DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:5104-49-4
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryflurbiprofen 5104-49-4 Items Standard Result Description White or almost white crystalline powder Conforms
Flurbiprofen Introduction Flurbiprofen is a propionic acid non-steroidal anti-inflammatory medicine. It mainly acts by inhibiting prostaglandin synthase, and has analgesic, anti-inflammatory and antipyretic effects. Flurbiprofen'
Cas:5104-49-4
Min.Order:1 Kilogram
FOB Price: $800.0 / 1050.0
Type:Other
inquiryFlurbiprofen CAS 5104-49-4 Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Food/Feed additives, Fine chemicals in distributing
Cas:5104-49-4
Min.Order:10 Kilogram
FOB Price: $10.0
Type:Trading Company
inquiryXi’an Quanao Biotech Co., Ltd. with 18 years experience in plant extract filed. Product grade: Medicine, Health care product, Cosmetics, Food, Beverage, Feed. Hot selling market: Europe, North America, South America, Middle East, Asia Pacifi
Cas:5104-49-4
Min.Order:50 Gram
FOB Price: $0.7 / 0.9
Type:Manufacturers
inquiryAPIs Appearance:White Crystalline Powder Storage:Store at RT Package:25kg/drum or acc to customers' request Application:(R)-2-Flurbiprofen is the R-isomer of Flurbiprofen (F598700), an anti-inflammatory used as an analgesic. Transportation:acc to c
Cas:5104-49-4
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryThe company has a professional R & D team, mature technology, very competitive prices and stable high quality products for customers to order high quality and low price product efforts! Appearance:White or off-white Solid Storage:Sealed, dry, m
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:5104-49-4
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiry5104-49-4 - Physico-chemical Properties Molecular Formula C15H13FO2 Molar Mass 244.26 Density 1.199±0.06 g/cm3(Predicted) Melting Point 110-113°C(lit.) Boling Point 376.2±
Cas:5104-49-4
Min.Order:1 Gram
FOB Price: $159.0 / 170.0
Type:Lab/Research institutions
inquiryShanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu
Cas:5104-49-4
Min.Order:1 Kilogram
FOB Price: $1.0
Type:Manufacturers
inquiryLIDE PHARMACEUTICALS LIMITED is a professional chemicals and APIs leading manufacturer in China. Our core business line covers APIs, Intermediates, Herb extract, etc.
Cas:5104-49-4
Min.Order:1 Kilogram
FOB Price: $0.9 / 1.0
Type:Lab/Research institutions
inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:5104-49-4
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
Cas:5104-49-4
Min.Order:1 Gram
FOB Price: $6.0 / 9.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:5104-49-4
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:5104-49-4
Min.Order:10 Kilogram
Negotiable
Type:Trading Company
inquiryName Flurbiprofen CAS No. 5104-49-4 EINECS 225-827-6 MF C15H13FO2 MW 244.26 Storage temp. Store at RT MP
We are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED
Cas:5104-49-4
Min.Order:1 Gram
FOB Price: $2.0
Type:Lab/Research institutions
inquiry1,In No Less five years exporting experience. 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Onchem (China) Co.,Ltd is Specia
Cas:5104-49-4
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryWe are the manufacturers and suppliers of API in China, and warehouse in Germany and USA of California, which can quickly and safely deliver to your address 1.High quality and competitive price. 2.Free sample for your evaluation. 3.Promptly delivery
Cas:5104-49-4
Min.Order:10 Gram
FOB Price: $1.3
Type:Trading Company
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
Cas:5104-49-4
Min.Order:1 Kilogram
FOB Price: $105.0 / 120.0
Type:Trading Company
inquiryFlurbiprofen CAS:5104-49-4 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates
Cas:5104-49-4
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:5104-49-4
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiry1.high quality: quality is life. quality is the most important element for all goods. we have a lab doing research in wuhan china. hplc and nmr is available if needed. 2.reasonable price: we provide high quality products with competi
Cas:5104-49-4
Min.Order:10 Gram
Negotiable
Type:Lab/Research institutions
inquiryProduct quality: Our company have high quality product , and also the product we have good manufacture . First of all, this product is of fine quality. Every finish should be checked by quality inspection system.And every one should be also tried
Cas:5104-49-4
Min.Order:1 Metric Ton
FOB Price: $11000.0 / 12000.0
Type:Trading Company
inquiry1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s
Cas:5104-49-4
Min.Order:1 Kilogram
FOB Price: $40.0 / 60.0
Type:Lab/Research institutions
inquiryTriumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Service 1.Own made fine chemical products 2.Out sourcing and quality c
Cas:5104-49-4
Min.Order:100 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryOur Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
ProName: 5104-49-4 flurbiprofen 99% YL CasNo: 5104-49-4 Molecular Formula: C15H13FO2 Appearance: White fine crystalline powder. Application: Intermediates. DeliveryTime:Have stock. Processing period:1 kg/12 weeks. PackAge: 25 kg/barrel.
