; mineral oil at 20℃; for 0.5h; Stage #2: methyl iodide In tetrahydrofuran; mineral oil at 20℃; for 1h; | 92% |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 18h; Inert atmosphere; | 91% |
4-methoxy-1H-indole
Conditions | Yield |
---|---|
With carbon monoxide; triphenylphosphine; palladium diacetate In acetonitrile under 3040 Torr; for 20h; Heating; | 89% |
acetaldehyde 3-methoxyphenylhydrazone
A
6-methoxylindole
B
4-methoxy-1H-indole
Conditions | Yield |
---|---|
GIPKh-115 In benzene at 260 - 280℃; (g) phase; | A n/a B 85% |
GIPKh-115 In benzene at 180 - 320℃; (g) phase. Object of study: effect of electronic factors; | A n/a B 85% |
GIPKh-115 at 260 - 280℃; Yield given. Yields of byproduct given; |
4-methoxy-1H-indole
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In ethanol under 3102.9 Torr; for 6h; | 82% |
Conditions | Yield |
---|---|
With C55H49N4OP2Ru In o-xylene at 140℃; under 750.075 Torr; for 48h; Inert atmosphere; Schlenk technique; Green chemistry; | 82% |
With potassium tert-butylate In o-xylene at 140℃; for 36h; Inert atmosphere; | 55% |
3-methoxy-trans-2-[β-(dimethylamino)vinyl]-nitrobenzene
4-methoxy-1H-indole
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In tetrahydrofuran for 1h; | 70% |
With hydrogen; palladium on activated charcoal In methanol; dichloromethane at 20℃; | 63% |
4-methoxy-1H-indole
Conditions | Yield |
---|---|
With potassium tert-butylate In tert-butyl alcohol for 5h; Heating; | 70% |
4-methoxy-1H-indole
Conditions | Yield |
---|---|
With titanium(III) chloride; ammonium acetate buffer for 0.166667h; | 61% |
N-(3-methoxyphenyl)ethenesulfinamide
A
6-methoxylindole
B
4-methoxy-1H-indole
Conditions | Yield |
---|---|
In toluene at 110℃; for 1h; | A 25% B 5% |
tris(piperidino)-methane
6-methoxy-2-nitrotoluene
4-methoxy-1H-indole
Conditions | Yield |
---|---|
With iron; silica gel 1) 120 deg C, 4 h, under vacuum 2) 1 h reflux in toluene-acetic acid; Yield given. Multistep reaction; |
(2-Methoxy-6-nitro-phenyl)-acetaldehyde
4-methoxy-1H-indole
Conditions | Yield |
---|---|
With sodium acetate; iron; acetic acid In ethanol; water for 2h; Heating; Yield given; |
1-[(E)-2-(2-Methoxy-6-nitro-phenyl)-vinyl]-piperidine
4-methoxy-1H-indole
Conditions | Yield |
---|---|
With titanium(III) chloride; ammonium acetate In acetone Yield given; |
Acetic acid 1-chloro-2-(2-methoxy-6-nitro-phenyl)-ethyl ester
4-methoxy-1H-indole
Conditions | Yield |
---|---|
With sodium acetate; iron; acetic acid In ethanol; water for 2h; Heating; |
N-(2,2-Diethoxy-ethyl)-2,2,2-trifluoro-N-(3-methoxy-phenyl)-acetamide
A
6-methoxylindole
B
4-methoxy-1H-indole
Conditions | Yield |
---|---|
With potassium hydroxide; trifluoroacetic anhydride 1) CF3COOH, 56 deg C, 56 h; 2) methanol, room temperature; Yield given. Multistep reaction. Yields of byproduct given; |
6-methoxy-2-nitrotoluene
N,N-dimethyl-formamide dimethyl acetal
4-methoxy-1H-indole
Conditions | Yield |
---|---|
With pyrrolidine; hydrazine hydrate; nickel 1.) DMF, 125 deg C, 3 h; 2.) methanol, 50-60 deg C, 3 h; Yield given. Multistep reaction; |
triethanolamine
m-Anisidine
A
6-methoxylindole
B
4-methoxy-1H-indole
Conditions | Yield |
---|---|
With tin(ll) chloride; ruthenium trichloride; triphenylphosphine In 1,4-dioxane at 180℃; for 20h; Yield given. Yields of byproduct given; |
4-methoxy-1H-indole
Conditions | Yield |
---|---|
at 245 - 250℃; |
methyl 4-methoxy-1H-indole-2-carboxylate
4-methoxy-1H-indole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 99 percent / aq. NaOH / 0.5 h / Heating 2: 94 percent / Cu; quinoline / 2 h / Heating View Scheme |