Cas:5104-49-4
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHubei Yuanmeng Biological Technology Co., Ltd., which is located in Wuhan, China. We are specializing in the exportation of APIs, and plant extracts ect. Our products has been exported to America, Australia, Brazil, the Europe, Middle East and other
Cas:5104-49-4
Min.Order:1 Kilogram
FOB Price: $3.0 / 5.0
Type:Trading Company
inquirymethyl 2-(2-fluoro-4-biphenylyl)propionate
fluorobiprofen
Conditions | Yield |
---|---|
With sulfuric acid; water In 1,4-dioxane at 120℃; for 4h; Inert atmosphere; | 99% |
With potassium hydroxide In ethanol | 75% |
With sodium hydroxide |
Conditions | Yield |
---|---|
Stage #1: C12H16FNO5S; phenylboronic acid With potassium phosphate; bis(tricyclohexylphosphine)nickel(II) dichloride In toluene at 130℃; for 24h; Suzuki-Miyaura coupling reaction; Inert atmosphere; Stage #2: With sulfuric acid In 1,4-dioxane; water at 100℃; for 6h; | 99% |
α-methyl-(2-fluoro-4-biphenylyl)acetonitrile
fluorobiprofen
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol; water at 110℃; for 5h; | 99% |
With sodium hydroxide In ethanol; water at 110℃; for 7h; Inert atmosphere; | 84% |
Stage #1: α-methyl-(2-fluoro-4-biphenylyl)acetonitrile With sodium hydroxide In ethanol; water for 5h; Inert atmosphere; Reflux; Stage #2: With sulfuric acid In ethanol; water at 20℃; Inert atmosphere; | 82% |
With sulfuric acid In water at 100℃; for 3h; |
3-(2-fluorobiphenyl-4-yl)butan-2-one
fluorobiprofen
Conditions | Yield |
---|---|
With sodium hypochlorite at 70℃; for 0.25h; | 95% |
Conditions | Yield |
---|---|
With palladium on activated charcoal; sodium carbonate In water for 6h; Reflux; | 94.98% |
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate In ethanol; water; toluene for 6h; Concentration; Reagent/catalyst; Suzuki Coupling; Inert atmosphere; Reflux; | 81.7 g |
2-(2-fluoro-[1,1'-biphenyl]-4-yl)acetic acid
methyl iodide
fluorobiprofen
Conditions | Yield |
---|---|
Stage #1: 2-(2-fluoro-[1,1'-biphenyl]-4-yl)acetic acid With lithium hexamethyldisilazane In tetrahydrofuran at 20℃; for 0.333333h; Inert atmosphere; Stage #2: methyl iodide In tetrahydrofuran at 20℃; for 0.333333h; Inert atmosphere; | 77% |
With potassium tert-butylate; lithium diisopropyl amide 1.) THF, hexane, -25 deg C, 2 h; Yield given; Multistep reaction; | |
Stage #1: 2-(2-fluoro-[1,1'-biphenyl]-4-yl)acetic acid With n-butyllithium In tetrahydrofuran; hexanes at 0℃; for 0.166667h; Inert atmosphere; Stage #2: methyl iodide In tetrahydrofuran; hexanes Inert atmosphere; |
Conditions | Yield |
---|---|
With (4s,6s)-2,4,5,6-tetra(9H-carbazol-9-yl)isophthalonitrile; triisopropylsilanethiol In N,N-dimethyl-formamide at 0℃; under 3040.2 Torr; for 24h; Irradiation; Sealed tube; | 76% |
fluorobiprofen
Conditions | Yield |
---|---|
With ozone In acetone at -78℃; | 75% |
ethyl 2-(2-fluoro-4-biphenylyl)-propionate
fluorobiprofen
Conditions | Yield |