(Z)-2-azido-3-(2-methoxyphenyl)acrylic acid methyl ester
4-methoxy-1H-indole
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 88 percent / xylene / 1 h / Heating 2: 99 percent / aq. NaOH / 0.5 h / Heating 3: 94 percent / Cu; quinoline / 2 h / Heating View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 68 percent / methanol / 1.5 h / -10 °C 2: 88 percent / xylene / 1 h / Heating 3: 99 percent / aq. NaOH / 0.5 h / Heating 4: 94 percent / Cu; quinoline / 2 h / Heating View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 54 percent / CuI; DMF / acetonitrile / 10 h / 180 °C / 6000.6 - 7500.75 Torr / microwave irradiation 2: 63 percent / H2 / Pd/C / methanol; CH2Cl2 / 20 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 83 percent / CuI; DMF / 3 h / 180 °C / 6000.6 - 7500.75 Torr / microwave irradiation 2: 63 percent / H2 / Pd/C / methanol; CH2Cl2 / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: pyrrolidine / dimethylformamide / 3 h / 125 °C 2: 61 percent / aq. TiCl3, ammonium acetate buffer / 0.17 h View Scheme | |
Multi-step reaction with 2 steps 1: 4 h / 110 °C 2: TiCl3, 4M NH4OAc / acetone View Scheme | |
Multi-step reaction with 2 steps 1: N,N-dimethyl-formamide / 3 h / Reflux 2: zinc; acetic acid; hydrogenchloride / water / 0.5 h / 20 °C View Scheme |
2-bromo-1-methoxy-3-nitrobenzene
4-methoxy-1H-indole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 89 percent / PPh3 / Pd(dba)2 / toluene / 23.5 h / Heating 2: 89 percent / PPh3, CO / Pd(OAc)2 / acetonitrile / 20 h / 3040 Torr / Heating View Scheme | |
Multi-step reaction with 5 steps 1: 88 percent / iron / ethanol; acetic acid / 3.5 h / Heating 2: 72 percent / pyridine / 6 h / Ambient temperature 3: tetrakis(triphenylphosphine)palladium(0) / toluene / 36 h / Heating 4: 68 percent / bis(acetonitrile)palladium chloride, p-benzoquinone, lithium chloride / dimethylformamide / 28 h / 100 - 110 °C 5: 96 percent / 20percent aq. NaOH / methanol / 12 h / Heating View Scheme |
1-tert-butoxycarbonyl-2-iodo-3-methoxyaniline
4-methoxy-1H-indole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 85 percent / CuI, Pd(PPh3)2Cl2 / triethylamine / 24 h / 80 °C 2: 70 percent / t-BuOK / 2-methyl-propan-2-ol / 5 h / Heating View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 41 percent / tBuOK / dimethylformamide / 0.5 h / -20 - -10 °C 2: 96 percent / H2, acetic acid / Pd/C (10percent Pd) / ethanol / 2 h / 2280 Torr / Ambient temperature View Scheme | |
Multi-step reaction with 2 steps 1: potassium tert-butylate / N,N-dimethyl-formamide / 2 h / -20 °C 2: acetic acid; palladium 10% on activated carbon; hydrogen / 12 h / 20 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 7 steps 1: 1.) hydrobromic acid, sodium nitrite, 2.) coopper(I) bromide / 1.) water, 1,4-dioxane, 0 deg C, 15 min, 2.) a) 0 deg C, 15 min, b) 60 deg C, 15 min 2: sodium hydroxide, / aq. ethanol / 14 h / Ambient temperature 3: 88 percent / iron / ethanol; acetic acid / 3.5 h / Heating 4: 72 percent / pyridine / 6 h / Ambient temperature 5: tetrakis(triphenylphosphine)palladium(0) / toluene / 36 h / Heating 6: 68 percent / bis(acetonitrile)palladium chloride, p-benzoquinone, lithium chloride / dimethylformamide / 28 h / 100 - 110 °C 7: 96 percent / 20percent aq. NaOH / methanol / 12 h / Heating View Scheme |
4-methoxy-1H-indole
N,N-dimethyl-formamide
4-methoxyindole-3-carboxaldehyde
Conditions | Yield |
---|---|
Stage #1: N,N-dimethyl-formamide With N-chloro-succinimide; triphenylphosphine In tetrahydrofuran for 1h; Reflux; Stage #2: 4-methoxy-1H-indole In tetrahydrofuran for 1h; Reflux; | 100% |
Stage #1: N,N-dimethyl-formamide With N-chloro-succinimide; triphenylphosphine In tetrahydrofuran at 20℃; Reflux; Stage #2: 4-methoxy-1H-indole In tetrahydrofuran for 1h; Reflux; | 100% |
Stage #1: 4-methoxy-1H-indole; N,N-dimethyl-formamide With trichlorophosphate at 0 - 45℃; for 1.08333h; Inert atmosphere; Stage #2: With sodium hydroxide In water Inert atmosphere; | 95% |
Conditions | Yield |
---|---|
With sodium cyanoborohydride; acetic acid | 100% |
With sodium cyanoborohydride; acetic acid for 0.5h; Ambient temperature; | 98% |
With sodium cyanoborohydride; acetic acid at 20℃; for 0.833333h; | 98% |
Conditions | Yield |
---|---|
Stage #1: 4-methoxy-1H-indole With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Inert atmosphere; Stage #2: bromopentene In N,N-dimethyl-formamide at 0 - 20℃; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
Stage #1: 4-methoxy-1H-indole With sodium hydride In acetonitrile at 0℃; for 0.5h; Stage #2: methyl iodide In acetonitrile at 0 - 20℃; for 16h; | 99% |
With sodium hydride In tetrahydrofuran at 0 - 20℃; | 95% |
With sodium hydride In tetrahydrofuran for 4h; | 82% |
4-methoxy-1H-indole
eschenmoser's salt
(4-methoxy-1H-indol-3-ylmethyl)dimethylamine
Conditions | Yield |
---|---|
In acetic acid; acetonitrile at 20℃; for 2h; | 99% |
Conditions | Yield |
---|---|
In acetonitrile at 20℃; for 3h; Electrochemical reaction; Inert atmosphere; | 99% |
With copper(II) choride dihydrate; oxygen In ethanol at 20℃; for 24h; Irradiation; | 98% |
With iodine In methanol for 1h; | 75% |
4-methoxy-1H-indole
di-tert-butyl dicarbonate
4-methoxyindole-1-carboxylic acid tert-butyl ester
Conditions | Yield |
---|---|
With dmap In acetonitrile at 20℃; for 1h; | 99% |
With dmap; triethylamine In 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran at 20℃; for 11h; | 97% |
With dmap In dichloromethane at 20℃; for 8h; Inert atmosphere; | 95% |
nitrostyrene
4-methoxy-1H-indole
4-methoxy-3-(2-nitro-1-phenylethyl)-1H-indole
Conditions | Yield |
---|---|
With pyrrolidinium 1,1,2,2-tetrafluoro-2-(1,1,2,2-tetrafluoroethoxy)ethanesulfonate at 50℃; for 12h; Friedel Crafts alkylation; | 99% |
4-methoxy-1H-indole
Conditions | Yield |
---|---|
With (11aR)-3,7-di-9-anthracenyl-10,11,12,13-tetrahydro-5-hydroxy-5-oxide diindeno[7,1de:10,70-fg][1,3,2] dioxaphosphocin In toluene at 60℃; for 3h; enantioselective reaction; | 99% |
Conditions | Yield |
---|---|
With trifluoroacetic acid In dichloromethane at 20℃; for 0.0708333h; Flow reactor; | 99% |
With tris(pentafluorophenyl)borate In water at 60℃; for 2h; | 52% |
4-methoxy-1H-indole
1-(1,3-benzothiazol-2-yl)-2,2,2-trifluoroethane-1,1-diol
Conditions | Yield |
---|---|
With (R)-6,6'-bis(2,4,6-triisopropylphenyl)-1,1'-spirobiindanyl-7,7'-diyl hydrogen phosphate In dichloromethane at 20℃; Friedel-Crafts Alkylation; Molecular sieve; enantioselective reaction; | 99% |
4-methoxy-1H-indole
tert-butyldimethylsilyl chloride
Conditions | Yield |
---|---|
Stage #1: 4-methoxy-1H-indole With n-butyllithium In tetrahydrofuran; hexane at -78 - -10℃; for 0.25h; Stage #2: tert-butyldimethylsilyl chloride In tetrahydrofuran; hexane at 0℃; for 3h; | 98% |
Conditions | Yield |
---|---|
With 1,2,2-tris[(4S)-4-iPr-4,5-dihydro-1,3-oxazol-2-yl]propane; copper(II) bis(trifluoromethanesulfonate) In 2-methyl-propan-1-ol at -25℃; for 50h; Friedel-Crafts alkylation of indoles; | 98% |
4-methoxy-1H-indole
diethyl benzalmalonate
(S)-ethyl-2-ethoxycarbonyl-3-[3-(4-methoxyindolyl)]-3-phenyl-propanoate
Conditions | Yield |
---|---|