---|---|
Stage #1: ethyl 2-(2-fluoro-4-biphenylyl)-propionate With water; sodium hydroxide at 95℃; for 3h; Stage #2: In ethyl acetate; Petroleum ether at 65℃; | 72.2% |
With sodium hydroxide Reflux; | |
With lithium hydroxide In tetrahydrofuran; water at 20℃; | 93.9 mg |
trimethylborane
1-bromo-3-fluoro-4-phenylbenzene
Ethyl oxalyl chloride
fluorobiprofen
Conditions | Yield |
---|---|
Stage #1: 1-bromo-3-fluoro-4-phenylbenzene With magnesium Stage #2: Ethyl oxalyl chloride Stage #3: trimethylborane Further stages; | 67% |
C12H16FNO5S
phenylboronic acid
A
fluorobiprofen
B
methyl 2-(2-fluoro-4-biphenylyl)propionate
Conditions | Yield |
---|---|
With potassium phosphate; bis(tricyclohexylphosphine)nickel(II) dichloride In toluene at 130℃; for 24h; Suzuki-Miyaura coupling reaction; Inert atmosphere; | A 29% B 56% |
diazomethane
carbon dioxide
4-ethenyl-2-fluorobiphenyl
fluorobiprofen
Conditions | Yield |
---|---|
Stage #1: carbon dioxide; 4-ethenyl-2-fluorobiphenyl With diethylzinc In N,N-dimethyl acetamide; toluene at 20 - 80℃; for 24h; Inert atmosphere; Sealed tube; Stage #2: diazomethane | 55% |
Conditions | Yield |
---|---|
With copper(l) iodide; cesium fluoride; sodium t-butanolate; 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride In 2-methyltetrahydrofuran at 120℃; for 24h; Sealed tube; | 53% |
Stage #1: carbon dioxide; C20H24BFO2 With potassium tert-butylate In tetrahydrofuran; toluene at -78 - 20℃; under 760.051 Torr; for 3h; Stage #2: With hydrogenchloride In tetrahydrofuran; water; toluene |
Conditions | Yield |
---|---|
In acetone; benzene | 38.5% |
diethyl 2-(2-fluorobiphenyl-4-yl)-2-methylmalonate
fluorobiprofen
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol; water for 6h; Reflux; | 34% |
Multi-step reaction with 2 steps 1.1: sodium hydroxide / ethanol / 6 h / 20 °C / Inert atmosphere; Schlenk technique 1.2: Inert atmosphere; Schlenk technique 2.1: Escherichia coli arylmalonate decarboxylase; tris hydrochloride / 1 h / 30 °C / pH 8.5 / Inert atmosphere; Schlenk technique View Scheme |
diphenyl N-<2-(2-fluoro-4-biphenylyl)-1-pyrrolidinopropylidene>phosphoramidate
fluorobiprofen
Conditions | Yield |
---|---|
With potassium hydroxide In ethylene glycol for 8h; Heating; | 30% |
Conditions | Yield |
---|---|
In acetone; benzene | 30% |
fluorobiprofen
Conditions | Yield |
---|---|
With potassium carbonate In water Yield given; |
Conditions | Yield |
---|---|
at 15℃; Thermodynamic data; Equilibrium constant; ΔG298, ΔH, ΔS298; stability constant; dissolution rate; other temperatures; |
fluorobiprofen
(S)-(+)-flurbiprofen
Conditions | Yield |
---|---|
Stage #1: fluorobiprofen With (S)-1-phenyl-ethylamine In methanol; toluene at 20 - 60℃; for 0.166667h; Stage #2: In methanol; toluene at 0 - 5℃; for 1h; | 85.2% |
Stage #1: fluorobiprofen With (S)-1-phenyl-ethylamine In toluene at 60℃; for 0.5h; Stage #2: With ammonium hydroxide In ethyl acetate for 0.166667h; | 66% |
Multi-step reaction with 4 steps 1.1: 99 percent / H2SO4 / 3 h / Heating 2.1: diisopropylamine; n-BuLi / tetrahydrofuran; hexane / 0.83 h / -78 °C 2.2: 90 percent / hexane; tetrahydrofuran / 2 h / 0 °C 3.1: 85 percent / KOH / H2O; ethanol / 1 h / 0 °C 4.1: Tris-HCl buffer; arylmalonate decarboxylaze EC 4.1.1.76 / H2O; ethanol / 0.67 h / 30 °C / pH 8.0 View Scheme |
fluorobiprofen
2-(2-fluoro-biphenyl-4-yl)-propan-1-ol
Conditions | Yield |
---|---|
Stage #1: fluorobiprofen With triethanolamine; isobutyl chloroformate In tetrahydrofuran for 1h; Stage #2: With sodium tetrahydroborate In tetrahydrofuran; water at -20 - 0℃; for 2.25h; | 95% |
Multi-step reaction with 2 steps 1: 94 percent / SOCl2 / 6 h / Heating 2: 78 percent / LAH / diethyl ether / 8 h / Heating View Scheme | |
With dimethylsulfide borane complex |
fluorobiprofen
α-Methyl-3-fluoro-4-phenylbenzeneacetyl chloride
Conditions | Yield |
---|---|
With thionyl chloride In DMF (N,N-dimethyl-formamide); 1,2-dichloro-ethane Heating / reflux; | 100% |
With oxalyl dichloride In benzene for 3h; Heating; | |
With phosphorus pentachloride In tetrachloromethane at 40℃; for 0.5h; |
fluorobiprofen
2-(2-fluoro-[1,1′-biphenyl]-4-yl)propanehydrazide
Conditions | Yield |
---|---|
Stage #1: fluorobiprofen With hydrazine hydrate; 1,1'-carbonyldiimidazole In tetrahydrofuran for 0.166667h; Stage #2: With hydrazine hydrate In tetrahydrofuran for 4h; Reflux; | 89% |
Multi-step reaction with 2 steps 1: sulfuric acid / 3 h / Reflux 2: hydrazine hydrate / ethanol / 2 h / Reflux View Scheme | |
Multi-step reaction with 2 steps 1: sulfuric acid / 0.25 h / Reflux; Microwave irradiation 2: hydrazine hydrate / ethanol / Reflux; Microwave irradiation View Scheme | |
Multi-step reaction with 2 steps 1: sulfuric acid / 6 h / Reflux 2: hydrazine hydrate / ethanol / 8 h / Reflux View Scheme | |
Multi-step reaction with 2 steps 1: sulfuric acid / 3 h / Reflux 2: hydrazine hydrate / 2 h / Reflux View Scheme |
methanol
fluorobiprofen
methyl 2-(2-fluoro-4-biphenylyl)propionate
Conditions | Yield |
---|---|
With sulfuric acid for 3h; Heating; | 99% |
With sulfuric acid for 0.25h; Reflux; Microwave irradiation; | 98.8% |
With sulfuric acid for 3h; Reflux; | 95% |
fluorobiprofen
1,2:3,4-di-O-isopropylidene-α-D-galactopyranose
diacetone 6'-O-flurbiprofen-D-galactopyranoside
Conditions | Yield |
---|---|
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap In dichloromethane at 20℃; for 12h; | 61% |
fluorobiprofen
Conditions | Yield |
---|---|
Stage #1: fluorobiprofen With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane; N,N-dimethyl-formamide at 25℃; for 0.5h; Stage #2: 2-selenocyanatopropanamine hydrobromide In dichloromethane; N,N-dimethyl-formamide at 25℃; for 16h; | 65% |
Stage #1: fluorobiprofen With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane; N,N-dimethyl-formamide at 25℃; for 0.5h; Inert atmosphere; Stage #2: 2-selenocyanatopropanamine hydrobromide In dichloromethane; N,N-dimethyl-formamide at 25℃; for 16h; Inert atmosphere; | 62% |