Stage #1: diethyl benzalmalonate With (3aR,8aS)-2-(3-(3,5-di-tert-butylphenyl)-2,2-bis((S)-4-isopropyl-4,5-dihydrooxazol-2-yl)propyl)-8,8a-dihydro-3aH-indeno[1,2-d]oxazole; copper(II) bis(trifluoromethanesulfonate) In iso-butanol at -25℃; for 0.25h; Friedel Crafts alkylation; Stage #2: 4-methoxy-1H-indole In iso-butanol at -25℃; Friedel Crafts alkylation; optical yield given as %ee; enantioselective reaction; | 98% |
1,1'-bis(4-(S)-isopropyl-1,3-oxazolin-2-yl)ethane*Cu(OTf)2 In water; iso-butanol at -15 - 0℃; | 90% |
4-methoxy-1H-indole
Conditions | Yield |
---|---|
With iodine In methanol at 20℃; for 24h; regioselective reaction; | 98% |
Conditions | Yield |
---|---|
With triphenylphosphine; sodium iodide In acetonitrile at 60℃; for 1.5h; Schlenk technique; Inert atmosphere; | 98% |
With phosphonic acid diethyl ester In acetonitrile at 90℃; for 10h; | 90% |
With 1,2,2,3,4,4-hexamethylphosphetane 1-oxide; phenylsilane In 1,4-dioxane at 40℃; for 1h; Schlenk technique; Sealed tube; Inert atmosphere; | 89% |
4-methoxy-1H-indole
Conditions | Yield |
---|---|
With tetra-(n-butyl)ammonium iodide In acetonitrile at 20℃; for 16h; Inert atmosphere; Irradiation; regioselective reaction; | 98% |
Conditions | Yield |
---|---|
With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate In dichloromethane; water at 20℃; | 97% |
4-methoxy-1H-indole
silver trifluoromethanesulfonate
2-phenylethynylbenzaldehyde p-toluenesulphonylhydrazone
1-(4-methoxyindol-3-yl)-2-amino-3-phenylisoquinolinium triflate
Conditions | Yield |
---|---|
With dysprosium(III) trifluoromethanesulfonate In 1,2-dichloro-ethane at 70℃; Inert atmosphere; | 97% |
4-methoxy-1H-indole
ethyl-3,3,3-trifluoropyruvate
Conditions | Yield |
---|---|
Stage #1: 4-methoxy-1H-indole With C33H52N4O4; zinc trifluoromethanesulfonate In dichloromethane at 35℃; for 0.5h; Stage #2: ethyl-3,3,3-trifluoropyruvate In dichloromethane at 0℃; for 0.5h; Friedel Crafts alkylation; optical yield given as %ee; enantioselective reaction; | 97% |
4-methoxy-1H-indole
methyldiphenylsilane
4-methoxy-1-(methyldiphenylsilyl)-1H-indole
Conditions | Yield |
---|---|
With dodecacarbonyl-triangulo-triruthenium In toluene at 120℃; for 12h; Schlenk technique; Inert atmosphere; | 97% |
With pyridine; zinc trifluoromethanesulfonate In propiononitrile at 80℃; for 15h; Inert atmosphere; | 94% |
4-methoxy-1H-indole
celastrol
Conditions | Yield |
---|---|
With aluminium(III) chloride hexahydrate In dichloromethane at 20℃; for 3h; Friedel-Crafts Alkylation; Sealed tube; | 97% |
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In acetonitrile at 50℃; for 24h; Schlenk technique; Inert atmosphere; Sealed tube; | 97% |
Conditions | Yield |
---|---|
With copper diacetate; 4,4'-di-tert-butyl-2,2'-bipyridine at 90℃; for 24h; Schlenk technique; regioselective reaction; | 97% |
Conditions | Yield |
---|---|
With piperidine; 2-(((S)-1-hydroxy-1,1,3-triphenylpropan-2-ylimino)methyl)-6-chlorophenol; zinc trifluoromethanesulfonate In toluene at 20℃; for 24h; Friedel Crafts alkylation; optical yield given as %ee; enantioselective reaction; | 96% |
4-methoxy-1H-indole
ethyl-3,3,3-trifluoropyruvate
Conditions | Yield |
---|---|
Stage #1: 4-methoxy-1H-indole With C33H52N4O4; zinc trifluoromethanesulfonate In dichloromethane at 35℃; for 0.5h; Stage #2: ethyl-3,3,3-trifluoropyruvate In dichloromethane at 0℃; for 0.5h; Friedel Crafts alkylation; optical yield given as %ee; enantioselective reaction; | 96% |
Conditions | Yield |
---|---|
With sulfuric acid In water at 20℃; for 0.0833333h; Green chemistry; | 96% |
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