Stage #1: fluorobiprofen With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane; N,N-dimethyl-formamide at 25℃; for 0.5h; Stage #2: 2-selenocyanatopropanamine hydrobromide In dichloromethane; N,N-dimethyl-formamide at 25℃; for 16h; |
fluorobiprofen
Conditions | Yield |
---|---|
Stage #1: fluorobiprofen With ascorbic acid In ethanol; water at 70 - 75℃; Large scale; Stage #2: With sodium hydroxide In ethanol; water for 1.5h; Large scale; | 95.7% |
fluorobiprofen
Conditions | Yield |
---|---|
With sodium methylate In methanol at 65℃; for 1.5h; Large scale; | 94.8% |
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In acetonitrile at 20℃; for 24h; | 91% |
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; for 5h; | 100% |
Conditions | Yield |
---|---|
With tributylphosphine In dichloromethane at -15℃; for 3h; Inert atmosphere; | 73% |
With tributylphosphine In dichloromethane at -15℃; for 3h; Inert atmosphere; | 73% |
Conditions | Yield |
---|---|
Stage #1: fluorobiprofen With oxalyl dichloride at 70℃; for 1h; Inert atmosphere; Stage #2: dichlorodihydroxydiamineplatinum In tetrahydrofuran at 70℃; for 2h; Temperature; Darkness; | 92.3% |
N-tert-butoxycarbonyl-3-aminopropanol
fluorobiprofen
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; Cooling with ice; | 94% |
Conditions | Yield |
---|---|
Stage #1: acetyl chloride With aluminum (III) chloride In dichloromethane at 0℃; for 0.5h; Friedel-Crafts Acylation; Stage #2: fluorobiprofen In dichloromethane at 20℃; for 3h; Friedel-Crafts Acylation; | 64.1% |
fluorobiprofen
methyl glycyrrhetinate
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; | 55% |
fluorobiprofen
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 40℃; Inert atmosphere; Sealed tube; | 84% |
Conditions | Yield |
---|---|
Stage #1: fluorobiprofen With 1,1'-carbonyldiimidazole In dichloromethane at 0 - 5℃; for 2h; Stage #2: 4-hydroxybenzenesulphonamide With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane at 20℃; for 6h; | 79% |
2-Methanesulfonyl-ethylamine
fluorobiprofen
Conditions | Yield |
---|---|
Stage #1: fluorobiprofen With 1,1'-carbonyldiimidazole In dichloromethane at 0 - 5℃; for 2h; Stage #2: 2-Methanesulfonyl-ethylamine In dichloromethane | 77% |
Conditions | Yield |
---|---|
Stage #1: fluorobiprofen With 1,1'-carbonyldiimidazole In dichloromethane at 0 - 5℃; for 2h; Stage #2: benzenesulfonamide With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane at 20℃; for 6h; | 79% |
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 0.5h; | 83% |
fluorobiprofen
Conditions | Yield |
---|---|
With dmap; triethylamine; trichlorophosphate In dichloromethane at 20℃; | 80% |
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 0.5h; | 72% |
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